scholarly journals Electroless Deposition of Composite Nickel-Phosphorous Coatings with Diamond Dispersoid

2016 ◽  
Vol 61 (2) ◽  
pp. 493-498 ◽  
Author(s):  
M. Petrova ◽  
M. Georgieva ◽  
V. Chakarova ◽  
E. Dobreva
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Chemical Composition ◽  
Electroless Deposition ◽  
Deposition Time ◽  
Composite Coatings ◽  
Flexible Substrates ◽  
Optimal Conditions ◽  
Sem Images ◽  
Scanning Electron

AbstractThe composite Ni-P coating with diamond particles (D) deposited on the flexible substrates of pressed polyethylene terephthalate material (PET) was obtained, to be used in the development of efficient, flexible grinding and polishing tools. The optimal conditions of the hydrodynamic regime, deposition time and temperature were found. The influence of the concentration and size of the D particles (3/7 ÷ 225/300 μm) on the coating thickness and number of co-deposited particles were studied. By Scanning Electron Microscopy (SEM) images were defined the morphology of dispersion coatings and number of co-deposited particles in them, and Energy Dispersive Spectroscopy (EDS/INCA) was used to determine the elemental chemical composition of the composite coatings.

scholarly journals Microscopy Methods for Biofilm Imaging: Focus on SEM and VP-SEM Pros and Cons

Biology ◽  
2021 ◽  
Vol 10 (1) ◽  
pp. 51
Author(s):  
Michela Relucenti ◽  
Giuseppe Familiari ◽  
Orlando Donfrancesco ◽  
Maurizio Taurino ◽  
Xiaobo Li ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Ion Beam ◽  
Ruthenium Red ◽  
Variable Pressure ◽  
Sem Images ◽  
Advantages And Disadvantages ◽  
Pros And Cons ◽  
Microscopy Techniques ◽  
Scanning Electron

Several imaging methodologies have been used in biofilm studies, contributing to deepening the knowledge on their structure. This review illustrates the most widely used microscopy techniques in biofilm investigations, focusing on traditional and innovative scanning electron microscopy techniques such as scanning electron microscopy (SEM), variable pressure SEM (VP-SEM), environmental SEM (ESEM), and the more recent ambiental SEM (ASEM), ending with the cutting edge Cryo-SEM and focused ion beam SEM (FIB SEM), highlighting the pros and cons of several methods with particular emphasis on conventional SEM and VP-SEM. As each technique has its own advantages and disadvantages, the choice of the most appropriate method must be done carefully, based on the specific aim of the study. The evaluation of the drug effects on biofilm requires imaging methods that show the most detailed ultrastructural features of the biofilm. In this kind of research, the use of scanning electron microscopy with customized protocols such as osmium tetroxide (OsO4), ruthenium red (RR), tannic acid (TA) staining, and ionic liquid (IL) treatment is unrivalled for its image quality, magnification, resolution, minimal sample loss, and actual sample structure preservation. The combined use of innovative SEM protocols and 3-D image analysis software will allow for quantitative data from SEM images to be extracted; in this way, data from images of samples that have undergone different antibiofilm treatments can be compared.

scholarly journals SEM, EDS and Electrical Capacitance Study on Electrodeposited Ni-Cu Layers

2019 ◽  
Vol 70 (9) ◽  
pp. 3210-3212
Author(s):  
Oana Claudia Ciobotea Barbu ◽  
Ioana Alina Ciobotaru ◽  
Anca Cojocaru ◽  
Florin Mihai Benga ◽  
Danut Ionel Vaireanu
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Chemical Composition ◽  
Electrochemical Method ◽  
Steel Substrate ◽  
Distilled Water ◽  
Electrical Capacitance ◽  
Nickel Copper ◽  
Scanning Electron

Nickel-Copper metallic layers were deposited onto a steel substrate by using the electrochemical method. The morphology and the chemical composition of the deposited layers were studied by scanning electron microscopy. The electrical capacitance was measured on a functional supercapacitor made of two Ni-Cu deposited layers and a Nafion 117� membrane hydrated with distilled water, which served as a dielectric separator.

scholarly journals Surface Properties of Silica–MWCNTs/PDMS Composite Coatings Deposited on Plasma Activated Glass Supports

