Anatomical changes to the wood of Croton sonderianus (Euphorbiaceae) when charred at different temperatures

IAWA Journal ◽  
2017 ◽  
Vol 38 (1) ◽  
pp. 117-123 ◽  
Author(s):  
Peter Gasson ◽  
Caroline Cartwright ◽  
Claudia Luizon Dias Leme
Keyword(s):  
Moisture Content ◽  
Ambient Temperature ◽  
Cell Walls ◽  
Structural Changes ◽  
Middle Lamella ◽  
Treatment Temperature ◽  
Anatomical Characteristics ◽  
Anatomical Changes ◽  
Different Temperatures ◽  
Two Temperatures

Wood retains most of its anatomical characteristics when charred, but charring temperature determines the appearance of the resulting charcoal and this depends largely on the proportions and distribution of the constituent vessels, fibres and parenchyma, as well as moisture content. This study describes the structural changes in the charcoal of the wood of Croton sonderianus Muell. Arg. at two temperatures, 400 °C or 600 °C. This species is an important source of charcoal in the caatinga of the northeast part of Brazil. The samples were heated for ten minutes to reach treatment temperature, charred for two hours at either 400 °C or 600 °C and then left to cool to ambient temperature for 30 to 60 minutes. Our observations showed that most of the changes occurred when charcoal was produced at 600 °C, but the qualitative features necessary for identification were retained. At this temperature, cells lost their circular shape, became angular and occasionally amorphous, the middle lamella disappeared and the walls of adjacent cells coalesced, cell walls became thinner, and the prismatic crystals developed cracks and became porous. Our findings are compared with those for two previously studied Mimosa species which have an entirely different anatomy.

Anatomical Changes to the wood of Mimosa Ophthalmocentra and Mimosa Tenuiflora when charred at different temperatures

IAWA Journal ◽  
2010 ◽  
Vol 31 (3) ◽  
pp. 333-351 ◽  
Author(s):  
Claudia Luizon Dias Leme ◽  
Caroline Cartwright ◽  
Peter Gasson
Keyword(s):  
Moisture Content ◽  
Wood Density ◽  
Anatomical Structure ◽  
Northeast Brazil ◽  
Axial Parenchyma ◽  
Anatomical Changes ◽  
Different Temperatures ◽  
Qualitative Changes ◽  
Mimosa Tenuiflora

Wood retains most of its qualitative features when charred, but the dimensions and appearance of the cells change in various ways. Wood density, anatomical structure, moisture content, duration and temperature all influence wood behaviour when charred. This paper explores the qualitative changes that take place in the wood of Mimosa ophthalmocentra and M. tenuiflora when charred artificially at temperatures of 400, 600 and 800 °C and compares them with charcoal produced in a traditional temporary kiln in northeast Brazil. Our findings can be applied to interpreting the conditions in which charcoal has been produced, and document what happens qualitatively to the vessels, fibres, axial parenchyma and rays in very dense Mimosa wood (>1.00). The observations are specific to these two species.

scholarly journals The impact of natural and artificial weathering on the anatomy of selected tropical hardwoods

IAWA Journal ◽  
2020 ◽  
Vol 41 (3) ◽  
pp. 333-355 ◽  
Author(s):  
Miroslava Mamoňová ◽  
Ladislav Reinprecht
Keyword(s):  
Cell Walls ◽  
Parenchyma Cell ◽  
Middle Lamella ◽  
Artificial Weathering ◽  
Hymenaea Courbaril ◽  
Anatomical Changes ◽  
Micro Cracks ◽  
Parenchyma Cells ◽  
Dipteryx Odorata ◽  
The Impact

