scholarly journals Study on the Changing Rules of Silty Clay’s Pore Structure under Freeze-Thaw Cycles

2019 ◽  
Vol 2019 ◽  
pp. 1-11 ◽  
Author(s):  
Zongfang Chen ◽  
Huie Chen ◽  
Jinfeng Li ◽  
Hui Li ◽  
Wenliang Ma
Keyword(s):  
Pore Structure ◽  
Fractal Theory ◽  
Freezing Temperature ◽  
Engineering Properties ◽  
Silty Clay ◽  
Freeze Thaw ◽  
Related Data ◽  
Remoulded Soil ◽  
Frost Depth ◽  
Soil Skeleton

For engineering construction in seasonally frozen regions, when the soil below the frost depth without freeze-thaw effect was exposed or reclaimed after excavation, long-term freeze-thaw will change soil skeleton and porous characteristics, thereby leading to the deterioration of soil engineering properties. This study focused on seasonally frozen silty clay from Changchun, China, and conducted different freeze-thaw cyclic tests on remoulded soil samples, during which both freezing temperature and the number of freeze-thaw cycles were varied. The related data of pore structures under different test conditions were acquired through mercury injection porosimetry (MIP) tests, and the effects of the number of freeze-thaw cycles and freezing temperature on the change of the soil’s pore structure were investigated in detail in combination with fractal theory. The variation rules of pores in the soil after freeze-thaw cycles were investigated from a microperspective so as to essentially analyze the mechanism of the deteriorating effect of freeze-thaw on a soil’s engineering properties.

scholarly journals Freeze–Thaw Resistance and Air-Void Analysis of Concrete with Recycled Glass–Pozzolan Using X-ray Micro-Tomography

Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 154
Author(s):  
Marija Krstic ◽  
Julio F. Davalos ◽  
Emanuele Rossi ◽  
Stefan C. Figueiredo ◽  
Oguzhan Copuroglu
Keyword(s):  
Fly Ash ◽  
Pore Structure ◽  
The United States ◽  
Adsorption Method ◽  
X Ray ◽  
Freeze Thaw ◽  
Void System ◽  
Spatial Parameters ◽  
Micro Tomography ◽  
Air Void

Recent studies have shown promising potential for using Glass Pozzolan (GP) as an alternative supplementary cementitious material (SCM) due to the scarcity of fly ash and slag in the United States. However, comprehensive studies on the freeze–thaw (FT) resistance and air void system of mixtures containing GP are lacking. Therefore, this study aimed to evaluate GP’s effect on FT resistance and characterize mixtures with different GP contents, both macro- and microscopically. In this study, six concrete mixes were considered: Three mixes with 20%, 30% and 40% GP as cement replacements and two other comparable mixes with 30% fly ash and 40% slag, as well as a mix with 100% Ordinary Portland cement (OPC) as a reference. Concrete samples were prepared, cured and tested according to the ASTM standards for accelerated FT resistance for 1000 cycles and corresponding dynamic modulus of elasticity (Ed). All the samples showed minimal deterioration and scaling and high F/T resistance with a durability factor of over 90%. The relationships among FT resistance parameters, air-pressured method measurements of fresh concretes and air void analysis parameters of hardened concretes were examined in this study. X-ray micro-tomography (micro-CT scan) was used to evaluate micro-cracks development after 1000 freeze–thaw cycles and to determine spatial parameters of air voids in the concretes. Pore structure properties obtained from mercury intrusion porosimetry (MIP) and N2 adsorption method showed refined pore structure for higher cement replacement with GP, indicating more gel formation (C-S-H) which was verified by thermogravimetric analysis (TGA).