2021 ◽  
Vol 11 (19) ◽  
pp. 9256
Author(s):  
Michał Chodkowski ◽  
Iryna Ya. Sulym ◽  
Konrad Terpiłowski ◽  
Dariusz Sternik
Keyword(s):  
Electron Microscopy ◽  
Carbon Nanotubes ◽  
Scanning Electron Microscopy ◽  
Multiwalled Carbon Nanotubes ◽  
Composite Coatings ◽  
Thermal Analyses ◽  
Sol Gel ◽  
Visible Range ◽  
Multiwalled Carbon ◽  
Scanning Electron

In this paper, we focus on fabrication and physicochemical properties investigations of silica–multiwalled carbon nanotubes/poly(dimethylsiloxane) composite coatings deposited on the glass supports activated by cold plasma. Air or argon was used as the carrier gas in the plasma process. Multiwalled carbon nanotubes were modified with poly(dimethylsiloxane) in order to impart their hydrophobicity. The silica–multiwalled carbon nanotubes/poly(dimethylsiloxane) nanocomposite was synthesized using the sol–gel technique with acid-assisted tetraethyl orthosilicate hydrolysis. The stability and the zeta potential of the obtained suspension were evaluated. Then, the product was dried and used as a filler in another sol–gel process, which led to the coating application via the dip-coating method. The substrates were exposed to the hexamethyldisilazane vapors in order to improve their hydrophobicity. The obtained surfaces were characterized by the wettability measurements and surface free energy determination as well as optical profilometry, scanning electron microscopy, and transmittance measurements. In addition, the thermal analyses of the carbon nanotubes as well as coatings were made. It was found that rough and hydrophobic coatings were obtained with a high transmittance in the visible range. They are characterized by the water contact angle larger than 90 degrees and the transmission at the level of 95%. The X-ray diffraction studies as well as scanning electron microscopy images confirmed the chemical and structural compositions of the coatings. They are thermally stable at the temperature up to 250 °C. Moreover, the thermal analysis showed that the obtained composite material has greater thermal resistance than the pure nanotubes.

Fabrication of Ultra Thick Ferromagnetic Structures in Silicon

2004 ◽  
Author(s):  
Debbie G. Jones ◽  
Albert P. Pisano
Keyword(s):  
Electron Microscopy ◽  
Thin Films ◽  
Scanning Electron Microscopy ◽  
Saturation Magnetization ◽  
Silicon Wafer ◽  
Fabrication Process ◽  
Sem Images ◽  
Deep Reactive Ion Etching ◽  
Scanning Electron

A novel fabrication process is presented to create ultra thick ferromagnetic structures in silicon. The structures are fabricated by electroforming NiFe into silicon templates patterned with deep reactive ion etching (DRIE). Thin films are deposited into photoresist molds for characterization of an electroplating cell. Results show that electroplated films with a saturation magnetization above 1.6 tesla and compositions of approximately 50/50 NiFe can be obtained through agitation of the electrolyte. Scanning electron microscopy (SEM) images show that NiFe structures embedded in a 500 μm thick silicon wafer are realized and the roughening of the mold sidewalls during the DRIE aids in adhesion of the NiFe to the silicon.

The Fracture Failure Analysis of Precision Centrifuge Spindle

2014 ◽  
Vol 971-973 ◽  
pp. 802-805
Author(s):  
Wei Feng Zhang ◽  
Li Yan ◽  
Fu Xia Zhang
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Chemical Composition ◽  
Fracture Mechanics ◽  
Failure Analysis ◽  
Fatigue Failure ◽  
High Speed ◽  
Experimental Results ◽  
Fracture Failure ◽  
Scanning Electron

For the problem of high-speed rotating centrifuge spindle fracture failures, relevant analyses are conducted from the perspective of microstructure, chemical composition and fracture mechanics by using scanning electron microscopy and related instruments. Experimental results and analyses indicate that the spindle fracture is fatigue failure, mainly caused by cold cracks generated on the journal surfacing. Based on the analysis results, improvements and measures are suggested to better solve the spindle weld fracture failure problems.

