scholarly journals Organic Residues Analysis of Oil Bottle of Goryeo Dynasty Excavated from the Soejeoul Site, Geumneung-dong, Chungju

2021 ◽  
Vol 37 (6) ◽  
pp. 638-647
Author(s):  
Eun Young Yun ◽  
Suyeon Kim
Keyword(s):  
Fatty Acids ◽  
Fourier Transform ◽  
Sesame Oil ◽  
Organic Residues ◽  
Gas Chromatograph ◽  
Natural Sources ◽  
Sesame Seeds ◽  
Scientific Analysis ◽  
Ft Ir ◽  
Characteristic Component

Organic residues are substances derived from diverse natural sources. Recent scientific analysis of organic residues has yielded important information in restoring the lifestyles of ancient peoples. In this study, the organic material contained within the celadon oil bottle of the Goryeo dynasty, excavated from the Soejoul site in Geumneung-dong, Chungju, was analyzed using Fourier-transform infrared spectroscopy (FT-IR) and gas chromatograph-mass spectrometer (GC-MS). The results showed that the organic materials in the bottle were plant-derived oils. In particular, polyunsaturated fatty acids and phytosterols were detected using GC-MS analysis. Sesamin components were also identified. Sesamin, which is a characteristic component of sesame seeds, is a lignan and an antioxidant. As the organic residues in the oil bottle were derived from sesame seeds, it is presumed that sesame oil was stored in the bottle.

scholarly journals Extraction and Characterization of Sugarcane Peel Wax

ISRN Agronomy ◽  
2012 ◽  
Vol 2012 ◽  
pp. 1-6 ◽  
Author(s):  
Mangesh B. Inarkar ◽  
S. S. Lele
Keyword(s):  
Fatty Acids ◽  
Molecular Weight ◽  
Gas Chromatography ◽  
Fourier Transform ◽  
Dry Weight ◽  
Weight Basis ◽  
Ft Ir ◽  
Gas Chromatography Mass Spectroscopy ◽  
Layer Chromatography

Sugarcane peel is an agrowaste product and contains considerable amount of wax. This has a good technoeconomic potential. In view of this, the present study aims at extraction and characterization of wax from sugarcane peel. The yield of crude wax was 0.95% on dry weight basis. During Fourier transform-infrared spectroscopy (FT-IR) prominent peaks obtained at 2921.73 and 2851.64 (–CH), 1463.44 (–CH2), 1376.96 (–CH3), 1108.4 and 1170.16 (–C–O) 3395.60 (–OH), 1710.25 (–CHO), and 1736.63 (–COOH) indicate presence of alkanes, ketones, alcohols, aldehydes, and carboxylic acids, respectively. Alcohol and hydrocarbon fractions were also found by thin layer chromatography (TLC). Melting point of crude wax was observed to be 62.1°C. Molecular weight of wax was estimated to be 1706 Dalton. Composition of crude wax found using gas chromatography-mass spectroscopy (GC-MS) was alkanes (28.83%), ester (66.26%), fatty acids (4.58%), aldehyde (0.11%), and alcohol (0.22%).

scholarly journals Effects of encapsulated black caraway extract and sesame oil on kolompeh quality

2019 ◽  
pp. 311-320
Author(s):  
Fatemeh Soltaninejad ◽  
Seyed Saeed Sekhavatizadeh
Keyword(s):  
Adverse Effect ◽  
Fatty Acids ◽  
Gas Chromatography ◽  
Fourier Transform ◽  
Infrared Spectroscopy ◽  
Oxidative Stability ◽  
Size Distribution ◽  
Sesame Oil ◽  
Colour Parameters ◽  
Oleic And Linoleic Acids

In this study, the physicochemical and sensory properties of kolompeh containing black caraway and sesame oil were investigated. Black caraway extract (BCE), encapsulated black caraway extract (EBCE), and black caraway powder (BCP) were added to kolompeh and compared to the sample without black caraway (FBC). All products contained sesame oil and were compared to control (without sesame oil). Among the samples, kolompeh with encapsulated extract demonstrated a higher oxidative stability (24.37 h), with a high IC50 of black caraway extract (124.1 μg·mL–1). In addition, the emulsion exhibited size distribution between 3.20 and 8.51 μm, and Fourier transform infrared spectroscopy confirmed the well encapsulated extract. Gas chromatography identified oleic and linoleic acids as the main fatty acids in kolompeh with the black caraway encapsulated extract. Although, there were no significant differences in the colour parameters (L*, a* and b*) of the samples, kolompeh with EBCE had the highest score given by panelists. The control had a higher (2466 g) hardness compared to kolompeh containing EBCE (1688 g) at the end of storage. Therefore, the encapsulated extract of black caraway not only had no an adverse effect on the properties of kolompeh but also improved its quality.

scholarly journals Genetic Potential and Possible Improvement of Sesamum indicum L.

