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2022 ◽  
Author(s):  
Shuaipu Wang ◽  
Jie Liang

Abstract In order to reduce the delamination damage of carbon fiber reinforced polymer (CFRP) drilling and improve the drilling quality. A variable feed drilling method based on sinusoidal curve was proposed, that is, when the drill at a distance of 1mm from the hole exit, the feed rate of the drill would be reduced according to the rule of sinusoidal curve. The method is compared with the traditional feed drilling by experiment, and the influence of the variable feed drilling on thrust force, delamination factor, surface quality, surface roughness of hole wall and exit hole wall morphology are analyzed. The results show that compared with constant-feed drilling, the variable-feed drilling based on sinusoidal curve reduces the thrust force near the hole exit, and greatly improves the delamination factor, surface quality and hole wall morphology at the exit. But the influence on the hole wall roughness is not particularly obvious.


2022 ◽  
Author(s):  
Le Anh Duc ◽  
Pham Minh Hieu ◽  
Nguyen Minh Quang

Abstract The material yttrium aluminum oxide (Y3Al5O12) is one of the materials commonly used in laser devices. For application in optical devices, it is necessary to produce ultra-precise surface quality, however, Y3Al5O12 material belongs to the group of difficult-to-machine materials with high brittleness and hardness. Therefore, it is very difficult to ensure that the main criterion when finishing this material to produce a quality surface in the nanometer form with the ability to remove the material is very difficult. To solve this problem, this work provided a new chemical - mechanical polishing mixture. The proposed polishing mixture of ZrO2, Na2SiO3–5H2O, and MgO abrasives has a weight ratio of 8%, 5% and 1% respectively, with the remainder being deionized water. The surface result after polishing is obtained with a material removed rate of 38 (nm/min) along with an ultra-smooth surface produced with Ra = 0.41 nm. With the help of X-ray photoelectron spectroscopy (XPS) method before and after polishing by CMS, the reaction mechanisms were elucidated. Analytical results show that Y3Al5O12 material produces YOOH and AlOOH in Na2SiO3 solution, then combines with –Si–OH to form (Y-Si) and (Al-Si) with significantly reduced hardness compared to other Y3Al5O12 materials, these products combine with MgO to form montmorillonites (3MgO–Al2O3–3SiO2–3Y2O3–5Al2O3). With this formation, the surface layer of Y3Al5O12 material becomes soft and is easily removed by ZrO2 abrasive particles under the influence of mechanical polishing, resulting in superfine surfaces are generated from the proposed CMS model.


Author(s):  
Zhao Ding ◽  
Shiwei Niu ◽  
Yao Qingyu ◽  
Yongguang Wang ◽  
Huaijun Guan ◽  
...  

Abstract Overcoming the low fabricating efficiency of traditional chemical mechanical polishing (CMP) for Gallium nitride (GaN) is a challenge owing to its high hardness, high brittleness, and chemical inertness. Here, electrochemical etching is proposed to increase the material removal rate and acquire a high-quality surface on GaN wafers. To reveal the synergistic etching mechanism of oxidizing agent and corrosion inhibitor on the GaN wafers, electrochemical etching experiments were carried out. The optimal etching solution contained 4 wt% H2O2 and 10 mmol/L purified terephthalic acid. Experiments with various polishing parameters were comparatively investigated to verify the auxiliary effect of etching and determine the ideal parameters. Cathodoluminescence spectroscopy shows that the electrochemical etching removes the SSDs completely and the CMP process with befitting parameters does not induce supernumerary SSDs.


2021 ◽  
Author(s):  
Sachini Perera ◽  
Alejandra Durand-Silva ◽  
Ashele Remy ◽  
Shashini Diwakara ◽  
Ronald Smaldone

Vat photopolymerization is a versatile 3D printing method that produces parts using polymeric materials with uniform mechanical properties, high quality surface finish and high-resolution features. However, it is challenging to make composite materials with vat photopolymerization mainly due to the imperfect filler dispersion in the photo resin. Herein, we describe a methodology to incorporate aramid nanofibers (ANFs) into a 3D printable photoresin as a dispersion, followed by a solvent exchange process that limits anisotropic shrinkage and cracking of the printed polymer. By incorporating 0.60 wt.% of ANFs, both the tensile strength and toughness increased by 264 % and 219 % respectively, while the Young’s modulus had a 406 % increase compared to the control photoresin.


Coatings ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1381
Author(s):  
Ruozheng Wang ◽  
Qiang Wei ◽  
Jie Li ◽  
Jiao Fu ◽  
Yiwei Liu ◽  
...  