Characterization of Micro-Pore Structure in Novel Cement Matrices

2014 ◽  
Vol 1712 ◽  
Author(s):  
Seyoon Yoon ◽  
Isabel Galan ◽  
Kemal Celik ◽  
Fredrik P. Glasser ◽  
Mohammed S. Imbabi
Keyword(s):  
Portland Cement ◽  
Pore Structure ◽  
Engineering Properties ◽  
Calcium Sulfoaluminate ◽  
Pore Structures ◽  
Porosity And Permeability ◽  
Experimental Protocols ◽  
Novel Processing ◽  
Main Component

ABSTRACTCalcium sulfoaluminate (CSA) cements are being developed using a novel processing method having as its objective lowering specific CO2 emissions by ∼50% relative to a Portland cement benchmark. We need to be able to measure the properties of the products. Porosity and permeability measurements help define the engineering properties but their quantification is influenced by the choice of experimental protocols. In the present study we used ordinary Portland cement (PC) paste as a benchmark and hydrated ye’elimite, which is a main component of CSA cements, to understand its pore structure. We report on the use of synchrotron-sourced radiation for µCT (Computerized Tomography) and 3D image re-construction of the internal micro-pore structure of PC and ye’elimite-gypsum pastes. As a comparison, porosity and permeability measurements were traditionally obtained using Mercury Intrusion Porosimetry (MIP). The Mori-Tanaka method and the polynomial statistical model were used to analyze the effects of different 3-D micro-pore structures on mechanical properties. The results show that e micro-pore structures differ considerably between PC and ye’elimite pastes and their bulk modulus is significantly affected by the shapes of their micro-pore structures.

FRACTAL MODELS FOR GAS–WATER TRANSPORT IN SHALE POROUS MEDIA CONSIDERING WETTING CHARACTERISTICS

Fractals ◽  
2020 ◽  
Vol 28 (07) ◽  
pp. 2050138
Author(s):  
QI ZHANG ◽  
XINYUE WU ◽  
QINGBANG MENG ◽  
YAN WANG ◽  
JIANCHAO CAI
Keyword(s):  
Fractal Dimension ◽  
Pore Structure ◽  
Pore Pressure ◽  
Surface Diffusion ◽  
Water Transport ◽  
Relative Permeability ◽  
Fluid Transport ◽  
Water Saturation ◽  
Fractal Theory ◽  
Gas Slippage

Complicated gas–water transport behaviors in nanoporous shale media are known to be influenced by multiple transport mechanisms and pore structure characteristics. More accurate characterization of the fluid transport in shale reservoirs is essential to macroscale modeling for production prediction. This paper develops the analytical relative permeability models for gas–water two-phase in both organic and inorganic matter (OM and IM) of nanoporous shale using the fractal theory. Heterogeneous pore size distribution (PSD) of the shale media is considered instead of the tortuous capillaries with uniform diameters. The gas–water transport models for OM and IM are established, incorporating gas slippage described by second-order slip condition, water film thickness in IM, surface diffusion in OM, and the total organic carbon. Then, the presented model is validated by experimental results. After that, sensitivity analysis of gas–water transport behaviors based on pore structure properties of the shale sample is conducted, and the influence factors of fluid transport behaviors are discussed. The results show that the gas relative permeability is larger than 1 at the low pore pressure and water saturation. The larger pore pressure causes slight effect of gas slippage and surface diffusion on the gas relative permeability. The larger PSD fractal dimension of IM results in larger gas relative permeability and smaller water relative permeability. Besides, the large tortuosity fractal dimension will decrease the gas flux at the same water saturation, and the surface diffusion decreases with the increase of tortuosity fractal dimension of OM and pore pressure. The proposed models can provide an approach for macroscale modeling of the development of shale gas reservoirs.

FRACTAL PORE STRUCTURE MODEL AND MULTILAYER FRACTAL ADSORPTION IN SHALE

Fractals ◽  
2014 ◽  
Vol 22 (03) ◽  
pp. 1440010 ◽  
Author(s):  
LIEHUI ZHANG ◽  
JIANCHAO LI ◽  
HONGMING TANG ◽  
JINGJING GUO
Keyword(s):  
Fractal Dimension ◽  
Pore Structure ◽  
Saturated Vapor ◽  
Adsorption Property ◽  
Fractal Theory ◽  
Complex Structure ◽  
Structure Model ◽  
Adsorption Model ◽  
Adsorption Volume ◽  
Isothermal Adsorption

