Adhesion improvement of plasma-deposited silica thin films on stainless steel substrate studied by x-ray photoemission spectroscopy and in situ infrared ellipsometry

1998 ◽  
Vol 16 (1) ◽  
pp. 6-12 ◽  
Author(s):  
N. Bertrand ◽  
B. Drévillon ◽  
A. Gheorghiu ◽  
C. Sénémaud ◽  
L. Martinu ◽  
...  
2013 ◽  
Vol 536 ◽  
pp. 63-67 ◽  
Author(s):  
Ivalina Avramova ◽  
Sefik Suzer ◽  
Desislava Guergova ◽  
Dimitar Stoychev ◽  
Plamen Stefanov

2012 ◽  
Vol 490-495 ◽  
pp. 3486-3490
Author(s):  
Qiang Yu ◽  
Zhen Chen ◽  
Zhong Cheng Guo

In order to prepare a new type of anode material, stainless steel was selected as substrate material. The β-PbO2 coating on stainless steel substrate was prepared under the appropriate plating solution, and the PbO2-MnO2 coating was prepared with thermal decomposition. The crystal structure was determined by X-ray diffraction; Surface morphology was test by Scanning Electron Microscopy; the energy spectrum was used to determine element mass-fraction and the ratio of atomic number of the coatings.


2016 ◽  
Vol 23 (1) ◽  
pp. 70-81 ◽  
Author(s):  
Kristian Myhre ◽  
Jonathan Burns ◽  
Harry Meyer ◽  
Nathan Sims ◽  
Rose Boll

2017 ◽  
Vol 69 (2) ◽  
pp. 182-189
Author(s):  
Lubomir Krabac ◽  
Vladimir Pejaković ◽  
Vladislav Drinek ◽  
Nicole Dörr ◽  
Ewald Badisch

Purpose The purpose of this paper is to study the friction and wear behavior of germanium (Ge) thin films deposited by low-pressure chemical vapor deposition method on a chromium (Cr)-nickel (Ni) stainless steel substrate after being exposed to relatively mild sliding conditions (low loads and sliding distances). Design/methodology/approach Wear and friction experiments were conducted with a 100Cr6 steel ball sliding against flat Ge thin-film-coated stainless steel sheets (ball-on-flat microtribometer, no lubricant, normal loads of 50-100 mN, initial Hertzian contact pressures of 385-485 MPa, total sliding distance up to 200 mm and room temperature). Findings Scanning electron microscopy results revealed that prepared Ge thin films consisted of two different morphologies: curved nanowires and cone-shaped nano-/microdroplets. Regarding friction and wear characteristics of the investigated samples, the substrates coated with Ge thin films did not affect the coefficient of friction significantly by load. The wear of the base material (Cr-Ni stainless steel) was not observed under the mentioned experimental conditions (see the “Design/methodology/approach” section); however, with increased sliding distance and/or applied load, a rupture of the Ge film and an exposure of the stainless steel substrate to the 100Cr6 ball can be expected. Furthermore, the observations suggest that the smearing of Ge nano- and microstructures, plastically deformed during tribotesting, over the surface exposed to the sliding contact is the dominant tribological process. Originality/value For the first time, the tribological interaction between Ge thin film and steel surface was investigated under dry sliding conditions using a ball-on-flat microtribometer, and the obtained results provide a useful base for the further research on tribology of Ge-based thin films.


1989 ◽  
Vol 03 (06) ◽  
pp. 465-470 ◽  
Author(s):  
MASAYUKI TSUKIOKA ◽  
TASUKU MASHIO ◽  
MASAJI SHIMAZU ◽  
TAKESHI NAKAMURA

Using rf-sputtering method, modified BNN ( Ba 2 NaNb 5 O 15) thin-films, which are highly aligned, were prepared on a polished surface of a stainless steel plate and on a polished silicon wafer. It was found that preferably aligned thin-films were successfully obtained only when modified Nb-rich BNN target was used. Preferable orientation of these thin-films was confirmed by X-ray diffraction measurement. In order to find the correlation between preferable orientation and separation from plasma center, X-ray measurement was carried out at several points on the thin-film sputtered on a long stainless steel substrate (5×100 mm ). The result indicated that preferable orientation was dominant near the position of plasma center. In order to distinguish whether the strong X-ray peak observed in the preferably aligned BNN thin-film is due to (200) peak of Nb 2 O 5 or (440) peak of BNN, X-ray measurements and the following quantitative analyses; fluorescent X-ray, ICP (Induced Coupled Radio Frequency Plasma) and an Atomic Absorption Method, were carried out for films sputtered from Nb-rich BNN target. The results reveal that the thin-films include considerable quantity of barium and sodium. This suggests that the highly aligned thin-film is composed of modified BNN and not Nb 2 O 5.


2017 ◽  
Vol 246 ◽  
pp. 278-283 ◽  
Author(s):  
Zeheng Yang ◽  
Kun Wang ◽  
Zongming Shao ◽  
Yuan Tian ◽  
Gongde Chen ◽  
...  

1996 ◽  
Vol 290-291 ◽  
pp. 264-270 ◽  
Author(s):  
N. Bertrand ◽  
B. Drévillon ◽  
J.E. Klemberg-Sapieha ◽  
L. Martinu

2014 ◽  
Vol 1604 ◽  
Author(s):  
Ying-Chung Chen ◽  
Wei-Tsai Chang ◽  
Chien-Chuan Cheng ◽  
Chun-Kai Mao ◽  
Kuo-Sheng Kao

ABSTRACTThis paper reports a novel means of integrating a high-performance dual-modal ZnO piezoelectric transducer with a flexible stainless steel substrate (SUS304) to construct dual-modal vibration-power transducers. To fabricate vibration-power transducers, the off-axis RF magnetron sputtering method for the growth of ZnO piezoelectric thin films is adopted. The stainless steel substrate has a higher Young’s modulus than those of the other substrates, and behaves the long-term stability under vibration. The transducer includes a ZnO piezoelectric thin film deposited on the stainless steel substrate combined with Pt/Ti layers at room temperature, which is fabricated by an RF magnetron two-step sputtering system. In this report, the ZnO piezoelectric thin films deposited with the tilting angle of 34° are set by controlling the deposition parameters. Scanning electron microscopy and X-ray diffraction of ZnO piezoelectric thin films reveal a rigid surface structure and a high dual-modal orientation. To investigate the generating characteristics of the dual-modal transducer, two basic experiments of longitudinal and shear modes are carried out. Based on cantilever vibration theory, the cantilever length of 1 cm and a vibration area of 1 cm2 are used to fabricate a transducer with a low resonant-frequency of 65 Hz for the natural vibration. A mass loading at the front-end of the cantilever is critical to increase the amplitude of vibration and the power generated by the piezoelectric transducer. The maximum open circuit voltage of the power transducer is 19.4 V.


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