Mechanical characterization and damage events of flax fabric-reinforced biopolymer composites

2019 ◽  
Vol 28 (8-9) ◽  
pp. 631-644
Author(s):  
Abderrazak Chilali ◽  
Mustapha Assarar ◽  
Wajdi Zouari ◽  
Hocine Kebir ◽  
Rezak Ayad
Keyword(s):  
Tensile Modulus ◽  
Tensile Tests ◽  
Natural Fibre ◽  
Poly Lactic Acid ◽  
Fibre Reinforcement ◽  
Butylene Succinate ◽  
Environment Friendly ◽  
Biodegradable Composite ◽  
Biodegradable Poly ◽  
Biopolymer Composites

Natural fibre-reinforced biopolymer composites are of special interest because they are entirely bioresourced, recyclable and biodegradable. Poly(lactic acid) (PLA), poly(hydroxybutyrate- co-hydroxyvalerate) (PHBV) and poly(butylene succinate) (PBS) are among the most known environment-friendly biodegradable thermoplastics. Unfortunately, they present unbalanced mechanical characteristics when they are taken separately. The aim of this work is to overcome this problem using a blending process accompanied with fibre reinforcement. For this purpose, entirely biodegradable composite materials were fabricated and characterized. These biocomposites are based on two different ternary PLA/PHBV/PBS blends reinforced with twill flax fabrics and fabricated using extrusion and film-stacking techniques. Monotonic and cyclic load–unload tensile tests followed by acoustic emission and scanning electron microscopy observations were performed. In particular, the obtained biocomposites present interesting mechanical properties with a tensile modulus of 20 GPa and an ultimate tensile strength of 110 MPa.

scholarly journals Impact Toughness and Ductility Enhancement of Biodegradable Poly(lactic acid)/Poly(ε-caprolactone) Blends via Addition of Glycidyl Methacrylate

2013 ◽  
Vol 2013 ◽  
pp. 1-8 ◽  
Author(s):  
Wei Kit Chee ◽  
Nor Azowa Ibrahim ◽  
Norhazlin Zainuddin ◽  
Mohd Faizal Abd Rahman ◽  
Buong Woei Chieng
Keyword(s):  
Lactic Acid ◽  
Impact Strength ◽  
Glycidyl Methacrylate ◽  
Interfacial Adhesion ◽  
Tensile Modulus ◽  
Sem Analysis ◽  
Poly Lactic Acid ◽  
Biodegradable Poly ◽  
Interfacial Compatibility ◽  
The Impact

Poly(lactic acid) (PLA)/poly(ε-caprolactone) (PCL) blends were prepared via melt blending technique. Glycidyl methacrylate (GMA) was added as reactive compatibilizer to improve the interfacial adhesion between immiscible phases of PLA and PCL matrices. Tensile test revealed that optimum in elongation at break of approximately 327% achieved when GMA loading was up to 3wt%. Slight drop in tensile strength and tensile modulus at optimum ratio suggested that the blends were tuned to be deformable. Flexural studies showed slight drop in flexural strength and modulus when GMA wt% increases as a result of improved flexibility by finer dispersion of PCL in PLA matrix. Besides, incorporation of GMA in the blends remarkably improved the impact strength. Highest impact strength was achieved (160% compared to pure PLA/PCL blend) when GMA loading was up to 3 wt%. SEM analysis revealed improved interfacial adhesion between PLA/PCL blends in the presence of GMA. Finer dispersion and smooth surface of the specimens were noted as GMA loading increases, indicating that addition of GMA eventually improved the interfacial compatibility of the nonmiscible blend.

scholarly journals Morphology, Thermal, Mechanical Properties and Rheological Behavior of Biodegradable Poly(butylene succinate)/poly(lactic acid) In-Situ Submicrofibrillar Composites

Materials ◽  
2018 ◽  
Vol 11 (12) ◽  
pp. 2422 ◽  
Author(s):  
Zhiwen Zhu ◽  
Hezhi He ◽  
Bin Xue ◽  
Zhiming Zhan ◽  
Guozhen Wang ◽  
...  
Keyword(s):  
Lactic Acid ◽  
Cold Drawing ◽  
Mechanical Analysis ◽  
Poly Lactic Acid ◽  
Fiber Morphology ◽  
Molding Process ◽  
Butylene Succinate ◽  
Low Frequencies ◽  
Biodegradable Poly

In this study, biodegradable poly(butylene succinate)/poly(lactic acid) (PBS/PLA) in-situ submicrofibrillar composites with various PLA content were successfully produced by a triple-screw extruder followed by a hot stretching−cold drawing−compression molding process. This study aimed to investigate the effects of dispersed PLA submicro-fibrils on the thermal, mechanical and rheological properties of PBS/PLA composites. Morphological observations demonstrated that the PLA phases are fibrillated to submicro-fibrils in the PBS/PLA composites, and all the PLA submicro-fibrils produced seem to have a uniform diameter of about 200nm. As rheological measurements revealed, at low frequencies, the storage modulus (G’) of PBS/PLA composites has been increased by more than four orders of magnitude with the inclusion of high concentrations (15 wt % and 20 wt %) of PLA submicro-fibrils, which indicates a significant improvement in the elastic responses of PBS melt. Dynamic Mechanical Analysis (DMA) results showed that the glass transition temperature (Tg) of PBS phase slightly shifted to the higher temperature after the inclusion of PLA. DSC experiments proved that fiber morphology of PLA has obvious heterogeneous nucleation effect on the crystallization of PBS. The tensile properties of the PBS/PLA in-situ submicrofibrillar composites are also improved compared to neat PBS.

