Improvement of physicomechanical properties of grafted coir fiber with ethyleneglycol dimethacrylate: effect of UV radiation

2012 ◽  
Vol 32 (2) ◽  
Author(s):  
Haydar U. Zaman ◽  
Mubarak A. Khan ◽  
Ruhul A. Khan
Keyword(s):  
Monomer Concentration ◽  
Curing Temperature ◽  
Coir Fiber ◽  
Curing Time ◽  
Thermal Curing ◽  
Optimum Conditions ◽  
Coir Fibers ◽  
Different Temperatures ◽  
Curing Method ◽  
Different Doses

Abstract Coir fibers were modified with ethyleneglycol dimethacrylate (EGDMA)+MeOH solutions under thermal curing method at different temperatures (50°C–90°C) and curing times (30–70 min). Monomer concentration, curing temperature, and curing time were optimized in terms of grafting and mechanical properties, and 50% EGDMA, 70°C and 50 min curing time, respectively, registered better performance. Coir fibers were pretreated with ultraviolet radiation at different doses, soaked in optimized solution, and cured under optimum conditions. These fibers showed improved properties than EGDMA-treated fibers. Water uptake and simulated weathering test of untreated and treated fibers were studied.

scholarly journals Lamination Curing Method for Inkjet Printed Flexible Angle Sensors

2021 ◽  
Author(s):  
Dila Türkmen ◽  
Merve Acer Kalafat
Keyword(s):  
Sheet Resistance ◽  
Single Layer ◽  
Time Dependent ◽  
Curing Time ◽  
Thermal Curing ◽  
Curing Methods ◽  
Curing Method ◽  
Lower Sheet Resistance ◽  
Sensing Performance ◽  
Pet Substrate

In this paper we present the lamination curing as a stand-alone method to activate the silver nanoparticle (Ag NP) inkjet printed angle sensors on a 0.14 mm PET substrate, with a desktop printer. (With the term “lamination curing”, we refer passing the printed sample through a lamination machine, without any actual laminating purpose, only for curing.) We compared the method with the oven curing, which is the widest used method for the intended sensors, and found that lamination cured sensors give lower sheet resistance, lower fabrication uncertainty and more consistent angle sensing behaviors with higher sensing performance. Different curing parameters are inspected and a process under 3 minutes is achieved giving a 0.06 Ohm/square sheet resistance. For such a low sheet resistance, presented method has the lowest thermal curing time among all single layer Ag NP printing studies in the literature. An experimental model is presented for the sheet resistance - aspect ratio relation for both methods. Time dependent resistance shifts of the lamination cured sensors are also inspected and proved to be insignificant. We state lamination curing as an advantageous and reliable alternative to oven curing and other fast curing methods both for sensor and circuitry printing implementations.

scholarly journals Lamination Curing Method for Inkjet Printed Flexible Angle Sensors

2021 ◽  
Author(s):  
Dila Türkmen ◽  
Merve Acer Kalafat
Keyword(s):  
Sheet Resistance ◽  
Single Layer ◽  
Time Dependent ◽  
Curing Time ◽  
Thermal Curing ◽  
Curing Methods ◽  
Curing Method ◽  
Lower Sheet Resistance ◽  
Sensing Performance ◽  
Pet Substrate

In this paper we present the lamination curing as a stand-alone method to activate the silver nanoparticle (Ag NP) inkjet printed angle sensors on a 0.14 mm PET substrate, with a desktop printer. (With the term “lamination curing”, we refer passing the printed sample through a lamination machine, without any actual laminating purpose, only for curing.) We compared the method with the oven curing, which is the widest used method for the intended sensors, and found that lamination cured sensors give lower sheet resistance, lower fabrication uncertainty and more consistent angle sensing behaviors with higher sensing performance. Different curing parameters are inspected and a process under 3 minutes is achieved giving a 0.06 Ohm/square sheet resistance. For such a low sheet resistance, presented method has the lowest thermal curing time among all single layer Ag NP printing studies in the literature. An experimental model is presented for the sheet resistance - aspect ratio relation for both methods. Time dependent resistance shifts of the lamination cured sensors are also inspected and proved to be insignificant. We state lamination curing as an advantageous and reliable alternative to oven curing and other fast curing methods both for sensor and circuitry printing implementations.

