scholarly journals Physicochemical characterization of natural honeys from different regions in Slovakia

2009 ◽  
Vol 57 (2) ◽  
pp. 125-134
Author(s):  
Marián Sudzina ◽  
Martin Melich ◽  
Vladimíra Kňazovická ◽  
Soňa Felšöciová ◽  
Guillermo Kociubinski ◽  
...  
Keyword(s):  
Water Activity ◽  
Ph Value ◽  
Physicochemical Characterization ◽  
Physicochemical Characteristics ◽  
Invertase Activity ◽  
Glucose Content ◽  
Codex Alimentarius ◽  
Geographical Regions ◽  
Saccharose Content

This study is intended to determine the physicochemical characteristics of Slovakian honeys, and compare them with specifications described in the Codex Alimentarius Standard, the European Ho­ney directive, the Slovak Codex Alimentarius and Slovak standard No. 1/2006. In addition, we tried to find out correlations between individual constituents of honeys. Physicochemical characterization was carried out following the harmonized methods dictated by the International Honey Commission IHC. Honey samples (n=50) were collected from three honey types (blossom, blends, honeydew), and from the three main Slovakian geographical regions (named ‘east’, ‘middle’ and ‘west’). The phy­si­co­che­mi­cal evaluation included moisture, reduced sugars, proline, hydroxymethylfurfural (HMF), conductivity, diastase and invertase activity, pH and water activity, following the techniques proposed by the European Honey Commission (EHC). The moisture content in the honey varied from 15.26 to 17.65 %, HMF levels ranged from 21.83 to 63.00 mg . kg−1, the diastase activity varied from 21.01 DN to 36.67, invertase activity varied from 121.73 to 164.11 U . kg−1, the proline content varied from 426.56 to 531.79 mg . kg−1,the fructose content values were found from 36.33 to 40.20 g . 100g−1, the glucose content values ranged from 27.67 to 31.00 g . 100g−1, the values of saccharose content were from 0.15 to 0.37 g . 100g−1, the conductivity varied from 29.48 to 97.24 mS . cm−1,the pH value varied from 4.06 to 4.80 and the water activity content varied from 0.55 to 0.57. Significant differences (P ≤ 0.05) were found between HMF and fructose, glucose and saccharose and conductivity and pH, significant differences (P ≤ 0.01) between fructose and glucose and significant differences (P ≤ 0.001) were found between HMF and conductivity. Between blossom honey and honeydew honey were found statistical significant differences in HMF (P ≤ 0.05) and conductivity between honeydew honey and blossom honey (P ≤ 0.001). Among regions were determined statistical differences between HMF and invertase (P ≤ 0.05) and conductivity (P ≤ 0.01).

scholarly journals THE PHYSICOCHEMICAL CHARACTERISTICS OF RECYCLED-PLASTIC PELLETS OBTAINED FROM DISPOSABLE FACE MASK WASTES

2021 ◽  
Vol 23 (1) ◽  
pp. 16
Author(s):  
Vienna Saraswaty ◽  
Rossy Choerun Nissa ◽  
Bonita Firdiana ◽  
Akbar Hanif Dawam Abdullah
Keyword(s):  
Tensile Strength ◽  
Physicochemical Characterization ◽  
Face Mask ◽  
Physicochemical Characteristics ◽  
Scanning Calorimetry ◽  
Elongation At Break ◽  
Ft Ir ◽  
The Government ◽  
Plastic Pellets

THE PHYSICOCHEMICAL CHARACTERISTICS OF RECYCLED-PLASTIC PELLETS OBTAINED FROM DISPOSABLE FACE MASK WASTES. The government policy to wear a face mask during the COVID-19 pandemic has increased disposable face mask wastes. Thus, to reduce such wastes, it is necessary to evaluate the physicochemical characteristics of disposable face masks wastes before the recycling process and the recycled products. In this study, physicochemical characterization of the 3-ply disposable face masks and the recycled plastic pellets after disinfection using 0.5% v/v sodium hypochlorite were evaluated. A set of parameters including the characterization of surface morphology by a scanning electron microscope (SEM), functional groups properties by a fourier transform infra-red spectroscopy (FT-IR), thermal behavior by a differential scanning calorimetry (DSC), tensile strength and elongation at break were evaluated. The surface morphological of each layer 3-ply disposable face mask showed that the layers were composed of non-woven fibers. The FT-IR evaluation revealed that 3-ply disposable face mask was made from a polypropylene. At the same time, the DSC analysis found that the polypropylene was in the form of homopolymer. The SEM analysis showed that the recycled plastic pellets showed a rough and uneven surface. The FT-IR, tensile strength and elongation at break of the recycled plastic pellets showed similarity with a virgin PP type CP442XP and a recycled PP from secondary recycling PP (COPLAST COMPANY). In summary, recycling 3-ply disposable face mask wastes to become plastic pellets is recommended for handling disposable face mask wastes problem.