Abstract The effect of natural and artificial weathering on the anatomy of seven tropical hardwoods: Bangkirai (Shorea obtusa Wall.), Cumaru (Dipteryx odorata (Aubl.) Wild.), Cumaru Rosa (Dipteryx magnifica (Ducke) Ducke), Ipé (Tabebuia serratifolia Nichols.), Jatobá (Hymenaea courbaril L.), Kusia (Nauclea diderrichii Merill) and Massaranduba (Manilkara bidentata A. Chev.), was studied. As a result of weathering some characteristic anatomical changes occurred: the weakening of connections between cell elements related to the degradation of the middle lamella; micro-cracks in cell walls; total degradation of parenchyma cells in xylem rays, or significant thinning of parenchyma cell walls and their extreme shrinkage; micro-cracks in the vicinity of xylem rays; significant transversal disruptions in libriform fibres; ablation of pit membranes in vessels and parenchyma cells; changes in the secondary wall of libriform fibres, for example, their defibrillation and weathering-degradation of the S1 layer; and spherical formations on the S3 layer of cell walls produced from condensing compounds of degraded lignin and hemicelluloses as well as thermo-mechanical wrinkling. The highest incidence of micro-cracks after both modes of weathering was found in the densest species; Cumaru, Ipé, and Massaranduba.

Silicification of wood-cell walls

1994 ◽  
Vol 52 ◽  
pp. 428-429
Author(s):  
S. E. Keckler ◽  
D. M. Dabbs ◽  
N. Yao ◽  
I. A. Aksay
Keyword(s):  
Electron Microscopy ◽  
Cell Wall ◽  
Cell Walls ◽  
Lignin Content ◽  
Resin Composite ◽  
Middle Lamella ◽  
Cellulose Fibers ◽  
Complex Structures ◽  
Rich Region ◽  
Inorganic Precursors

Cellular organic structures such as wood can be used as scaffolds for the synthesis of complex structures of organic/ceramic nanocomposites. The wood cell is a fiber-reinforced resin composite of cellulose fibers in a lignin matrix. A single cell wall, containing several layers of different fiber orientations and lignin content, is separated from its neighboring wall by the middle lamella, a lignin-rich region. In order to achieve total mineralization, deposition on and in the cell wall must be achieved. Geological fossilization of wood occurs as permineralization (filling the void spaces with mineral) and petrifaction (mineralizing the cell wall as the organic component decays) through infiltration of wood with inorganics after growth. Conversely, living plants can incorporate inorganics into their cells and in some cases into the cell walls during growth. In a recent study, we mimicked geological fossilization by infiltrating inorganic precursors into wood cells in order to enhance the properties of wood. In the current work, we use electron microscopy to examine the structure of silica formed in the cell walls after infiltration of tetraethoxysilane (TEOS).

CATFISH DRYING (Clarias Batraclus) USING ‘TEKO BERSAYAP’ SOLAR DRYER

2012 ◽  
Vol 2 (1) ◽  
pp. 14-20
Author(s):  
Yuwana Yuwana
Keyword(s):  
Relative Humidity ◽  
Moisture Content ◽  
Ambient Temperature ◽  
Drying Rate ◽  
Drying Process ◽  
Drying Time ◽  
Ambient Relative Humidity ◽  
Solar Dryer

Experiment on catfish drying employing ‘Teko Bersayap’ solar dryer was conducted. The result of the experiment indicated that the dryer was able to increase ambient temperature up to 44% and decrease ambient relative humidity up to 103%. Fish drying process followed equations : KAu = 74,94 e-0,03t for unsplitted fish and KAb = 79,25 e-0,09t for splitted fish, where KAu = moisture content of unsplitted fish (%), KAb = moisture content of splitted fish (%), t = drying time. Drying of unsplitted fish finished in 43.995 hours while drying of split fish completed in 15.29 hours. Splitting the fish increased 2,877 times drying rate.

Heat Treatment Influence on the Corrosion Resistance of a Cu-Al-Fe-Mn Bronze

2018 ◽  
Vol 69 (5) ◽  
pp. 1055-1059 ◽  
Author(s):  
Mariana Ciurdas ◽  
Ioana Arina Gherghescu ◽  
Sorin Ciuca ◽  
Alina Daniela Necsulescu ◽  
Cosmin Cotrut ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Corrosion Resistance ◽  
Structural Changes ◽  
Heating Temperature ◽  
Galvanic Corrosion ◽  
Cooling Water ◽  
Open Circuit ◽  
Water Quenching ◽  
Heat Treated ◽  
Different Temperatures