Production of a Green Composite: Mixture of Poly (Latic Acid) and Keratin Fibers from Chicken Feathers

2008 ◽  
Vol 47-50 ◽  
pp. 1225-1228 ◽  
Author(s):  
Yong Qing Zhao ◽  
Kin Tak Lau ◽  
Tao Liu ◽  
Sha Cheng ◽  
Pou Man Lam ◽  
...  
Keyword(s):  
Tensile Modulus ◽  
Tensile Tests ◽  
Poly Lactic Acid ◽  
Green Composite ◽  
Elongation At Break ◽  
Chicken Feathers ◽  
Composite Mixture ◽  
Keratin Fibers ◽  
Feather Fiber ◽  
First Time

A new biocomposite based on chicken feather fiber (CFF) and Poly (lactic acid) (PLA) was fabricated for the first time by melting compound methods. Its mechanical properties and fracture surfaces were investigated by using tensile tests and scanning electron microscopy (SEM), respectively. The results showed that the tensile modulus and elongation at break of PLA samples were improved by adding a small amount of CFF. The elongation at break of a CFF/PLA sample with 2 wt% of CFF was 56% higher than that of pure PLA. This may ascribe to the good adhesion and interactions between the CFF and PLA matrix.

scholarly journals Tensile Properties of Pandanus Atrocarpus based Composites

1970 ◽  
Vol 1 (1) ◽  
Author(s):  
Hoo Tien Nicholas Kuan ◽  
Meng Chuen Lee
Keyword(s):  
Tensile Properties ◽  
Composite Laminates ◽  
Volume Fraction ◽  
Tensile Tests ◽  
Natural Fibre ◽  
Engineering Industry ◽  
Strength Increase ◽  
Fibre Reinforcement ◽  
Compression Moulding ◽  
Composite Fabrication

Pandanus atrocarpus, or locally known as mengkuang plant is likely to be potential natural fibre reinforcement in composite. Both the Pandanus leaves, and fibres extracted from the Pandanus leaves were used in composite fabrication. Fibres were extracted from Pandanus leaves with water retting process. Pandanus composites were laminated using compression moulding method. The tensile properties of composite laminates based on lamination of Pandanus leaf- and extracted Pandanus fibre-reinforced polyethylene were investigated. Tensile tests have shown that composite laminates based on extracted Pandanus fibre reinforced polyethylene were more superior than using the Pandanus leaf itself without extracting its fibre. Tests exhibited that increasing the volume fraction of Pandanus fibre resulted in strength increase. This suggests that Pandanus fibre- based composites could offer a range of mechanical properties for use in the engineering industry.

A Review on Mechanical Properties of Natural Fibre Reinforced PLA Composites

2021 ◽  
Vol 15 ◽  
Author(s):  
Agnivesh Kumar Sinha ◽  
Kasi Raja Rao ◽  
Vinay Kumar Soni ◽  
Rituraj Chandrakar ◽  
Hemant Kumar Sharma ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Polymer Composites ◽  
Biodegradable Polymer ◽  
Weight Ratio ◽  
Natural Fibre ◽  
Polymer Matrices ◽  
Poly Lactic Acid ◽  
Butylene Succinate ◽  
Reinforced Polymer ◽  
Fibre Reinforced Polymer

Presently, scientists and researchers are in an endless quest to develop green, recyclable, and eco-friendly materials. Natural fibre reinforced polymer composites became popular among materialists due to their lightweight, high strength-to-weight ratio, and biodegradability. However, all-natural fibre reinforced polymer composites are not biodegradable. Polymer matrices like poly-lactic acid (PLA) and poly-butylene succinate (PBS) are biodegradable, whereas epoxy, polypropylene, and polystyrene are non-biodegradable polymer matrices. Besides biodegradability, PLA has been known for its excellent physical and mechanical properties. This review emphasises the mechanical properties (tensile, flexural, and impact strengths) of natural fibrereinforced PLA composites. Factors affecting the mechanical properties of PLA composites are also discussed. It also unveils research gaps from the previous literature, which shows that limited studies are reported based on modeling and prediction of mechanical properties of hybrid PLA composites reinforcing natural fibres like abaca, aloe vera, and bamboo fibres.