ISOLATION OF A STEROID-LIKE SUBSTANCE FROM URINE AND CITROUS FRUITS

1958 ◽  
Vol 36 (1) ◽  
pp. 869-881 ◽  
Author(s):  
Wojciech Nowaczynski ◽  
Thomas Sandor ◽  
Erich Koiw ◽  
R. Norman Jones ◽  
Jacques Genest
Keyword(s):  
Physicochemical Characterization ◽  
Oxidative Degradation ◽  
Physicochemical Characteristics ◽  
Fruit Juices ◽  
Free Form ◽  
Elementary Analysis ◽  
Males And Females ◽  
Normal Males ◽  
Partial Chemical

The isolation and the partial chemical and physicochemical characterization of a chloroform-soluble substance obtained from human urine and citrous fruit juices are presented. The urinary compound, designated as compound III, is present mostly as a conjugate hydrolyzed by animal β-glucuronidase whereas it is in free form in fruit juices. It is present in the urine of normal males and females and in a number of pathological conditions. Its urinary excretion is significantly increased as a result of diets rich in potassium (250 meq./day). In various paper chromatographic systems, the compound has a mobility similar to that of aldosterone. Detailed study of its chemical and physicochemical characteristics, including oxidative degradation and infrared and elementary analysis, suggests a steroidal or sesquiterpinoidal structure. However, at the present time, the data obtained do not permit the final elucidation of the chemical formula of compound III.

scholarly journals Chemical and Physicochemical Characterization of Winter Squash (Cucurbita moschata D.)

2011 ◽  
Vol 39 (1) ◽  
pp. 34 ◽  
Author(s):  
Noelia JACOBO-VALENZUELA ◽  
Jose de Jesus ZAZUETA-MORALES ◽  
Jose Alberto GALLEGOS-INFANTE ◽  
Floridelia AGUILAR-GUTIERREZ ◽  
Irma Leticia CAMACHO-HERNANDEZ ◽  
...  
Keyword(s):  
Animal Feed ◽  
Physicochemical Characterization ◽  
Physicochemical Characteristics ◽  
Total Phenolic ◽  
Cucurbita Moschata ◽  
Mineral Contents ◽  
Large Variability ◽  
Nutritional Needs ◽  
Winter Squash

Winter squash cv 'Cehualca' (Cucurbita moschata Duchense) is a seasonal crop that has been used as food and animal feed. The objective of the present study was to characterize physical, chemical and physicochemical properties of the winter squash cv 'Cehualca'. Morphological, chemical and physicochemical analyses were performed, including fiber, carotenoids, phenolic and mineral contents in the winter squash. The morphological analysis showed that the squash 'Cehualca' did not have a homogeneous morphology. Data about their physical and physicochemical characteristics showed large variability. Also, high content of carotenoids and dietary fiber was observed in squash. The oil and total phenolic content was low in comparison with other fruits. The mineral content exceeded the values recommended to meet the nutritional needs of consumers, except for sodium (both in pulp and shell), potassium and magnesium in the shell.

scholarly journals Physicochemical characterization of the pulp oil of bacuri Attalea phalerata Mart. ex Spreng. (Arecaceae)

2020 ◽  
Vol 21 (3) ◽  
pp. 1-11
Author(s):  
Michelle Cardoso Coimbra ◽  
Débora Maria Moreno Luzia ◽  
Neuza Jorge
Keyword(s):  
Fatty Acids ◽  
Gas Chromatography ◽  
Refractive Index ◽  
Fatty Acid ◽  
Potassium Hydroxide ◽  
High Performance ◽  
Physicochemical Characterization ◽  
Physicochemical Characteristics ◽  
Total Phenolic

The aim of the study was to characterize the pulp oil of bacuri Attalea phalerata Mart. ex Spreng. (Arecaceae) according to official analytical methods. Total phenolic and carotenoids contents were evaluated by spectrophotometry, and tocopherols composition by high-performance liquid chromatography. The fatty acid profile was obtained through gas chromatography from samples transesterified with potassium hydroxide in methanol and n-hexane. According to the proximate composition, bacuri pulp contained 41.5 % carbohydrates and 39.2 % lipids. Regarding its physicochemical properties, the oil showed a free fatty acids content of 0.7 %, a peroxide value of 1.4 meq/kg, a refractive index of 1.463, an iodine number of 84.3 g I2/100 g, a saponification number of 193.5 mg KOH/g, an unsaponifiable matter of 0.5 %, and 48.7 h of oxidative stability. Total phenolic, carotenoids, and tocopherols contents recorded values of 2.4 mg GAE/g, 243.0 µg/g, and 86.8 mg/kg, respectively. The bacuri oil showed a fatty acid composition similar to olive oil and a high percentage of unsaturation, finding 67.3 % of monounsaturated acids, and 11.3 % of polyunsaturated acids. The main fatty acids were oleic (67.3 %), palmitic (13.3 %), and linoleic (10.5 %). Due to its physicochemical characteristics, bacuri oil has a great potential to be used in food preparations, such as salad oil or in margarine formulation.