scholarly journals INFLUENCE OF SYNTHESIS FACTORS ON PROPERTIES OF GEOPOLYMERS BASED ON RED MUD AND RICE HUSK ASH

2017 ◽  
Vol 55 (4) ◽  
pp. 461
Author(s):  
Tran Ngoc Tuyen ◽  
Nguyen Duc Vu Quyen ◽  
Ho Van Minh Hai ◽  
Dang Xuan Tin ◽  
Tran Ngoc Quang
Keyword(s):  
Compressive Strength ◽  
Rice Husk ◽  
Red Mud ◽  
Rice Husk Ash ◽  
Raw Materials ◽  
Curing Temperature ◽  
Mixing Ratio ◽  
Curing Time ◽  
Optimum Conditions ◽  
Total Shrinkage

In this paper, the effect of mixing ratio of raw materials, curing temperature and time on geopolymerization between red mud and rice husk ash were investigated. The results showed that the optimum conditions were SiO2/Al2O3 ratio of 4 and Na2O/Al2O3 ratio of 2.0, curing temperature of 100oC and curing time of 24 hours. The compressive strength, bulk density, total shrinkage of the obtained product were 22.8 MPa, 2.39 g.cm-3, 15%, respectively that met requirement of unsintered bricks using for construction.

SINTESIS DAN MODIFIKASI STRUKTUR DAN PORI MEMBRAN KITOSAN TERCROSSLINK UNTUK STERILISASI MEDIA PERTUMBUHAN BAKTERI

2019 ◽  
Vol 3 (2) ◽  
pp. 27
Author(s):  
Emma Savitri ◽  
Natalia Suseno ◽  
Tokok Adiarto
Keyword(s):  
Tensile Strength ◽  
Chitosan Solution ◽  
Curing Temperature ◽  
Growth Media ◽  
Optimum Conditions ◽  
Separation Processes ◽  
Crosslinking Process ◽  
Chitosan Membrane ◽  
Chitosan Membranes ◽  
Crosslinked Chitosan

Many mass-transfer applications have used chitosan membrane in separation processes. This research applied crosslinked chitosan membrane to sterillize bacterial growth media. Chitosan membranes having 79 % DD were produced by casting and drying chitosan solution. The images of the membrane were characterized by SEM and other characterizations such as permeability, permselectivity and tensile strength were investigated. The flux increased with longer submersion period but the rejection decreased. Otherwise, the flux decreased and rejection increased in line with an increase in curing temperature. Tensile strength increased with the increase of submersion period and curing temperature. The optimum conditions of crosslinking process are 2 hours of submersion periods and curing temperature at 90 oC.  It gives flux 5.8930 L/jam.m2, rejection 97.47 % and tensile strength 49640 kN/m2

scholarly journals Coir Fibers Treated with Henna as a Potential Reinforcing Filler in the Synthesis of Polyurethane Composites

Materials ◽  
2021 ◽  
Vol 14 (5) ◽  
pp. 1128
Author(s):  
Sylwia Członka ◽  
Anna Strąkowska ◽  
Agnė Kairytė
Keyword(s):  
Mechanical Properties ◽  
High Energy ◽  
Dynamic Mechanical Properties ◽  
Milling Process ◽  
Coir Fiber ◽  
Lawsonia Inermis ◽  
Coir Fibers ◽  
Mechanical Performances ◽  
The Impact ◽  
Reinforcing Filler

In this study, coir fibers were successfully modified with henna (derived from the Lawsonia inermis plant) using a high-energy ball-milling process. In the next step, such developed filler was used as a reinforcing filler in the production of rigid polyurethane (PUR) foams. The impact of 1, 2, and 5 wt % of coir-fiber filler on structural and physico-mechanical properties was evaluated. Among all modified series of PUR composites, the greatest improvement in physico-mechanical performances was observed for PUR composites reinforced with 1 wt % of the coir-fiber filler. For example, on the addition of 1 wt % of coir-fiber filler, the compression strength was improved by 23%, while the flexural strength increased by 9%. Similar dependence was observed in the case of dynamic-mechanical properties—on the addition of 1 wt % of the filler, the value of glass transition temperature increased from 149 °C to 178 °C, while the value of storage modulus increased by ~80%. It was found that PUR composites reinforced with coir-fiber filler were characterized by better mechanical performances after the UV-aging.