We report the fabrication of bottom gate a-IGZO TFTs based on HfO2 stacked dielectrics with decent electrical characteristics and bias stability. The microscopic, electrical, and optical properties of room temperature deposited a-IGZO film with varied oxygen content were explored. In order to suppress the bulk defects in the HfO2 thin film and hence maximize the quality, surface modification of the SiNx film was investigated so as to achieve a more uniform layer. The root mean square (RMS) roughness of SiNx/HfO2/SiNx (SHS) stacked dielectrics was only 0.66 nm, which was reduced by 35% compared with HfO2 single film (1.04 nm). The basic electrical characteristics of SHS-based a-IGZO TFT were as follows: Vth is 2.4 V, μsat is 21.1 cm2 V−1 s−1, Ion/Ioff of 3.3 × 107, Ioff is 10−11 A, and SS is 0.22 V/dec. Zr-doped HfO2 could form a more stable surface, which will decrease the bulk defect states so that the stability of device can be improved. It was found that the electrical characteristics were improved after Zr doping, with a Vth of 1.4 V, Ion/Ioff of 108, μsat of 19.5 cm2 V−1 s−1, Ioff of 10−12 A, SS of 0.18 V/dec. After positive gate bias stress of 104 s, the ΔVth was decreased from 0.43 V (without Zr doping) to 0.09 V (with Zr doping), the ΔSS was decreased from 0.19 V/dec to 0.057 V/dec, respectively, which shows a meaningful impact to realize the long-term working stability of TFT devices.


Materials ◽  
2021 ◽  
Vol 14 (20) ◽  
pp. 6178
Author(s):  
Shikang Gao ◽  
Li Zhou ◽  
Guangda Sun ◽  
Huihui Zhao ◽  
Xiaolong Chu ◽  
...  

In the present study, 8 mm-thick 5251 aluminum alloy was self-reacting friction stir welded (SRFSW) employing an optimized friction stir tool to analyze the effect of welding speed from 150 to 450 mm/min on the microstructure and mechanical properties at a constant rotation speed of 400 rpm. The results indicated that high-quality surface finish and defect-free joints were successfully obtained under suitable process parameters. The microhardness distribution profiles on the transverse section of joint exhibited a typical “W” pattern. The lowest hardness values located at the heat-affected zone (HAZ) and the width of the softened region decreased with increasing welding speed. The tensile strength significantly decreased due to the void defect, which showed mixed fracture characteristics induced by the decreasing welding speed. The average tensile strength and elongation achieved by the SRFSW process were 242.61 MPa and 8.3% with optimal welding conditions, and the fracture surface exhibited a typical toughness fracture mode.


2021 ◽  
Vol 119 (12) ◽  
pp. 122101
Author(s):  
Evyn L. Routh ◽  
Mostafa Abdelhamid ◽  
Peter Colter ◽  
N. A. El-Masry ◽  
S. M. Bedair

PLoS ONE ◽  
2021 ◽  
Vol 16 (8) ◽  
pp. e0254974
Author(s):  
Orlando Cómbita-Heredia ◽  
Connor J. Gulbronson ◽  
Ronald Ochoa ◽  
Edwin Javier Quintero-Gutiérrez ◽  
Gary Bauchan ◽  
...  

Studies of female genital structures have generally lagged behind comparable studies of male genitalia, in part because of an assumption of a lower level of variability, but also because internal genitalia are much more difficult to study. Using multiple microscopy techniques, including video stereomicroscopy, fluorescence microscopy, low-temperature scanning electron microscopy (LT-SEM), and confocal laser scanning microscopy (CLSM) we examined whether the complex sperm transfer structures in males of Megalolaelaps colossus (Acari: Mesostigmata) are matched by similarly complex internal structures in the female. While both LT-SEM and CLSM are well suited for obtaining high-quality surface images, CLSM also proved to be a valuable technique for observing internal anatomical structures. The long and coiled sperm transfer organ on the chelicera of the males (spermatodactyl) largely matches an equally complex, but internal, spiral structure in the females in shape, size, and direction. This result strongly suggests some form of genital coevolution. A hypothesis of sexual conflict appears to provide the best fit for all available data (morphology and life history).


2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Mohammad Javad Hooshmand ◽  
Saeed Mansour ◽  
Amin Dehghanian

Purpose The advancement of additive manufacturing technologies has resulted in producing parts of high quality and reduced manufacturing time. This paper aims to achieve a simultaneous optimal solution for build time and surface roughness as the output data and also to find the best values for the input data consisting of build orientation, extrusion width, layer thickness, infill percentage and raster angle. Design/methodology/approach For this purpose, the effects of process parameters on the response variables were investigated by the design of experiments approach to develop empirical models using response surface methodology. The experimental parts of this research were conducted using an inexpensive and locally assembled fused filament fabrication (FFF) machine. A total of 50 runs for 4 different geometries, namely, cylinder, prism, 3DBenchy and twist gear vase, were performed using the rotatable central composite design, and each process parameters were investigated in two levels to develop empirical models. Also, a novel optimization method, namely, the posterior-based method, was accomplished to find the best values for the response variables. Findings The results demonstrated that not only the build orientation and layer thickness have notable effects on both response variables but also build time is dependent on extrusion width and infill percentage. Low infill percentage and high extrusion width resulted in increasing build time. By reducing layer thickness and infill percentage while increasing extrusion width, parts of high-quality surface finish and reduced built time were produced. Optimum process parameters were found to be of build direction of 0°, extrusion width of 0.61 mm, layer thickness of 0.22 mm, infill percentage of 20% and raster angle of 0°. Originality/value Through the developed empirical models and by minimizing build orientation and layer thickness, and also considerations for process parameters, parts of high-quality surface finish and reduced built time could be produced on FFF machines. To compensate for increased build time because of reduction in layer thickness, extrusion width and infill percentage must have their maximum and minimum value, respectively.


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