scholarly journals Physicochemical characterization of different trademarks of compound Yerba Maté and their herbs

2007 ◽  
Vol 50 (4) ◽  
pp. 735-741 ◽  
Author(s):  
Griselda Patricia Scipioni ◽  
Darío Jorge Ferreyra ◽  
Miguel Eduardo Schmalko
Keyword(s):  
Moisture Content ◽  
Physicochemical Characterization ◽  
Water Extract ◽  
Physicochemical Characteristics ◽  
Yerba Mate ◽  
Caffeine Concentration ◽  
Water Extracts ◽  
Aromatic Herbs

The objectives of this study were to evaluate the physicochemical characteristics of the main herbs used in the mixture of yerba maté with other aromatic herbs and the characterization of the trademarks of compound yerba maté. Moisture, water extract, total ash, acid-insoluble ash and caffeine concentration were determined. Results showed higher values of moisture content, total and aci-insoluble ash and lower water extracts in the herbs. Determinations were carried out in nine trademarks of compound yerba maté. In most cases they complied with the standards of the country with the exception of one trademark from Argentina.

scholarly journals Evaluation of freshness and physicochemical characteristics of blankets of pirarucu (Arapaima gigas) bred in captivity at different ages in relation to the seasons

2021 ◽  
Author(s):  
Krishna Rodrigues de Rosa ◽  
Alessandra Almeida da Silva ◽  
Wander Miguel de Barros ◽  
Anaqueli Lucia Pedroso ◽  
Maria Fernanda Evelin Ferreira ◽  
...  
Keyword(s):  
Water Activity ◽  
Shear Force ◽  
Physicochemical Characterization ◽  
Physicochemical Characteristics ◽  
Water Retention Capacity ◽  
Retention Capacity ◽  
Mato Grosso ◽  
Different Ages ◽  
In Captivity ◽  
Inspection Service

This study aimed to evaluate the freshness and physicochemical characterization of pirarucu blankets at different ages bred in captivity in excavated tanks in northern Mato Grosso State, Brazil, in different seasons (rain and dry seasons). Four harvests were performed in two different tanks and five specimens obtained in each evaluated period, with animals aged 18 and 24 months, respectively, at the beginning of the experiment. The animals were slaughtered in a local establishment that had an inspection service following humane standards, and the blankets were later sent to analysis. The samples were analyzed for freshness via total volatile nitrogenous bases and physicochemical characteristics (pH in 24 h, water activity, water retention capacity, dripping loss, cooking loss, and shear force). There was a statistical difference for total nitrogenous volatile bases and shear force with higher values in the rainy season (24 month-of-old animals). Additionally, pH and water activity differed statistically at 24 h in the same period, albeit for 18-month-of-old animals. It was possible to conclude that climate variation affected the freshness and physicochemical characteristics of the pirarucu blankets while age did not.

scholarly journals Physicochemical characteristics of Croatian royal jelly

2019 ◽  
Vol 11 (2) ◽  
pp. 266-271
Author(s):  
Ivana Flanjak ◽  
Ljiljana Priomorac ◽  
Blanka Bilić Rajs ◽  
Zlatko Puškadija ◽  
Marin Kovačić ◽  
...  
Keyword(s):  
Protein Content ◽  
Nutritive Value ◽  
Royal Jelly ◽  
Ph Value ◽  
National Level ◽  
Physicochemical Characteristics ◽  
Total Acidity ◽  
Native Form ◽  
Glucose Content ◽  
International Standard

Due to its high nutritive value, royal jelly usage is increasing, both in human nutrition in native form and as bioactive component in other products (dietary supplements, medicines). The database and regulations on royal jelly characteristics are established in several countries, but not in Croatia. Physicochemical characteristics: moisture, protein content, pH value, total acidity, carbohydrate composition and 10-HDA content in 13 Croatian royal jelly samples were determined with the aim of getting insight to quality of royal jelly produced in Croatia. The obtained results showed that regarding 10-HDA content, one of the most important quality parameter, all samples fulfilled the international standard for royal jelly specifications. Moisture of three samples was higher than prescribed (69.5%, 76.3% and 72.0%, respectively) while one sample had slightly lower protein content than minimum 11% prescribed in international standard. Sucrose content in two royal jelly samples was higher than 3%. Statistically significant correlations were obtained between moisture and protein content, 10-HDA and total acidity as well as between fructose and glucose content. The results of this study will contribute to creation the database of Croatian royal jelly physicochemical characteristics and thus help in setting the royal jelly quality criteria at national level

scholarly journals Evaluation of cassava starch as raw material according to the characteristics of the granules