Characterization and Utilization of Coconut Fibers of the Caribbean

2014 ◽  
Vol 1611 ◽  
pp. 95-104 ◽  
Author(s):  
Nadira Mathura ◽  
Duncan Cree ◽  
Ryan P. Mulligan
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Electron Micrographs ◽  
Saline Water ◽  
Gauge Length ◽  
Scanning Electron Micrographs ◽  
Coir Fiber ◽  
Coir Fibers ◽  
The Caribbean ◽  
Scanning Electron

ABSTRACTIn many tropical countries coconut (coir) fiber production is a major source of income for rural communities. The Caribbean has an abundance of coconuts but research into utilizing its by-products is limited. Environmentally friendly coir fibers are natural polymers generally discarded as waste material in this region. Research has shown that coir fiber from other parts of the world has successfully been recycled. This paper therefore investigates the mechanical properties of Caribbean coir fiber for potential applications in civil engineering.Approximately four hundred fibers were randomly taken from a coir fiber stack and subjected to retting in both distilled and saline water media. The mechanical properties of both the retted and unretted coir fibers were evaluated at weekly increments for a period of 3 months. Tensile strength test, x-ray diffraction analysis and scanning electron micrographs were used to assess trends and relationships between fiber gauge lengths, diameter, tensile strength and Young’s modulus. Diameters ranged between 0.11 mm-0.46 mm, while fiber samples were no longer than 250 mm in length. The tensile strength and strain at break decreased as the gauge length increased for both unretted and retted fibers. The opposite occurred for the relationship between the gauge length and Young’s modulus. Additionally, the tensile strength and modulus decreased as the fiber diameter increased. Neither distilled nor saline water improved the coir fiber’s crystalline index. Scanning electron micrographs qualitatively assessed fiber surfaces and captured necking and microfibril degradation at the fractured ends.The analysis revealed that the tensile strength, modulus, strain at break and crystallinity properties of the Caribbean coir fibers were comparable to commercially available coir fiber which are currently being used in many building applications.

scholarly journals A Modified Photoactivation Protocol Using Two Simultaneous Light-Curing Units for Bonding Brackets to Enamel

2015 ◽  
Vol 26 (4) ◽  
pp. 393-397 ◽  
Author(s):  
Adauê Siegert de Oliveira ◽  
Rafael Correa Mirapalhete ◽  
Cássia Cardozo Amaral ◽  
Rafael Ratto de Moraes
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Curing Time ◽  
Thermal Cycles ◽  
Adhesive Remnant Index ◽  
Light Curing ◽  
Standard Deviations ◽  
Curing Method

<p>This study investigated the effect of a modified photoactivation protocol using two simultaneous light-curing units on the shear bond strength (SBS) of brackets to enamel. Metal brackets were bonded to bovine incisors using the resin-based orthodontic cement Transbond XT (3M Unitek). Four photoactivation protocols of the orthodontic cement were tested (n=15): Control: photoactivation for 10 s on each proximal face of the bracket at a time; Simultaneous: photoactivation for 10 s on both proximal faces of the bracket at the same time; One side-20s: photoactivation for 20 s at one proximal face of the bracket only; and One side-10s: photoactivation for 10 s only at one proximal face of the bracket. SBS was tested immediately or after 1000 thermal cycles. Adhesive remnant index (ARI) was classified. Data were subjected to two-way ANOVA and Student-Newman-Keuls' test (α=0.05). Pooled means ± standard deviations for SBS to enamel (MPa) were: 10.2±4.2 (Control), 9.7±4.5 (Simultaneous), 5.6±3.1 (One side-20s), and 4.6±1.9 (One side-10s). Pooled SBS data for immediate and thermal cycled groups were 6.3±2.6 and 8.8±5.2. A predominance of ARI scores 1-2 and 0-1 was observed for the immediate and thermally cycled groups, respectively. In conclusion, simultaneous photoactivation of the orthodontic cement using two light-curing units, one positioned at each proximal face of the bracket, yielded similar bonding ability compared to the conventional light-curing method. Photoactivation of the orthodontic cement at one proximal face of the bracket only is not recommended, irrespective of the light-curing time used.</p>

scholarly journals Synthesis of Geopolymer from Inorganic Construction Waste

2013 ◽  
Vol 30 ◽  
pp. 45-51 ◽  
Author(s):  
Arbind Pathak ◽  
Vinay Kumar Jha
Keyword(s):  
Compressive Strength ◽  
Coal Fly Ash ◽  
Chemical Society ◽  
Raw Material ◽  
Curing Temperature ◽  
Alkali Concentration ◽  
Curing Time ◽  
Mass Ratio ◽  
Construction Waste ◽  
Alumino Silicate

