scholarly journals Investigations on the Process of Lead Removal from Cu-Pb Alloys During their Melting in Vacuum Induction Furnace

2017 ◽  
Vol 62 (4) ◽  
pp. 2449-2453 ◽  
Author(s):  
G. Siwiec ◽  
P. Buliński ◽  
M. Palacz ◽  
J. Smołka ◽  
L. Blacha

AbstractThe paper presents analysis and assessment of operating power of vacuum induction furnace in relation to the efficiency of lead removal from Cu-Pb alloy in VIM (vacuum induction melting) technology. Thermodynamic analysis of the process is performed as well.

Author(s):  
B. L. Krasnii ◽  
K. I. Ikonnikov ◽  
V. S. Anikanov ◽  
A. L. Galganova ◽  
M. A. Mikhailov

The prospect of using crystalline fused magnesia (FL LC) in the manufacture technology of melting crucibles by the method of isostatic pressing is shown. It has been established that the production of a material based on MgO using concrete technology is limited to the hydration and loosening of the structure due to the formation and subsequent decomposition of brucite (native magnesia). The physical and mechanical characteristics of the obtained products are given. The effect of the CaO/SiO2 ratio on the corrosion and erosion resistance of products is considered. The raw material should have a molar ratio of these oxides of more than 1,7. Pressed crucibles were tested in the production of nickel, cobalt and tin based alloys in a vacuum induction furnace. The parameters of operation of products in the enterprise are shown. The effect of clogging by crucible materials during smelting of pure nickel has also been studied. The absence of contamination of the melt with crucible materials such as silicon dioxide, aluminosilicates and oxide films, etc., has been established.


2019 ◽  
Vol 62 (4) ◽  
pp. 257-262
Author(s):  
A. I. Demchenko ◽  
E. N. Korzun ◽  
E. A. Chernyshov

The analysis of technological processes of smelting and casting of cylindrical bars from Inconel 718 alloy, obtained in a vacuum induction furnace at PJSC “Ruspolimet”, was performed. The existing technology does not ensure the production of a sound bar of the required quality due to the presence of porosity in the axial zone, and also due to liquation at the macro level of elements such as chromium, nickel, niobium. The results have shown the need to adjust the parameters of casting and solidification of bars from the Inconel 718 alloy. The task to get high-quality sound bar was set without changing the main technical parameters of production, namely: type of furnace – vacuum induction furnace with capacity of 3 tons; material of the furnace lining – ceramics based on aluminum oxide Al2O3 ; type of the casting mold – cylindrical mold for bar diameter of410 mm; diameter of crystallizer for vacuum-arc remelting –450 mm. With the use of the Thermo-Calc program (version 2017a), the solidus temperatures for the equilibrium solidification process and for the non-equilibrium process were clarified, which were 1211 °С and 1091 °С, respectively. Based on the results obtained, the casting speed (SCM LP) system corrects casting speed by reducing the diameter of the casting nozzle from 32 to28 mm and casting temperature by reducing it from 1470 to1460 °C. According to the corrected technology, a batch of bars has been smelted. From the bar of the first batch, transverse templates were selected to determine the chemical composition and longitudinal temp lates for metallographic analysis. Metallographic studies have been carried out that suggest a decrease in porosity of axial zone of the bar and a decrease in phase separation at the macro level. Based on the results obtained, the authors proposed to introduce approp riate changes in casting technology. It is shown that computer modeling of metallurgical processes of metal casting and crystallization allows developing a technology of obtaining a high-quality bar already at the first redistribution, while avoiding appearance of products that do not meet customer requirements.


2012 ◽  
Vol 476-478 ◽  
pp. 164-169
Author(s):  
Wei Xiang Wang ◽  
Zheng Liang Xue ◽  
Sheng Qiang Song ◽  
Ping Li ◽  
Zhi Chao Chen

The basic thermodynamic analysis of silicothermic reduction during direct alloying to smelting vanadium steel with V2O5 was discussed in this paper. The high-temperature carbon tube furnace and medium frequency vacuum induction furnace were used to study the phase compositions of the reduction products and the change law of the yield of vanadium when V2O5 was reduced by ferrosilicon. The research shows that the main phases of the silicothermic reduction products were VSi2、FeVO4 and Ca2SiO4 under the condition of using CaO to restrain the volatile of V2O5. Yield of vanadium was gradually improved with the increase of ferrosilicon during the direct alloying. The yield of vanadium in the steel is as high as 95.25% when the addition of ferrosilicon is 35%.


