scholarly journals Effect of Microarc Oxidation Treatment with Different Concentrations of MgSiF6 on Titanium-Porcelain Bonding Strength

2020 ◽  
Vol 2020 ◽  
pp. 1-7
Author(s):  
Jing Lv ◽  
Mujie Yuan ◽  
Pei Sun ◽  
Changlei Wei ◽  
Shaojun Zhang ◽  
...  
Keyword(s):  
Bonding Strength ◽  
Oxygen Diffusion ◽  
Electrolyte Concentration ◽  
Microarc Oxidation ◽  
Negative Influence ◽  
Bending Test ◽  
Control Group ◽  
Oxidation Treatment ◽  
Three Point Bending ◽  
Scanning Electron

This study aims to evaluate the effects of different electrolyte concentrations on titanium-porcelain bonding strength after microarc oxidation (MAO) treatment. Four MgSiF6 electrolyte concentrations (10 g/L, 20 g/L, 30 g/L, and 40 g/L) were chosen for the MAO bath solutions. According to ISO 9693, the bonding strengths of titanium-porcelain restorations were detected by the three-point bending test. Scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDS) were applied to evaluate the morphologies and elemental compositions of the MAO coating, titanium-porcelain fracture surfaces, titanium-porcelain interfaces, and oxygen diffusion. The bonding strength of the 20 g/L MgSiF6 group was significantly higher than that of the control group. However, overly high MgSiF6 concentrations had a negative influence on the bonding strength between titanium and porcelain. The results demonstrate that MAO treatment with only appropriate electrolyte concentration can improve the titanium-porcelain bonding strength.

scholarly journals Evaluation of low-fusing ceramic systems combined with titanium grades II and V by bending test and scanning electron microscopy

2003 ◽  
Vol 11 (4) ◽  
pp. 354-360 ◽  
Author(s):  
Wilson José Garbelini ◽  
Guilherme Elias Pessanha Henriques ◽  
Manoel Troia Junior ◽  
Marcelo Ferraz Mesquita ◽  
Cássia Cilene Dezan
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Bond Strength ◽  
Bending Strength ◽  
Bending Test ◽  
Control Group ◽  
Three Point Bending ◽  
Grade Ii ◽  
Titanium Grade ◽  
Scanning Electron

The bond strength by three point bending strength of two metal substrates (commercially pure titanium or grade II, and Ti-6Al-4V alloy or grade V) combined to three distinct low-fusing ceramic systems (LFC) and the nature of porcelain-metal fracture by scanning electron microscopy (SEM) were evaluated. The results were compared to a combination of palladium-silver (Pd-Ag) alloy and conventional porcelain (Duceram VMK68). Sixty metal strips measuring 25x3x0.5mm were made - 30 of titanium grade II and 30 of titanium grade V, with application of the following types of porcelain: Vita Titankeramik, Triceram or Duceratin (10 specimens for each porcelain). The porcelains were bonded to the strips with dimensions limited to 8x3x1mm. The control group consisted of ten specimens Pd-Ag alloy/Duceram VMK68 porcelain. Statistical analyses were made by one-way analysis of variance (ANOVA) and Tukey test at 5% significance level. Results showed that the bond strength in control group (48.0MPa ± 4.0) was significantly higher than the Ti grade II (26.7MPa ± 4.1) and Ti grade V (25.2MPa ± 2.2) combinations. When Duceratin porcelain was applied in both substrates, Ti grade II and Ti grade V, the results were significantly lower than in Ti grade II/Vitatitankeramik. SEM analysis indicated a predominance of adhesive fractures for the groups Ti grade II and Ti grade V, and cohesive fracture for control group Pd-Ag/Duceram. Control group showed the best bond strength compared to the groups that employed LFC. Among LFC, the worst results were obtained when Duceratin porcelain was used in both substrates. SEM confirmed the results of three point bending strength.