The complex structure and surface property of porous media have significant impact on its accumulation and adsorption capacity. Based on the fractal theory, this paper presents a fractal pore structure model for shales. The effect of different pore structures on fractal dimension is discussed, and the influence of fractal dimension and pore size distribution on porosity is also analyzed. It is shown that the fractal dimension D decreases with the increase of structure parameter q/m for a certain pore diameter ratio, and porosity has positive relationship with fractal dimension. This paper also presents a multilayer fractal adsorption model which takes into account the roughness of adsorption surface by using fractal theory. With the introduction of pseudo-saturated vapor pressure in the supercritical temperature condition, the proposed adsorption model can be applied into a wider range of temperature. Based on the low-pressure nitrogen adsorption and methane isothermal adsorption experiments, the effect of fractal dimension on the adsorption behavior of shales is discussed. Fractal dimension has significant impact on the surface adsorption property and adsorption layer number n. The monolayer saturated adsorption volume Vm increases with the increase of D, while parameter C has the opposite variation trend. Finally, the optimal combination of fractal parameters for describing pore structure of shale samples is selected.

scholarly journals Degradation of Mechanical Behavior of Sandstone under Freeze-Thaw Conditions with Different Low Temperatures

2021 ◽  
Vol 11 (22) ◽  
pp. 10653
Author(s):  
Jingwei Gao ◽  
Chao Xu ◽  
Yan Xi ◽  
Lifeng Fan
Keyword(s):  
Compressive Strength ◽  
Elastic Modulus ◽  
Mechanical Behavior ◽  
Energy Absorption ◽  
Uniaxial Compressive Strength ◽  
Dynamic Strength ◽  
Freezing Temperature ◽  
P Wave ◽  
Freeze Thaw ◽  
P Wave Velocity

This study investigated the effects of freezing temperature under freeze-thaw cycling conditions on the mechanical behavior of sandstone. First, the sandstone specimens were subjected to 10-time freeze-thaw cycling treatments at different freezing temperatures (−20, −40, −50, and −60 °C). Subsequently, a series of density, ultrasonic wave, and static and dynamic mechanical behavior tests were carried out. Finally, the effects of freezing temperature on the density, P-wave velocity, stress–strain curves, static and dynamic uniaxial compressive strength, static elastic modulus, and dynamic energy absorption of sandstone were discussed. The results show that the density slightly decreases as temperature decreases, approximately by 1.0% at −60 °C compared with that at 20 °C. The P-wave velocity, static and dynamic uniaxial compressive strength, static elastic modulus, and dynamic energy absorption obviously decrease. As freezing temperature decreases from 20 to −60 °C, the static uniaxial compressive strength, static elastic modulus, dynamic strength, and dynamic energy absorption of sandstone decrease by 16.8%, 21.2%, 30.8%, and 30.7%, respectively. The dynamic mechanical behavior is more sensitive to the freezing temperature during freeze-thawing cycling compared with the static mechanical behavior. In addition, a higher strain rate can induce a higher dynamic strength and energy absorption.

scholarly journals Effect of Grain Size on Microscopic Pore Structure and Fractal Characteristics of Carbonate-Based Sand and Silicate-Based Sand

2021 ◽  
Vol 5 (4) ◽  
pp. 152
Author(s):  
Shao-Heng He ◽  
Zhi Ding ◽  
Hai-Bo Hu ◽  
Min Gao
Keyword(s):  
Grain Size ◽  
Fractal Dimension ◽  
Pore Structure ◽  
Pore Size ◽  
Quartz Sand ◽  
Glass Bead ◽  
Fractal Theory ◽  
Calcareous Sand ◽  
Wide Range ◽  
Fractal Characteristics