2020 ◽  
Author(s):  
Muthulakshmi Chellamuthu ◽  
Selvi Subramanian ◽  
Manonmani Swaminathan
Keyword(s):  
Fatty Acids ◽  
Unsaturated Fatty Acids ◽  
Saturated Fatty Acids ◽  
Sesame Seed ◽  
Sesamum Indicum ◽  
Sesame Oil ◽  
Sesame Seeds ◽  
High Yielding Varieties ◽  
Sugar Levels ◽  
The Stability

Sesame (Sesamum indicum L.) is one of the traditional oil seed crop widely cultivated in many countries. The top producers of sesame seeds are mainly Tanzania, Myanmar, India, China and Japan. Sesame oil contains high level of unsaturated fatty acids (80%) and low levels of saturated fatty acids (20%). The main fatty acids are palmitic, stearic, oleic, linoleic and trace amounts of linolenic fatty acids. Sesame seed contains 50–60% of high-quality oil rich in natural antioxidants such as sesamin, sesamolin, sesaminol and sesamol it enhances the stability and keeping quality of sesame oil. Sesame seeds have good sources of dietary fibre, fats, vitamins, minerals, proteins and rich in anti-oxidants. Polyunsaturated fatty acids in sesame will reduce the risk of high blood pressure, cardiac disorders and blood sugar levels. Sesame is believed to have been originated in India where maximum variability of genetic resources is available. High yielding varieties available to date have reached the yield plateau even with the advanced cultivation practices. The area under oilseed crops cultivation also reducing every year. Hence, there is an urgent need to increase the oil content and yield of Indian sesame varieties. Understanding the available germplasm and novel interventions to develop high yielding varieties warrant both molecular and phenotypic data which is meagre in case of sesame.

scholarly journals Characterization of Neocarya Macrophylla Seed Oil using Gas Chromatography-Mass Spectrometry (GC-MS) and Fourier Transform Infra-Red (FT-IR) Techniques

2019 ◽  
pp. 1-7
Author(s):  
Aliyu Ahmad Warra ◽  
Lawal Gusau Hassan ◽  
Leye Jonathan Babatola ◽  
Adedara Adejoju Omodolapo ◽  
Richard Undigweundeye Ukpanukpong ◽  
...  
Keyword(s):  
Fatty Acids ◽  
Gas Chromatography ◽  
Fourier Transform ◽  
Seed Oil ◽  
Saturated Fatty Acids ◽  
Soxhlet Extraction ◽  
Industrial Applications ◽  
Pharmaceutical Products ◽  
Gas Chromatography Mass Spectrometry ◽  
Ft Ir

Aim: Modern researches described incorporating gingerbread plum (Neocarya macrophylla) kernel oils into food, cosmetics and pharmaceutical products by exploiting its physicochemical properties. Study Design: Experimental and instrumental study was done to determine the general and the saturated fatty acids present in the seed oil and its suitability for industrial applications. This study examined the fatty acids by qualitative determination from hexane extracts of Neocarya macrophylla seed using GC-MS. Materials and Methods: Indigenous Neocarya macrophylla   seeds obtained from Gingerbread plum tree were collected in the Month of August from Birnin Kebbi, Kebbi State, Nigeria. soxhlet extraction method was used for the oil extraction. The GC-MS analysis was by coupling system of Shimadzu QP2010 series gas chromatography with Shimadzu QP2010 plus mass spectroscopy detector (GCMS).  For the FT-IR analysis, software of OMNIC operating system (Version 7.0 Thermo Nicolet) was connected to Fourier Transform Infrared Spectrometer Nicolet 8400S equipped with a detector of deuterated triglycine sulphate (DTGS). Conclusion: These results showed the potential of this oil in cosmetic industry.

scholarly journals Fourier Transform Infra-Red (FT-IR) Characterization of Plant Oils from Selected Cultivars Grown in Nigeria

2019 ◽  
pp. 1-10
Author(s):  
A. A. Warra ◽  
L. J. Babatola ◽  
L. G. Hassan ◽  
M. N. V. Prasad ◽  
A. A. Odutuga ◽  
...  
Keyword(s):  
Fatty Acids ◽  
Fourier Transform ◽  
Energy Demand ◽  
Alternative Energy ◽  
Degree Of Saturation ◽  
Plant Oils ◽  
Background Spectrum ◽  
Infra Red ◽  
Ft Ir