2014 ◽  
Vol 788 ◽  
pp. 158-163
Author(s):  
Bin Guo Fu ◽  
Hong Wei Wang ◽  
Chun Ming Zou ◽  
Pan Ma ◽  
Zun Jie Wei

A high temperature alloy Ti-1100 was produced by vacuum induction melting technology. The effects of casting modulus on the microstructure and hardness of the cast alloys were determined and the results were presented and briefly discussed. Results demonstrate that the microstructure of cast alloys with different modulus are all widmanstatten structure with basket weave features where individual α-laths are separated by a thin layer of retained prior β phase. The greater the modulus, the larger the prior β grain size and α-laths spacing, and the less the Vickers hardness. The roles of the casting modulus governing the microstructures and hardness of the alloys were also discussed.


Metals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1223 ◽  
Author(s):  
Frederic Brinkmann ◽  
Carolin Mazurek ◽  
Bernd Friedrich

Due to its enhancing properties in high-tech material applications, the rare earth element Scandium (Sc) is continuously gaining interest from researchers and material developers. The aim of this research is to establish an energy and resource efficient process scheme for an in situ extraction of Al-Sc master alloys, which offers usable products for the metallurgical industry. An AlSc20 alloy is targeted with an oxyfluoridic slag as a usable by-product. The thermochemical baseline is presented by modelling using the software tool FactSage; the experimental metal extraction is conducted in a vacuum induction furnace with various parameters, whereas kinetic aspects are investigated by thermogravimetric analysis. The Sc-containing products are analyzed by ICP-OES/IC concerning their chemical composition. Optimum parameters are derived from a statistical evaluation of the Sc content in the obtained slag phase. The material obtained was high in Ta due to the crucible material and remarkably low in Al and F; a comparison between the modelled and the obtained phases indicates kinetic effects inhibiting the accomplishment of equilibrium conditions. The formation of a Sc-rich Al-Sc phase (32.5 wt.-% Sc) is detected by SEM-EDS analysis of the metal phase. An in situ extraction of Al from Ca with subsequent metallothermic reduction of ScF 3 as a process controlling mechanism is presumed.


2010 ◽  
Vol 24 (15n16) ◽  
pp. 2940-2945 ◽  
Author(s):  
XIAOJIAN LI ◽  
HU ZHANG ◽  
JIANGBO SHA

This paper dealt with the effect of different induction melting technologies on mechanical properties of Nb -16 Si -22 Ti -2 Al -2 Hf -17 Cr alloy. The cast ingots were fabricated first by arc-melting, and then remolten in the vacuum induction furnace. The results showed that the ingot with refining process of 1800°C/15min and 0.1 at% C addition had finer microstructure and higher room-temperature fracture toughness. In addition, the compressive strength of the ingot with refining technology of 1700°C/10min was 315MPa at 1250°C. However, the arc melting ingot had the lowest fracture toughness and high-temperature compressive strength.


Author(s):  
June D. Kim

Iron-base alloys containing 8-11 wt.% Si, 4-8 wt.% Al, known as “Sendust” alloys, show excellent soft magnetic properties. These magnetic properties are strongly dependent on heat treatment conditions, especially on the quenching temperature following annealing. But little has been known about the microstructure and the Fe-Si-Al ternary phase diagram has not been established. In the present investigation, transmission electron microscopy (TEM) has been used to study the microstructure in a Sendust alloy as a function of temperature.An Fe-9.34 wt.% Si-5.34 wt.% Al (approximately Fe3Si0.6Al0.4) alloy was prepared by vacuum induction melting, and homogenized at 1,200°C for 5 hrs. Specimens were heat-treated in a vertical tube furnace in air, and the temperature was controlled to an accuracy of ±2°C. Thin foils for TEM observation were prepared by jet polishing using a mixture of perchloric acid 15% and acetic acid 85% at 10V and ∼13°C. Electron microscopy was performed using a Philips EM 301 microscope.


Alloy Digest ◽  
1987 ◽  
Vol 36 (1) ◽  

Abstract UDIMET 700 is a wrought nickel-base alloy produced by vacuum-induction melting and further refined by vacuum-arc remelting. It has excellent mechanical properties at high temperatures. Among its applications are blades for aircraft, marine and land-based gas turbines and rotor discs. This datasheet provides information on composition, physical properties, elasticity, and tensile properties as well as creep. It also includes information on high temperature performance and corrosion resistance as well as forming, heat treating, machining, joining, and surface treatment. Filing Code: Ni-51. Producer or source: Special Metals Corporation. Originally published March 1959, revised January 1987.


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