DPP IV inhibitor treatment attenuates bone loss and improves mechanical bone strength in male diabetic rats

2014 ◽  
Vol 307 (5) ◽  
pp. E447-E455 ◽  
Author(s):  
Lorenzo Glorie ◽  
Geert J. Behets ◽  
Lesley Baerts ◽  
Ingrid De Meester ◽  
Patrick C. D'Haese ◽  
...  
Keyword(s):  
Bone Loss ◽  
Bone Strength ◽  
Serum Levels ◽  
Diabetic Rats ◽  
Bending Test ◽  
Control Group ◽  
Mechanical Resistance ◽  
Three Point Bending ◽  
Dpp Iv

Dipeptidyl peptidase IV (DPP IV) modulates protein activity by removing dipeptides. DPP IV inhibitors are currently used to improve glucose tolerance in type 2 diabetes patients. DPP IV substrates not only increase insulin secretion but also affect bone metabolism. In this study, the effect of DPP IV inhibitor sitagliptin on bone was evaluated in normal and streptozotocin-induced diabetic rats. This study included 64 male Wistar rats divided into four groups ( n = 16): two diabetic and two control groups. One diabetic and one control group received sitagliptin through drinking water. Tibiae were scanned every 3 wk using an in vivo μCT scanner. After 6 and 12 wk, rats were euthanized for histomorphometric analysis of bone parameters. The mechanical resistance of femora to fracture was assessed using a three-point bending test, and serum levels of bone metabolic markers were measured. Efficient DPP IV inhibition was achieved in sitagliptin-treated groups. Trabecular bone loss, the decrease in trabecular number, and the increase in trabecular spacing was attenuated through sitagliptin treatment in diabetic rats, as shown by in vivo μCT. Bone histomorphometry was in line with these results. μCT analysis furthermore showed that sitagliptin prevented cortical bone growth stagnation in diabetic rats, resulting in stronger femora during three-point bending. Finally, the serum levels of the resorption marker CTX-I were significantly lower in sitagliptin-treated diabetic animals compared with untreated diabetic animals. In conclusion, sitagliptin treatment attenuates bone loss and increases bone strength in diabetic rats probably through the reduction of bone resorption and independent of glycemic management.

scholarly journals Influence of Different Reline Materials and Processing Methods on Flexural Strength of Denture Base Material

2021 ◽  
Vol 25 (2) ◽  
pp. 108-113
Author(s):  
Ozlem Gurbuz Oflezer ◽  
Hakan Bahadır ◽  
Senem Ünver ◽  
Ceyhan Oflezer
Keyword(s):  
Flexural Strength ◽  
Base Material ◽  
Acrylic Resin ◽  
Bending Test ◽  
Control Group ◽  
Processing Methods ◽  
Denture Base ◽  
Three Point Bending ◽  
Heat Cure ◽  
And Control

Summary Background/Aim: Relining is defined as the procedure used to resurface the tissue side of a denture with new base material, thus producing an accurate adaptation is provided at the denture foundation area. During mastication, relined dentures have to withstand masticatory forces to prevent fracture. The aim of this study was to evaluate the flexural strength of acrylic resin denture base relined with different methods and materials. Material and Methods: Fourteen experimental groups and one control group were determined to consider different reline materials and processing methods. Acrylic resin specimens were prepared with the dimensions of 65× 10× 1.5 mm and reline materials (1.5 mm thickness) were placed on acrylic resins. Reline material was not used in control group specimens. Flexural strength values of relined and control specimens were measured with three-point bending test at a speed of 5 mm/min. Data were analyzed with using one way Anova and Student t tests. Results: The highest flexural strength values were shown in control group (86.51±1.08 MPa). There were significant differences among relined specimens (p< 0.05). For the relined specimens, the highest flexural strength values were found in the relined specimens with denture base material (77.90±1.93 MPa), and the lowest values were found in relined with autopolymerize acrylic material (59.81±1.50 MPa). Conclusions: Relining of the heat cure denture base material significantly decreases the flexural strength for all processing methods and materials.

scholarly journals Comparative analysis of ceramic flexural strength in co-cr and ni-cr alloys joined by TIG welding and conventional brazing

2017 ◽  
Vol 16 ◽  
pp. 1-9
Author(s):  
Adaias Oliveira Matos ◽  
Cristiane de Castro Castelo Branco ◽  
Eliza Burlamaqui Klautau ◽  
Bruno Pereira Alves
Keyword(s):  
Flexural Strength ◽  
Tig Welding ◽  
Bending Test ◽  
Control Group ◽  
Cobalt Chromium ◽  
Bond Failure ◽  
Three Point Bending ◽  
Nickel Chromium ◽  
Ceramic Bond ◽  
Bond Strengths

The purpose of the present study was to evaluate the flexural strength of specimens made of nickel-chromium (Ni-Cr) and cobalt-chromium (Co-Cr) alloys and joined by tungsten inert gas (TIG) welding and conventional brazing. Ni–Cr and Co–Cr base metal specimens (n = 40, each) were cast and welded by TIG or brazing. The specimens were divided into six groups (2 base metals, four welded specimens). Ceramic systems were applied to the central part of all the specimens. A three-point bending test with a velocity of 0.5 mm/m was performed on the specimens up to the point of the first ceramic bond failure by measuring the flexural strength. Data were analyzed using two-way ANOVA and Bonferroni’s tests. Conventional welding showed the lowest flexural strength results for both alloys, while the TIG weld and the control group presented with varying bond strengths for the alloys studied. We concluded that TIG welding was superior to the conventional welding method for both Ni–Cr and Co–Cr alloys with regard to the flexural strength of the ceramic.