Background and Objectives: The developments of fourier transform infrared (FT-IR) spectroscopic instrumentation, and application, over the years has made it a powerful analytical tool in the study of oils and fats. This work has explored fourier transform Infra-Red for characterization of plant oils from selected cultivars grown in Nigeria. The selection of these plants oils that flourishes in Nigeria aside their used primarily for nutritional applications, is dependent on the fatty acid (FA) composition of triacylglycerol (TAG which make them potential for bioenergy and biofiuel production considering the explosion of energy demand through alternative energy sources. They are also needed for the preparations of chemical feedstocks, biopolymer and composites, skin care products. Oils from these plants can provide renewable sources of high-value fatty acids for both the chemical and health-related industries. We report here several areas where these plant oils can have a significant impact on the emerging bioeconomy. Materials and Methods: The samples were each placed in contact with KBr disc and FT-IR spectra were collected in frequency 4500-400 cm-1 by coadding 32 scans and at resolution of 4 cm-1. All spectra were rationed against a background spectrum. In each scan, a new reference background spectrum was detected. Results: The spectra of oils of the present investigation revealed the following bands 1522, 1449.55, 1364.68, 1444.73, 1364.68, 1445.09, 1369.50, 1447.62, 1362.75, 1449.55, 1371.43, 1447.62, 1366.54, 1447.62, 1450.5, 1360.82, 1370.47, 1446.66, 1246.06, 1364.47, 1448.59 for Adansonia digitata, Ricinus communis, Sesamum indicum, Jatropha curcas, Allium cepa, Cucumis melo, Lannea microcarpa, Lagenaria vulgaris and Sesamun indicum seed oil respectively. 1450 cm-1- 1444 is related to bending vibration of CH2, and CH3; (cis =C–H bending) and at 1360 - 1370 cm-1 is concerned with the bending vibrations CH2 groups which showed total unsaturation. The results obtained shows that all the oils are unsaturated because there is no band around 3005- 3009 which is the band that normally determine the index of degree of unsaturation. Conclusion: The FT- IR spectroscopy proved to be an important technique for identification, analysis, determination of degree of saturation of fatty acids in oils suitable for industrial applications.

FR-IR Molecular Microanalysis System

1990 ◽  
Vol 48 (2) ◽  
pp. 270-271
Author(s):  
John A. Reffner ◽  
William T. Wihlborg
Keyword(s):  
Fourier Transform ◽  
Fourier Transform Infrared ◽  
Integrated System ◽  
Morphological Examination ◽  
Fully Integrated ◽  
Ir Microscopy ◽  
Normal Functions ◽  
Infrared Microspectroscopy ◽  
Infrared Spectral ◽  
Ft Ir

The IRμs™ is the first fully integrated system for Fourier transform infrared (FT-IR) microscopy. FT-IR microscopy combines light microscopy for morphological examination with infrared spectroscopy for chemical identification of microscopic samples or domains. Because the IRμs system is a new tool for molecular microanalysis, its optical, mechanical and system design are described to illustrate the state of development of molecular microanalysis. Applications of infrared microspectroscopy are reviewed by Messerschmidt and Harthcock.Infrared spectral analysis of microscopic samples is not a new idea, it dates back to 1949, with the first commercial instrument being offered by Perkin-Elmer Co. Inc. in 1953. These early efforts showed promise but failed the test of practically. It was not until the advances in computer science were applied did infrared microspectroscopy emerge as a useful technique. Microscopes designed as accessories for Fourier transform infrared spectrometers have been commercially available since 1983. These accessory microscopes provide the best means for analytical spectroscopists to analyze microscopic samples, while not interfering with the FT-IR spectrometer’s normal functions.

Effects of in-Office and at-Home Bleaching on Human Enamel and Dentin: An in vitro Application of Fourier Transform Infrared Study

2008 ◽  
Vol 62 (11) ◽  
pp. 1274-1279 ◽  
Author(s):  
Feride Severcan ◽  
Kurtulus Gokduman ◽  
Ayca Dogan ◽  
Sukran Bolay ◽  
Saadet Gokalp
Keyword(s):  
Fourier Transform ◽  
Structural Changes ◽  
Protein Denaturation ◽  
Random Coil ◽  
Protein Ratio ◽  
Band Frequency ◽  
Human Enamel ◽  
Ft Ir ◽  
At Home

In-office and at-home bleaching techniques are widely used methods for the whitening of teeth. However, the safety of these techniques has not been clarified yet. The aim of the current study is to investigate the in-office- and at-home-bleaching-induced structural and quantitative changes in human enamel and dentin at the molecular level, under in vitro conditions. The Fourier transform mid-infrared (mid-FT-IR) spectroscopic technique was used to monitor bleaching-induced structural changes. Band frequency and intensity values of major absorptions such as amide A, amide I, phosphate (PO4), and carbonate (CO3−2) bands, for treatment groups and control, were measured and compared. The results revealed that both procedures have negligible effects on dentin constituents. In office-bleached enamel, in addition to demineralization, a decrease in protein and polysaccharide concentrations, mineral-to-protein ratio, and the strength of hydrogen bonds around NH groups, as well as a change in protein secondary structure were observed. The protein structure changed from β-sheet to random coil, which is an indication of protein denaturation. However, no significant variations were observed for at-home bleached enamel. The control, at-home, and in-office bleached enamel samples were differentiated with a high accuracy using cluster analysis based on FT-IR data. This study revealed that office bleaching caused deleterious alterations in the composition and structure of enamel that significantly affected the crystallinity and mineralization of the tissue. Therefore, at-home bleaching seems to be much safer than in-office bleaching in terms of molecular variations.

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