Bio-nanocomposites based on compatibilized poly(lactic acid) blend-reinforced agave cellulose nanocrystals

BioResources ◽  
2021 ◽  
Vol 16 (3) ◽  
pp. 5538-5555
Author(s):  
Noor Afizah Rosli ◽  
Wan Hafizi Wan Ishak ◽  
Siti Salwani Darwis ◽  
Ishak Ahmad ◽  
Mohammad Fauzul Azim Mohd Khairudin
Keyword(s):  
Lactic Acid ◽  
Water Absorption ◽  
Cellulose Nanocrystals ◽  
Tensile Modulus ◽  
Crystallization Rate ◽  
Tensile Tests ◽  
Absorption Capacity ◽  
Poly Lactic Acid ◽  
Mechanical And Thermal Properties ◽  
Green Materials

Enhancing the mechanical, thermal, and degradation properties of a poly(lactic acid) (PLA) blend without deteriorating its other useful features was the goal of this work. The isolation of cellulose nanocrystals (CNCs) from Agave angustifolia fibers was carried out, and the properties of the bio-nanocomposites comprising these CNCs were evaluated, which included PLA, natural rubber (NR), and liquid NR (LNR). Transmission electron microscopy and zeta potential analysis confirmed the successful isolation of CNCs from agave fibers after several chemical treatment steps. The effects of different CNC loadings on the properties of the bio-nanocomposites were investigated using tensile tests, thermal analysis, morphological analysis, and water absorption tests. Bio-nanocomposites containing 5 wt% and 7.5 wt% CNC had the optimal tensile modulus and strength, respectively. Different levels of CNC did not noticeably affect the thermal stability of the bio-nanocomposites, although the thermogram curves increased slightly as CNC content increased. The addition of CNC at different loadings affects the crystallization rate of PLA blend. The water absorption capacity increased as CNC level increased, and 5 wt% CNC gave rise to the highest water absorption. The four-component bio-nanocomposites created in this study provided an alternative for producing new green materials with tunable physical, mechanical, and thermal properties.

Additive Manufacturing of PA6 with Short Carbon Fibre Reinforcement Using Fused Deposition Modelling

2018 ◽  
Vol 928 ◽  
pp. 26-31 ◽  
Author(s):  
Frantisek Sedlacek ◽  
Václava Lašová
Keyword(s):  
Additive Manufacturing ◽  
Tensile Modulus ◽  
Tensile Tests ◽  
Fused Deposition Modelling ◽  
Fibre Reinforcement ◽  
3D Printer ◽  
Carbon Fibres ◽  
Fused Deposition ◽  
Additive Manufacturing Technology ◽  
Short Carbon

The aim of this research was to determine the influence of the short carbon fibres in nylon PA6 polymer used for fused deposition modelling (additive manufacturing) technology. Specimens from pure PA6 and PA6 with short carbon fibres were fabricated, with both main directions of the material with respect to the build orientation in a 3D printer. Experimental tensile tests of the specimens were carried out at several temperatures according to ISO standards. The strength, tensile modulus and ductility in relation to the temperature were compared. A significant influence of the short carbon fibres on the strength and heat deflection temperature of the part was found in PA6 and also for the orientation of the build in the 3D printer.

scholarly journals Fully Biodegradable Composites: Thermal, Flammability, Moisture Absorption and Mechanical Properties of Natural Fibre-Reinforced Composites with Nano-Hydroxyapatite

Materials ◽  
2019 ◽  
Vol 12 (7) ◽  
pp. 1145 ◽  
Author(s):  
Pooria Khalili ◽  
Xiaoling LIU ◽  
Zirui ZHAO ◽  
Brina Blinzler
Keyword(s):  
Mechanical Properties ◽  
Moisture Absorption ◽  
Flexural Modulus ◽  
Tensile Modulus ◽  
Natural Fibre ◽  
Poly Lactic Acid ◽  
Degradation Temperature ◽  
Conventional Film ◽  
Natural Fabrics ◽  
Burn Rate

Natural fibre-reinforced poly(lactic acid) (PLA) laminates were prepared by a conventional film stacking method from PLA films and natural fabrics with a cross ply layup of [0/90/0/90/0/90], followed by hot compression. Natural fibre (NF) nano-hydroxyapatite (nHA) filled composites were produced by the same manufacturing technique with matrix films that had varying concentrations of nHA in the PLA. Their flammability, thermal, moisture absorption and mechanical properties were analysed in terms of the amount of nHA. The flame behavior of neat PLA and composites evaluated by the UL-94 test demonstrated that only the composite containing the highest quantity of nHA (i.e., 40 wt% nHA in matrix) was found to achieve an FH-1 rating and exhibited no recorded burn rate, whereas other composites obtained only an FH-3. The thermal degradation temperature and mass residue were also observed, via thermogravimetric analysis, to increase when increasing concentrations of nHA were added to the NF composite. The tensile strength, tensile modulus and flexural modulus of the neat resin were found to increase significantly with the introduction of flax fibre. Conversely, moisture absorption was found to increase and mechanical properties to decrease with both the presence of NF and increasing concentrations of nHA, and subsequent mechanical properties experienced an obvious reduction.

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