Aluminium bronzes are exhibiting good corrosion resistance in saline environments combined with high mechanical properties. Their corrosion resistance is obviously confered by the alloy chemical composition, but it can also be improved by heat treatment structural changes. In the present paper, five Cu-Al-Fe-Mn bronze samples were subjected to annealing heat treatments with furnace cooling, water quenching and water quenching followed by tempering at three different temperatures: 200, 400 and 550�C. The heating temperature on annealing and quenching was 900�C. The structure of the heat treated samples was studied by optical and scanning electron microscopy. Subsequently, the five samples were submitted to corrosion tests. The best resistance to galvanic corrosion was showed by the quenched sample, but it can be said that all samples are characterized by close values of open-circuit potentials and corrosion potentials. Concerning the susceptibility to other types of corrosion (selective leaching, pitting, crevice corrosion), the best corrosion resistant structure consists of a solid solution, g2 and k compounds, corresponding to the quenched and 550�C tempered sample.

scholarly journals Temperature effect in physicochemical and bioactive behavior of biogenic hydroxyapatite obtained from porcine bones

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
P. A. Forero-Sossa ◽  
J. D. Salazar-Martínez ◽  
A. L. Giraldo-Betancur ◽  
B. Segura-Giraldo ◽  
E. Restrepo-Parra
Keyword(s):  
Structural Changes ◽  
Biological Fluid ◽  
Treatment Temperature ◽  
Mineral Phase ◽  
Calcination Temperatures ◽  
Bioactive Properties ◽  
Temperature Ranges ◽  
Compositional Changes ◽  
Type Substitution ◽  
Biogenic Hydroxyapatite

AbstractBiogenic hydroxyapatite (BHAp) is a widely used material in the biomedical area due to its similarities with the bone tissue mineral phase. Several works have been spotlighted on the thermal behavior of bone. However, little research has focused on determining the influence of calcination temperature in the physicochemical and bioactive properties of BHAp. In this work, a study of the physicochemical properties’ changes and bioactive response of BHAp produced from porcine femur bones using calcination temperatures between 900 to 1200 °C was conducted. The samples’ structural, morphological, and compositional changes were determined using XRD, SEM, and FTIR techniques. XRD results identified three temperature ranges, in which there are structural changes in BHAp samples and the presence of additional phases. Moreover, FTIR results corroborated that B-type substitution is promoted by increasing the heat treatment temperature. Likewise, samples were immersed in a simulated biological fluid (SBF), following the methodology described by Kokubo and using ISO 23317:2014 standard, for 3 and 7 days. FTIR and SEM results determined that the highest reaction velocity was reached for samples above 1000 °C, due to intensity increasing of phosphate and carbonate bands and bone-like apatite morphologies, compared to other temperatures evaluated.

scholarly journals Cherry Tomato Drying: Sun versus Convective Oven

Horticulturae ◽  
2021 ◽  
Vol 7 (3) ◽  
pp. 40
Author(s):  
Vincenzo Alfeo ◽  
Diego Planeta ◽  
Salvatore Velotto ◽  
Rosa Palmeri ◽  
Aldo Todaro
Keyword(s):  
Moisture Content ◽  
Initial Moisture Content ◽  
Drying Process ◽  
Drying Time ◽  
Oven Drying ◽  
Sun Drying ◽  
Different Temperatures ◽  
Final Water Content ◽  
Drying Curves ◽  
Drying Conditions

Solar drying and convective oven drying of cherry tomatoes (Solanum lycopersicum) were compared. The changes in the chemical parameters of tomatoes and principal drying parameters were recorded during the drying process. Drying curves were fitted to several mathematical models, and the effects of air temperature during drying were evaluated by multiple regression analyses, comparing to previously reported models. Models for drying conditions indicated a final water content of 30% (semidry products) and 15% (dry products) was achieved, comparing sun-drying and convective oven drying at three different temperatures. After 26–28 h of sun drying, the tomato tissue had reached a moisture content of 15%. However, less drying time, about 10–11 h, was needed when starting with an initial moisture content of 92%. The tomato tissue had high ORAC and polyphenol content values after convective oven drying at 60 °C. The dried tomato samples had a satisfactory taste, color and antioxidant values.

