Synthesis of Pt Nanoparticles and Nanorods by Microwave-assisted Solvothermal Technique

2006 ◽  
Vol 61 (12) ◽  
pp. 1566-1572 ◽  
Author(s):  
Dongsheng Li ◽  
Sridhar Komarneni
Keyword(s):  
Particle Size ◽  
Pt Nanoparticles ◽  
Transmission Electron Microscopy Image ◽  
Molar Ratio ◽  
Reaction Conditions ◽  
Microwave Assisted ◽  
Metal Sources ◽  
Transmission Electron ◽  
Particle Size And Morphology ◽  
Size And Morphology

Platinum nanoparticles and nanorods were synthesized by microwave-assisted solvothermal techniques. Changing the reaction conditions controlled particle size and morphology. The effects of the reaction conditions, such as the molar ratio of the polyvinylpyrrolidone (PVP) repeating unit to the metal sources, the concentration of metal sources, the reaction temperature, and the presence of distilled water were investigated. Nanoparticles of Pt were approximately 3 nm in size. Produced nanoparticles and nanorods were characterized by transmission electron microscopy. Image JTM software was used to calculate the particle size and size distribution.

Nanoparticles of Pd: Synthesis by Microwave-Solvothermal Method and Optical Properties

2008 ◽  
Vol 8 (8) ◽  
pp. 3930-3935 ◽  
Author(s):  
Dongsheng Li ◽  
Sridhar Komarneni
Keyword(s):  
Particle Size ◽  
Optical Properties ◽  
Pd Nanoparticles ◽  
Absorption Bands ◽  
Reaction Conditions ◽  
Transmission Electron ◽  
Vis Spectroscopy ◽  
Particle Size And Morphology ◽  
Particle Size And Shape ◽  
Size And Morphology

Well-dispersed Pd nanoparticles were synthesized by microwave-assisted solvothermal technique using methanol and ethanol. Particle size and morphology were controlled mainly by the reaction temperature. Particle size of Pd nanoparticles was controlled in the range of 2 to 11 nm by manipulating the reaction conditions. The Pd nanoparticles were characterized by transmission electron microscopy for particle size and shape and UV-Vis spectroscopy for optical properties. UV-Vis spectra showed that synthesized Pd nanoparticles stabilized with PVP had absorption bands at around 280 to 290 nm.

scholarly journals Colloidal Probes of PNIPAM-Grafted SiO2 in Studying the Microrheology of Thermally Sensitive Microgel Suspensions

2020 ◽  
Vol 2020 ◽  
pp. 1-9
Author(s):  
Jing Shang ◽  
Ruonan Gao ◽  
Fu Su ◽  
Huaguang Wang ◽  
Dan Zhu
Keyword(s):  
Phase Transition ◽  
Particle Size ◽  
Depletion Effect ◽  
Transmission Electron ◽  
Particle Size And Morphology ◽  
Complex Rheology ◽  
Colloidal Probes ◽  
Size And Morphology ◽  
Collapsed States ◽  
Good Probe

The complex rheology and the phase behavior of thermally sensitive poly(N-isopropylacrylamide) (PNIPAM) microgels have been investigated in both the swollen and collapsed states by using microrheology. To avoid the interactions between the tracer probes and the PNIPAM microgels, such as the adsorption or the depletion effect, the probes of silica (SiO2) particles have been grafted with PNIPAM chains (SiO2-PNIPAM) and characterized with Fourier transform infrared spectroscopy (FTIR). The successful preparation of SiO2-PNIPAM has also been proved by the investigation of the particle size and morphology with dynamic light scattering (DLS) and transmission electron microscope (TEM) below and beyond the phase transition temperature of PNIPAM. The microrheology of the PNIPAM microgel suspension has been investigated by using the prepared SiO2-PNIPAM particles as microrheological probes, and the results show that the diffusive coefficient of the probes in the swollen state is one-fifth of that in the collapsed state, and the viscosity of the PNIPAM microgel suspension in the swollen state is four times higher than that in the collapsed state, indicating SiO2-PNIPAM is a good probe in the microrheological study of PNIPAM microgel suspensions.