Recently, the demolition of old houses and the construction of new buildings in Kathmandu valley are in the peak which in turn generates a huge amount of construction waste. There are two major types of construction wastes which are burden for disposal namely cement-sand-waste (CSW) and the coal fly ash (CFA). These construction wastes are rich source of alumino-silicate and thus used as raw material for the synthesis of geopolymer in this study. Geopolymers have been synthesized from CSW and CFA using NaOH-KOH and Na2SiO3 as activators. Some parameters like alkali concentration, amount of Na2SiO3 and curing time have been varied in order to improve the quality of geopolymeric product. The geopolymerization process has been carried out using 3-8M KOH/NaOH solutions, Na2SiO3 to CFA and CSW mass ratio of 0.25-2.00 and curing time variation from 5-28 days. The curing temperature was fixed at 40ºC in all the cases. 6M NaOH and 7M KOH solutions were found appropriate alkali concentrations while the ratio of sodium silicate to CSW and CFA of 0.5 and 1.75 respectively were found suitable mass ratio for the process of geopolymer synthesis. The maximum compressive strength of only 7.3 MPa after 15 days curing time with CSW raw material was achieved while with CFA, the compressive strength was found to be 41.9 MPa with increasing the curing time up to 28 days.DOI: http://dx.doi.org/10.3126/jncs.v30i0.9334Journal of Nepal Chemical Society Vol. 30, 2012 Page:  45-51 Uploaded date: 12/16/2013    

scholarly journals Optimum Multilayer-Graphene-Montmorillonite Composites From Sugar for Thermosolar Coatings Formulations

2017 ◽  
Vol 139 (3) ◽  
Author(s):  
Bàrbara Micó-Vicent ◽  
María López ◽  
Azucena Bello ◽  
Noelia Martínez ◽  
Francisco Martínez-Verdú
Keyword(s):  
Working Conditions ◽  
Low Cost ◽  
Multilayer Graphene ◽  
Optimum Conditions ◽  
Laminar Structure ◽  
Solar Absorptance ◽  
Solar Plant ◽  
Different Temperatures ◽  
Complex Deposition ◽  
Deposition Techniques

Solar thermal coatings are designed to achieve the highest incident solar flux into the receiver of a tower solar plant. These materials are subjected to extreme working conditions of temperature and solar concentrated radiation. Much effort is being made to develop a durable and high absorptive coating that can provide an excellent solar to heat conversion efficiency. Complex deposition techniques (PVD, CVD, electrodeposition, etc.) are developed and tested to achieve solar selectivity. High solar absorptance paints are an alternative technique, that is, easy to apply and implement in the field. In paint, pigments are the compound that provides high absorptance values, whose stability impacts the durability of optical properties. The search for new selective solar pigments for solar receivers is a promising route to improve the efficiency of this technology. In this work, novel nanocomposites were synthesized from low-cost organic materials such as table sugar. Promising results were obtained when intercalated and calcined in the laminar structure of montmorillonite, a type of smectite clay. The pigments were tested in a paint format on metallic coupons at different temperatures to obtain absorptivities above 96% of absorptance after 24 h at 700  °C. Further experiments are still needed to obtain optimum conditions to maximize the coating's absorptivity and durability at high temperature.

Effect of Adhesive Thickness on the Impact Toughness of Butt-Joints

2011 ◽  
Vol 230-232 ◽  
pp. 1350-1354 ◽  
Author(s):  
Min You ◽  
Jing Rong Hu ◽  
Xiao Ling Zheng ◽  
Ai Ping He ◽  
Cun Jun Chen
Keyword(s):  
Impact Toughness ◽  
Adhesive Layer ◽  
Curing Temperature ◽  
Curing Time ◽  
Optimum Thickness ◽  
Adhesively Bonded ◽  
Butt Joints ◽  
Notched Specimen ◽  
Adhesive Thickness ◽  
The Impact

The effect of the adhesive thickness on the impact toughness of the adhesively bonded steel joint under impact loading is studied using the experimental method. The results obtained show that the impact toughness increases when the adhesive thickness increased then it decrease as the adhesive thickness increase. When the curing time is set as a constant, the higher the curing temperature is, the lower the impact toughness of the joint. The optimum thickness of the adhesive layer for the specimen of impact toughness test cured at 60 C for 1 h is 0.6 mm and it is 0.4 mm to 0.6 mm for the specimen cured 1 h at temperature of 90 C or higher than it. It is recommended using the notched specimen to decrease the testing deviation.

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