scholarly journals Influence of Temperature and Moisture Content on Thermal Performance of Green Roof Media

Energies ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2421
Author(s):  
Bohan Shao ◽  
Caterina Valeo ◽  
Phalguni Mukhopadhyaya ◽  
Jianxun He
Keyword(s):  
Thermal Conductivity ◽  
Moisture Content ◽  
Green Roof ◽  
Green Roofs ◽  
Power Functions ◽  
Thick Substrate ◽  
Different Temperatures ◽  
Test Cells ◽  
Substrate Moisture ◽  
Phase Transition Zone

The influence of moisture content on substrate thermal conductivity at different temperatures was investigated for four different commercially available substrates for green roofs. In the unfrozen state, as moisture content increased, thermal conductivity increased linearly. In the phase transition zone between +5 and −10 °C, as temperature decreased, thermal conductivity increased sharply during the transition from water to ice. When the substrate was frozen, thermal conductivity varied exponentially with substrate moisture content prior to freezing. Power functions were found between thermal conductivity and temperature. Two equally sized, green roof test cells were constructed and tested to compare various roof configurations including a bare roof, varying media thickness for a green roof, and vegetation. The results show that compared with the bare roof, there is a 75% reduction in the interior temperature’s amplitude for the green roof with 150 mm thick substrate. When a sedum mat was added, there was a 20% reduction in the amplitude of the inner temperature as compared with the cell without a sedum mat.

scholarly journals Overview of Popular Techniques of Raman Spectroscopy and Their Potential in the Study of Plant Tissues

Molecules ◽  
2021 ◽  
Vol 26 (6) ◽  
pp. 1537
Author(s):  
Aneta Saletnik ◽  
Bogdan Saletnik ◽  
Czesław Puchalski
Keyword(s):  
Raman Spectroscopy ◽  
Cell Walls ◽  
Structural Changes ◽  
Spatial Information ◽  
Technological Development ◽  
Analytical Techniques ◽  
High Sensitivity ◽  
Plant Tissues ◽  
Wide Range ◽  
Identification Technique

Raman spectroscopy is one of the main analytical techniques used in optical metrology. It is a vibration, marker-free technique that provides insight into the structure and composition of tissues and cells at the molecular level. Raman spectroscopy is an outstanding material identification technique. It provides spatial information of vibrations from complex biological samples which renders it a very accurate tool for the analysis of highly complex plant tissues. Raman spectra can be used as a fingerprint tool for a very wide range of compounds. Raman spectroscopy enables all the polymers that build the cell walls of plants to be tracked simultaneously; it facilitates the analysis of both the molecular composition and the molecular structure of cell walls. Due to its high sensitivity to even minute structural changes, this method is used for comparative tests. The introduction of new and improved Raman techniques by scientists as well as the constant technological development of the apparatus has resulted in an increased importance of Raman spectroscopy in the discovery and defining of tissues and the processes taking place in them.

UV-microscopic analysis of acetylated spruce and birch cell walls

Holzforschung ◽  
2004 ◽  
Vol 58 (5) ◽  
pp. 483-488 ◽  
Author(s):  
Christian Hansmann ◽  
Manfred Schwanninger ◽  
Barbara Stefke ◽  
Barbara Hinterstoisser ◽  
Wolfgang Gindl
Keyword(s):  
Cell Walls ◽  
Middle Lamella ◽  
Microscopic Analysis ◽  
Weight Percent ◽  
Cellular Level ◽  
Uv Spectrum ◽  
Spectral Shifts ◽  
Microscopy Analysis ◽  
Absorbance Peak ◽  
Absorbance Spectra

Abstract Spruce and birch earlywood was acetylated to different weight percent gains using three different acetylation procedures. The absorbance spectra of secondary cell wall and compound cell corner middle lamella were determined by means of UV microscopy. Analysis of the spectra showed that the characteristic lignin absorbance peak in the UV spectrum of wood around 280 nm shifted to shorter wavelengths in acetylated samples. A distinct relationship between achieved weight percent gains after acetylation and observed spectral shifts could be established revealing a certain potential to measure acetylation on a cellular level by means of UV microscopy.

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