Synthesis of Calcium Carbonate from Calcium Chlorine Solution Using Homogeneous Precipitation Method

2005 ◽  
Vol 486-487 ◽  
pp. 542-545 ◽  
Author(s):  
Kyung Nam Kim ◽  
Dae Yong Shin ◽  
Se Gu Son ◽  
Yong Do Kim
Keyword(s):  
Particle Size ◽  
Calcium Carbonate ◽  
Precipitation Method ◽  
Homogeneous Precipitation ◽  
Reaction Conditions ◽  
Homogeneous Precipitation Method ◽  
Reaction Solution ◽  
Particle Size And Morphology ◽  
Size And Morphology ◽  
Hydrolysis Of

Calcium carbonate(CaCO3) was synthesized from aqueous CaCl2 solution, using the homogeneous precipitation technique, which uses the hydrolysis of urea. The effects of reaction conditions on the morphology of CaCO3 were examined at 50-90°C. Particle size of CaCO3 decreases, as the concentrations of urea and [Ca2+] are increased. Calcite is produced more, as the concentration of [Ca2+] is increased. Method to stir the reaction solution affects significantly the particle size and morphology of CaCO3. Uniform needle-like aragonite particles were obtained, when left at 90°C for 4hours without stirring.

Effect of Carbon Source Content on the Carbothermal Synthesis of AlN Powders Using a Combustion Synthesis Precursor

2012 ◽  
Vol 554-556 ◽  
pp. 526-531
Author(s):  
Ai Min Chu ◽  
Ming Li Qin ◽  
Bao Rui Jia ◽  
Hui Feng Lu
Keyword(s):  
Particle Size ◽  
Carbon Source ◽  
Combustion Synthesis ◽  
Aluminum Nitrate ◽  
Spherical Particles ◽  
Molar Ratio ◽  
Mixed Solution ◽  
Particle Size And Morphology ◽  
Size And Morphology ◽  
Average Size

AlN powders were synthesized by carbothermal reduction method using a combustion synthesis precursor derived from aluminum nitrate (oxidizer), glucose (carbon source), and urea (fuel) mixed solution. Effects of carbon source content on the combustion temperature of solutions, the particle size and morphology of the precursors and the synthesized AlN were studied in detail. The results indicated that a regular variation in the particle size and morphology of precursors had been observed with the increasing molar ratio of glucose to aluminum nitrate (C/Al). The products prepared with (C/Al=8–12), calcined at 1500 oC for 2 h, could have completed the nitridation reaction, while the nitridation products prepared with (C/Al=4 and 16) are opposite. The nitridation products prepared with (C/Al=8–12), calcined at 1500 oC for 2 h, are comprised of well-distributed spherical particles of AlN with the average size ranging from 50 to 80 nm.

Preparation and Characterization of Ag, Au and Ti Metal Nanoparticles Colloids by Pulsed Laser Ablation in Liquids

2011 ◽  
Vol 415-417 ◽  
pp. 648-651 ◽  
Author(s):  
Bing Xu ◽  
Ren Guo Song ◽  
Chao Wang
Keyword(s):  
Particle Size ◽  
Laser Ablation ◽  
Metal Nanoparticles ◽  
Pulsed Laser ◽  
Pulsed Laser Ablation ◽  
Average Diameter ◽  
Transmission Electron ◽  
Particle Size And Morphology ◽  
Size And Morphology

Ag, Au and Ti metal nanoparticles colloids have been prepared by pulsed laser ablation in various liquids. The particle size and morphology of the obtained nanoparticles colloids were characterized by transmission electron microscopy (TEM), the average diameter and its distribution were analyzed by Image-ProPlus software. The results showed that the Au nanoparticles were of the best characterization, the average diameter was the smallest (D=8.79 nm), and also, the distribution of particle size was the narrowest (=17.5 nm) and the morphologies were more homogeneous.