The Mechanical Strength of Rabbit Femurs Fixed with Calcium Phosphate Cement after Fracture

2011 ◽  
Vol 343-344 ◽  
pp. 1160-1162
Author(s):  
Jing Chen ◽  
Xiao Na Li ◽  
Shi En Tan ◽  
Wei Yi Chen
Keyword(s):  
Calcium Phosphate ◽  
Calcium Phosphate Cement ◽  
Bending Test ◽  
Control Group ◽  
Material Strength ◽  
Maximum Pressure ◽  
Tension Stress ◽  
Bone Material ◽  
Three Point Bending ◽  
Bone Material Strength

In this study, we invesgated the mechanical properties of the rabbit femurs fixed with calcium phosphate cement (CPC). Twenty adult rabbits were randomly divided into the control group and the group treated with femur fracture artifically, then fixed with CPC. Two weeks after surgery, all rabbits were sacrificed, and femurs were removed for the three point bending test to examine the changes of mechanical parameters of the femurs. Our results showed that although the maximum tension stress of the femurs in the treatment group was smaller than the control, its crosss-sectional area became bigger, which improved the ablity of the femur to bear more loading with the maximum pressure and absorbed energy during destroy up to 83.5% and 64.3% of normal bone material strength. It indicated that it was practicable to fix the fractured femur with CPC from the biomechanical view piont.

scholarly journals Flexural Strength and Hardness of Filler-Reinforced PMMA Targeted for Denture Base Application

Materials ◽  
2021 ◽  
Vol 14 (10) ◽  
pp. 2659
Author(s):  
Abdulaziz Alhotan ◽  
Julian Yates ◽  
Saleh Zidan ◽  
Julfikar Haider ◽  
Nikolaos Silikas
Keyword(s):  
Flexural Strength ◽  
Glass Fibre ◽  
Surface Hardness ◽  
Bending Test ◽  
Zro2 Nanoparticles ◽  
Filler Concentration ◽  
Control Group ◽  
Denture Base ◽  
Three Point Bending ◽  
Pmma Resin

The aim of this work was to evaluate the flexural strength and surface hardness of heat-cured Polymethyl methacrylate (PMMA) modified by the addition of ZrO2 nanoparticles, TiO2 nanoparticles, and E-glass fibre at different wt.% concentrations. Specimens were fabricated and separated into four groups (n = 10) to measure both flexural strength and surface hardness. Group C was the control group. The specimens in the remaining three groups differed according to the ratio of filler to weight of PMMA resin (1.5%, 3%, 5%, and 7%). A three-point bending test was performed to determine the flexural strength, while the surface hardness was measured using the Vickers hardness. Scanning Electron Microscope (SEM) was employed to observe the fractured surface of the specimens. The flexural strength was significantly improved in the groups filled with 3 wt.% ZrO2 and 5 and 7 wt.% E-glass fibre in comparison to Group C. All the groups displayed a significantly higher surface hardness than Group C, with the exception of the 1.5% TiO2 and 1.5% ZrO2 groups. The optimal filler concentrations to enhance the flexural strength of PMMA resin were between 3–5% ZrO2, 1.5% TiO2, and 3–7% E-glass fibre. Furthermore, for all composites, a filler concentration of 3 wt.% and above would significantly improve hardness.

scholarly journals PENGARUH POSISI SERAT KACA (FIBERGLASS) YANG BERBEDA TERHADAP KEKUATAN FLEKSURAL FIBER REINFORCED ACRYLIC RESIN

2016 ◽  
Vol 3 (2) ◽  
pp. 128
Author(s):  
Aprilia Dian Fatimina ◽  
Benni Benyamin ◽  
Helmi Fathurrahman
Keyword(s):  
Acrylic Resin ◽  
Bending Test ◽  
Control Group ◽  
Fiber Reinforced ◽  
Three Point Bending ◽  
Significant Difference ◽  
Bottom Side ◽  
Group 3 ◽  
Post Hoc