2020 ◽  
Vol 9 (12) ◽  
pp. e8491210879
Author(s):  
Daiana Cardoso de Oliveira ◽  
Helayne Aparecida Maieves ◽  
Cláudia Bernardo ◽  
Ismael Casagrande Bellettini ◽  
Bruna Barreto Remor ◽  
...  
Keyword(s):  
Amylose Content ◽  
Physicochemical Characterization ◽  
Crystallinity Index ◽  
Physicochemical Characteristics ◽  
Cassava Starch ◽  
Raw Material ◽  
Support Tools ◽  
Different Soils

In this study, the physicochemical characteristics of starch extracted from ten different cultivars of cassava roots, from different soils, were investigated. There are significant (p<0.05) variations in the proportion of starch damaged during extraction, even in samples of the same cultivar. Amylose content differs among cultivars and even within the same cultivar harvested in different soils (varying from 20.00 to 24.07%). According to the type of soil the starch samples showed distinct values for the crystallinity index. This indicates the need for the physicochemical characterization of starch samples to be carried out even when they originate from the same cultivar. The results obtained can be used as support tools for improvement of cassava genetics, optimizing the process of selection and maintenance of a genetic bank. The results, coupled with chemometric analyses (PCAs and clusters), allowed to distinguish cultivars according to their physicochemical and functional peculiarities, suggesting their potential to be used by industries and as food.

scholarly journals Natural sparkling guava wine: volatile and physicochemical characterization

2017 ◽  
Vol 47 (9) ◽  
Author(s):  
Silvana Maria Michelin Bertagnolli ◽  
Gabrieli Bernardi ◽  
Jossiê Zamperetti Donadel ◽  
Aline de Oliveira Fogaça ◽  
Roger Wagner ◽  
...  
Keyword(s):  
Volatile Compounds ◽  
Butyl Acetate ◽  
Solid Phase ◽  
Physicochemical Characterization ◽  
Physicochemical Characteristics ◽  
Tropical Fruit ◽  
Fruit Species ◽  
Ethyl Octanoate ◽  
Phenethyl Acetate

ABSTRACT: Although different tropical fruit species have been used in the development of fermented beverages, there are only few references in the literature to the production of natural sparkling wines from fruits other than grapes. In this sense, the objective of the present research was the development and physicochemical and volatile characterization of a natural sparkling guava wine produced by the champenoise method. Volatile compounds were identified by gas chromatography coupled to mass spectrometry using the headspace solid-phase microextraction (HS-SPME) technique on samples. Eighty-nine volatile compounds were detected, of which 51 were identified. Esters were the predominant class of volatile compounds (a total of 26), followed by alcohols (10), terpenes (9), ketones (3), and acids (3). Volatile compounds with possible odoriferous activity were reported in the beverage, including ethyl octanoate, ethyl 5-hexenoate, phenethyl acetate, (E)-β-damascenone, (E)-ethyl cinnamate, 2-methyl butyl acetate, 3-methylbutanol, ethyl 3-(E)-hexenoate, and methyl 5-hexenoate. Natural sparkling guava wine produced showed a complex composition of fruity and floral aromas. Furthermore, the use of the champenoise method, traditionally applied to grapes, enabled the manufacture of a natural sparkling guava wine with physicochemical characteristics equivalent to those of sparkling wines made from grapes.

ISOLATION OF A STEROID-LIKE SUBSTANCE FROM URINE AND CITROUS FRUITS

1958 ◽  
Vol 36 (8) ◽  
pp. 869-881 ◽  
Author(s):  
Wojciech Nowaczynski ◽  
Thomas Sandor ◽  
Erich Koiw ◽  
R. Norman Jones ◽  
Jacques Genest
Keyword(s):  
Physicochemical Characterization ◽  
Oxidative Degradation ◽  
Physicochemical Characteristics ◽  
Fruit Juices ◽  
Free Form ◽  
Elementary Analysis ◽  
Males And Females ◽  
Normal Males ◽  
Partial Chemical

The isolation and the partial chemical and physicochemical characterization of a chloroform-soluble substance obtained from human urine and citrous fruit juices are presented. The urinary compound, designated as compound III, is present mostly as a conjugate hydrolyzed by animal β-glucuronidase whereas it is in free form in fruit juices. It is present in the urine of normal males and females and in a number of pathological conditions. Its urinary excretion is significantly increased as a result of diets rich in potassium (250 meq./day). In various paper chromatographic systems, the compound has a mobility similar to that of aldosterone. Detailed study of its chemical and physicochemical characteristics, including oxidative degradation and infrared and elementary analysis, suggests a steroidal or sesquiterpinoidal structure. However, at the present time, the data obtained do not permit the final elucidation of the chemical formula of compound III.

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