In this study, a series of nuclear magnetic resonance (NMR) tests was conducted on calcareous sand, quartz sand, and glass bead with a wide range of grain sizes, to understand the effect of grain size on the micro-pore structure and fractal characteristics of the carbonate-based sand and silicate-based sand. The pore size distribution (PSD) of the tested materials were obtained from the NMR T2 spectra, and fractal theory was introduced to describe the fractal properties of PSD. Results demonstrate that grain size has a significant effect on the PSD of carbonate-based sand and silicate-based sand. As grain size increases, the PSD of sands evolves from a binary structure with two peaks to a ternary structure with three peaks. The increase in the grain size can cause a remarkable increase in the maximum pore size. It is also found that the more irregular the particle shape, the better the continuity between the large and medium pores. In addition, grain size has a considerable effect on the fractal dimension of the micro-pore structure. The increase of grain size can lead to a significant increase in the heterogeneity and fractal dimension in PSD for calcareous sand, quartz sand and glass bead.

Waste Tile Usage Effect on the Sandy Subgrade Stabilized with Emulsion Bitumen Performance

2021 ◽  
Vol 47 (1) ◽  
pp. 164-173
Author(s):  
Mohammad Mehdi Khabiri ◽  
Bahareh Ebrahimialavijeh
Keyword(s):  
Bearing Capacity ◽  
Compression Strength ◽  
Engineering Properties ◽  
Coarse Grained ◽  
Freeze Thaw ◽  
Thaw Cycle ◽  
Freeze Thaw Cycle ◽  
Number Of Cycles ◽  
Surface Analysis Method ◽  
Drop Rate

Improving the subgrade performance and increasing their efficiency can lead to improving the operation and increasing the life of the pavement. One of the common solutions to improve the resistance and engineering properties of the soils is using the stabilizing materials. Using the waste materials as a stabilizer in the soil can lead to a reduction in project costs and help the protection from the environment. In this study, emulsion bitumen and crushed waste tile are used to stabilize the sand dune which is soil with low bearing capacity and resistance properties. In the present study, the emulsion bitumen and crushed waste tile have been used. The effect of dimensions and percentage of crushed tile with different percentages of emulsion bitumen on the compressive pressure and bearing capacity as well as the compressive strength after applying freeze-thaw cycle. The results indicate that the addition of crushed waste tile increases the compression strength and bearing capacity and the tile with a higher dimension has shown more effectiveness. Applying the freeze-thaw cycle has reduced the compression strength and increasing the number of cycles has increased the resistance drop rate. Soil stabilized with coarse-grained tile has more resistance drop rate which increases by increasing the tile percentage. Then, the 3D graph and the recommended function related to each parameter investigated in the test were provided using the response surface analysis method.

STUDY ON EVOLUTION OF FRACTAL DIMENSION FOR FRACTURED COAL SEAM UNDER MULTI-FIELD COUPLING

Fractals ◽  
2020 ◽  
Vol 28 (04) ◽  
pp. 2050072 ◽  
Author(s):  
GUANNAN LIU ◽  
BOMING YU ◽  
DAYU YE ◽  
FENG GAO ◽  
JISHAN LIU
Keyword(s):  
Fractal Dimension ◽  
Coal Seam ◽  
Pore Structure ◽  
Fractal Theory ◽  
In Situ Stress ◽  
Volume Strain ◽  
Fracture Length ◽  
Field Coupling ◽  
Pore Evolution ◽  
Fractured Coal

In the process of gas extraction, fracture-pore structure significantly influences the macroscopic permeability of coal seam. However, under the multi-field coupling, the mechanism of coal seam fracture-pore evolution remains to be clarified. In this paper, considering the effect of adsorption expansion, the fractal theory for porous media coupled with the multi-field model for coal seam is considered, and a multi-field coupling mechanical model is constructed by considering the influence of fracture-pore structure. Furthermore, the evolution mechanism of fractal dimension with physical and mechanical parameters of coal seam is studied. It is found that the fractal dimension for coal seam is inversely proportional to mining time and in situ stress, proportional to elastic modulus, Langmuir volume constant and Langmuir volume strain constant, and inversely proportional to Langmuir pressure constant. Compared with other factors, Langmuir pressure constant and Langmuir volume strain constant have the significance influence on the fractal dimension for the fracture length.

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