Background: One of factor that increases the flexural strenght of fiberreinforced acrylic resin is a fiberglass position . Fiberglass is one of type that can be used in dentistry. The aim of this was to determine the influence of position of fiberglass to the flexural strenght of fiber reinforced acrylic resin.Method: This study was in vitro laboratory experimental. Samples was 16plate spesimens (65x10x2.5mm). The study group was divided into 4 group : 3 groups of fiber reinforced acrylic resin were given fiberglass at the upper, middle, and bottom side and 1 control group of resin acrylic without fiberglass. All of groups would be in the flexural strenght test with a three-point bending test using a universal testing machine.Result: Based on One Way ANOVA test showed that there were significantvalue 0.000 (p<0.05), it concluded that there were significant influencebetween all the groups. Based on the LSD Post Hoc test showed that therewere significant value between all of groups with fiberglass reinforced andcontrol group without fiberglass reinforced. Comparisson between the group that given fiberglass in a upper and middle side with the group that given in bottom side showed value of significant difference (p < 0.05).Conclusion: The result of study was concluded that there was an influenceon the position of fiberglass to flexural strenght of fiber reinforced acrylic resin

scholarly journals Degradation of a Micro-Hybrid Dental Composite Reinforced with Polyaramide Fiber under the Influence of Cyclic Loads

2020 ◽  
Vol 10 (20) ◽  
pp. 7296
Author(s):  
Leszek Szalewski ◽  
Aneta Kamińska ◽  
Eliza Wallner ◽  
Justyna Batkowska ◽  
Tomasz Warda ◽  
...  
Keyword(s):  
Glass Fibers ◽  
Tensile Modulus ◽  
Cyclic Fatigue ◽  
Dental Composite ◽  
Bending Test ◽  
Fatigue Properties ◽  
Control Group ◽  
Three Point Bending ◽  
Number Of Cycles ◽  
Composite Samples

Dental composites reinforced with glass fibers have a low tensile modulus and relatively low fatigue resistance. The aim of the study was to analyze the fatigue properties of a dental composite reinforced with polyaramide fibers under the influence of a cyclic, vertical load. For this purpose, we designed a thermoformable template, corresponding to the construction of adhesive bridges in the side section of the jaw. Fifty-four composite samples were made for the study. They were divided into three groups—control (K) and two experimental groups (R1 and R2). The experimental samples were subjected to cyclic fatigue using 75 N load. The number of cycles was 4690 and 20,100. The study used a three-point bending test. Statistical analysis showed a change in elasticity in groups related to the number of load cycles. The study showed that the samples from the control group required the greatest force to break in relation to those subjected to the work cycles. The maximum force in control (K) group was 738.1 N, R1—487.8 N, and R2—451.4 N. The determined algorithm showed a change in deflection associated with the increase of force value. The study did not show any relationship between the type of sample fracture and the number of load cycles.

scholarly journals Evaluation Flexural Strength of PMMA Resins with the Addition of Nanoparticles

2021 ◽  
Author(s):  
Canan Akay ◽  
Duygu Karakis
Keyword(s):  
Flexural Strength ◽  
Acrylic Resin ◽  
Bending Test ◽  
Zro2 Nanoparticles ◽  
Control Group ◽  
Test Machine ◽  
Three Point Bending ◽  
Acrylic Resins ◽  
Heat Cure ◽  
Topographic Characteristics

Abstract The flexural strength of heat cure acrylic resin was investigated by adding different concentrations of TiO2 and ZrO2 nanoparticles to increase its mechanical properties. ZrO2 and TiO2 nanoparticles were added at 1, 3, and 5% concentrations to the powder portion of heat polymerized acrylic resins. A total of 49 samples were prepared in 65 × 10 × 3 mm size. The structural characterisations of all experimental groups were determined by Fourier transform infrared spectroscopy. Flexural strength of the resin specimens was evaluated with a three-point bending test in a universal test machine and then examined under by scanning electron microscope to assess its topographic characteristics. The highest flexural strength value was obtained for 3% TiO2, while the lowest values were obtained for 1% and 5% TiO2. 1% ZrO2 and 3% TiO2 groups showed statistically higher flexural strength values than the control group. Addition of 3% and 5% ZrO2 and 1% and 5% TiO2 showed statistically lower flexural strength than the control group.

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