Biomimetic Crack Sensors Using Electrohydrodynamic Technology

2021 ◽  
Vol 21 (7) ◽  
pp. 3773-3778
Author(s):  
Keon-Young Kim ◽  
Se-Min Jeong ◽  
Chang-Yull Lee
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Crack Initiation ◽  
Health Monitoring ◽  
Grid Structure ◽  
Sem Images ◽  
Impact Tester ◽  
Microscopic Damage ◽  
Pet Substrate ◽  
Scanning Electron

This paper proposes a new mechanism for detecting microscopic damage of structures based on imitating the sensory organs of spiders. Therefore, it is essential to manufacture sensors that can react sensitively to the micro deformations of structures. Numerous cracks were intentionally generated to improve the sensitivity of the proposed sensor, and an increase in the gap of the crack was observed by scanning electron microscopy (SEM) observation. Electrohydrodynamic technology is used to detect deformations in a structure of depositing Ag nano paste on a polyethylene terephtha-late (PET) substrate. Ag nano lines are also observed by SEM images. The sensor is constructed as a grid structure, by forming layers patterned horizontally and vertically. An impact tester is used to verify the mechanism for structural health monitoring using the developed sensor. The resistance changes of the sensors are applied to estimate the structure’s damaged location. The intersections of the lines with varying resistance can be used to accurately detect crack initiation. The proposed mechanism is a powerful methodology for estimating and detecting microscopic deformations and damage to structures.

Effect of moisturized air on magnetoimpedance response of Fe-based ribbons

2020 ◽  
Vol 34 (24) ◽  
pp. 2050249
Author(s):  
L. Yoosefi ◽  
V. Setoodeh
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Environmental Conditions ◽  
Surface Condition ◽  
High Sensitivity ◽  
Response Ratio ◽  
Sem Images ◽  
Weak Magnetic Fields ◽  
Magnetic Elements ◽  
Scanning Electron

High sensitivity and response ratio of magnetoimpedance (MI) sensors have raised interest for using them in different environments for detection of weak magnetic fields of magnetic elements even though the high dependence of the MI response to the surface condition of the MI sensor has limited its application in some environments. In this study, we investigate the effects originating from the MI measurement in moisturized air. Using scanning electron microscopy (SEM) images, it is observed that the surface of an Fe-based MI sensor has become rough and granular after the presence of moisture on its surface. Results can be useful for developing MI sensors for use in different environmental conditions.

A comparative study of the morphology, chemical composition and weathering of rhyolitic and andesitic glass

Clay Minerals ◽  
1980 ◽  
Vol 15 (2) ◽  
pp. 165-173 ◽  
Author(s):  
J. H. Kirkman ◽  
W. J. McHardy
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
New Zealand ◽  
Chemical Composition ◽  
Electron Probe ◽  
Volcanic Glass ◽  
Chemical Activity ◽  
Rapid Rate ◽  
Bonding Characteristics ◽  
Scanning Electron

AbstractThe morphology of volcanic glass particles in rhyolitic and andesitic tephra of central North Island and Taranaki areas of New Zealand has been studied by scanning electron microscopy. Electron probe analyses of the glasses are compared with those of the clays to which they weather. Loss of silica characterizes the weathering of both glasses. The rapid rate of weathering of andesitic glass is attributed to its occurrence as fine, soft microlites and extensive substitution of Al for Si in the structure. Rhyolitic glass weathers more slowly because it occurs as hard and brittle particles containing relatively little alumina. It is suggested that the structure, chemical composition and chemical activity of allophane is governed largely by the chemical composition and bonding characteristics of the parent glass.

Comparative study of the oxide scale thermally grown on titanium alloys by ion beam analysis techniques and scanning electron microscopy

2008 ◽  
Vol 23 (8) ◽  
pp. 2245-2253 ◽  
Author(s):  
A. Gutiérrez ◽  
F. Pászti ◽  
A. Climent-Font ◽  
J.A. Jiménez ◽  
M.F. López
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Chemical Composition ◽  
Titanium Alloys ◽  
Oxide Scale ◽  
Ion Beam ◽  
Elastic Recoil ◽  
Detection Analysis ◽  
Nb Content ◽  
Scanning Electron

In the present work, the oxide layers developed at elevated temperature on three vanadium-free titanium alloys, of interest as implant biomaterials, were studied by Rutherford backscattering spectroscopy, elastic recoil detection analysis, and scanning electron microscopy. The chemical composition of the alloys investigated, in wt%, was Ti–7Nb–6Al, Ti–13Nb–13Zr, and Ti–15Zr–4Nb. Upon oxidation in air at 750 °C, an oxide scale forms, with a chemical composition, morphology, and thickness that depend on the alloy composition and the oxidation time. After equal exposure time, the Ti–7Nb–6Al alloy exhibited the thinnest oxide layer due to the formation of an Al2O3-rich layer. The oxide scale of the two TiNbZr alloys is mainly composed of Ti oxides, with small amounts of Nb and Zr dissolved. For both TiNbZr alloys, the role of the Nb-content on the mechanism of the oxide formation is discussed.

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