Direct manipulation of particle size and morphology of ordered mesoporous silica by flow synthesis

RSC Advances ◽  
2015 ◽  
Vol 5 (18) ◽  
pp. 13331-13340 ◽  
Author(s):  
T. N. Ng ◽  
X. Q. Chen ◽  
K. L. Yeung
Keyword(s):  
Particle Size ◽  
Mesoporous Silica ◽  
Hollow Spheres ◽  
Ordered Mesoporous Silica ◽  
Direct Manipulation ◽  
Flow Synthesis ◽  
Precise Control ◽  
Ordered Mesoporous ◽  
Particle Size And Morphology ◽  
Size And Morphology

Flow-synthesis of mesoporous silica allows deliberate and precise control over the size and shapes and enables the preparation of complex microstructures (i.e., hollow spheres).

scholarly journals Dehumidified Air-Assisted Spray-Drying of Cloudy Beetroot Juice at Low Temperature

2021 ◽  
Vol 11 (14) ◽  
pp. 6578
Author(s):  
Aleksandra Jedlińska ◽  
Alicja Barańska ◽  
Dorota Witrowa-Rajchert ◽  
Ewa Ostrowska-Ligęza ◽  
Katarzyna Samborska
Keyword(s):  
Particle Size ◽  
Physicochemical Properties ◽  
Spray Drying ◽  
Low Temperatures ◽  
Beetroot Juice ◽  
Particle Size And Morphology ◽  
Size And Morphology ◽  
Tapped Density ◽  
Lower Loss ◽  
Better Than

This paper discusses the physicochemical properties of powders obtained by spray drying of cloudy beetroot juice, using dehumidified air in variants with or without carriers. The inlet air temperature was 130 °C or 90 °C, and the addition of the carriers was at a ratio of juice to carrier solids of 3:2. In the obtained powders, the following physicochemical properties were determined: water content and water activity, apparent density, loose and tapped density, porosity, flowability, particle size and morphology, and the content and retention of betalains. It was possible to dry cloudy beetroot juice without the use of carriers at low temperatures (90 or 130 °C). The 100% beetroot powders were characterized by satisfactory physicochemical properties, often better than those with carriers (including lower hygroscopicity and higher color saturation and yield). A lower loss of betalains was found for the powders with the addition of carriers. The best process yields were obtained for the powder without carriers at 130 °C and 90 °C.

Synthesis and Characterization of Calcium Tartrate Dihydrate Nanoparticles

2015 ◽  
Vol 14 (04) ◽  
pp. 1550013 ◽  
Author(s):  
Urvisha Tarpara ◽  
Poorvesh Vyas ◽  
Mihir J. Joshi
Keyword(s):  
Average Crystallite Size ◽  
Powder Xrd ◽  
Xrd Pattern ◽  
Crystalline Materials ◽  
Transmission Electron ◽  
Calcium Tartrate ◽  
Particle Size And Morphology ◽  
Wet Chemical ◽  
Size And Morphology

Calcium tartrate finds various applications. In the present study, calcium tartrate nanoparticles were synthesized by wet chemical method using surfactant mediated approach. The powder XRD pattern revealed the typical broadening of peaks indicating the nanostructured nature. The average crystallite size was calculated by applying the Scherrer's formula to powder XRD pattern and was found in the range of 22.8–23.9 nm. The particle size and morphology of the synthesized nanoparticles was confirmed by using transmission electron microscopy (TEM). FTIR spectroscopy was used to confirm the presence of various functional groups. From TGA, it was found that calcium tartrate nanoparticles remained stable up to 120°C and were having two water molecules associated with them. The results are compared with the bulk crystalline materials available in the literature.

Synthesis and Properties of (Bi0.5Na0.5)TiO3 Powders by Hydrothermal Method

2007 ◽  
Vol 336-338 ◽  
pp. 140-142
Author(s):  
Jun Jie Hao ◽  
Xiao Hui Wang ◽  
Shi Yun Lin ◽  
Long Tu Li
Keyword(s):  
Particle Size ◽  
Hydrothermal Method ◽  
Single Phase ◽  
Piezoelectric Ceramics ◽  
Treatment Temperature ◽  
Lead Free ◽  
Excellent Candidate ◽  
Traditionally Prepared ◽  
Particle Size And Morphology ◽  
Size And Morphology

Na0.5Bi0.5TiO3 (NBT) is considered to be an excellent candidate for lead-free piezoelectric ceramics. In this study, we propose a hydrothermal method for the preparation of single phase NBT powder at relatively low treatment-temperature. The particle size and morphology of the synthesized powders were examined by SEM. The powders were further pressed into disk and sintered at 1120°C/2h in air, and its properties and microstructure were compared with traditionally prepared samples.

Sign in / Sign up

Export Citation Format

Share Document