Mechanical properties of AZ31 Mg alloy recycled by severe deformation

2006 ◽  
Vol 21 (3) ◽  
pp. 754-760 ◽  
Author(s):  
Yasumasa Chino ◽  
Tetsuji Hoshika ◽  
Jae-Seol Lee ◽  
Mamoru Mabuchi

AZ31 Mg machined chips were recycled by extrusion at 673 K with a low extrusion ratio of 45:1 and a high extrusion ratio of 1600:1. Oxide contaminants were dispersed more uniformly in the recycled specimen with the high extrusion ratio than in that with the low extrusion ratio. In tensile tests, the recycled specimens with the high extrusion ratio showed about 50% higher 0.2% yield stress and about 20% higher tensile strength compared with those of the reference specimens, which were the extruded AZ31 Mg blocks under the same conditions as the recycled specimens. The improvement of the tensile properties was attributed not only to the small grain size, but also to the dispersed oxide contaminants.

2010 ◽  
Vol 139-141 ◽  
pp. 180-184
Author(s):  
Yong Xue ◽  
Zhi Min Zhang ◽  
Li Hui Lang

In the present research, the influences of different extrusion ratios (15, 30, 45, 60, and 75) and extrusion temperatures (300°C, 330°C, 360°C, 390°C, 420°C) on the mechanical properties and microstructure of homogenized AZ80 alloy have been investigated through the tensile tests and via metallographic microscope observation. The results show that the alloy’s grain is small and small amounts of black hard and brittle second-phase β (Mg17Al12) are precipitated uniformly along the grain boundary causing the gradual increase of the alloy’s tensile strength at 330°C. When the extrusion temperature is up to 390°C, the grain size increases significantly, but the second phase precipitation along grain boundaries transforms into continuous and uniform-distribution precipitation within the grain. In this case, when the extrusion ratio is 60, the alloy’s tensile strength reaches its peak 390Mpa. As the extrusion temperature increases, inhomogeneous precipitation of the second-phase along grain boundaries increases, causing the decrease of the alloy’s strength. At the same temperature, the tensile strength increases firstly and then decreases as extrusion ratio increases. With the gradual increase of the refinement grain, the dispersed precipitates increase and the alloy’s tensile strength and plasticity reach their peaks when the extrusion temperature is 390°C. As the grain grows, the second phase becomes inhomogeneous distribution, and the alloy’s strength and plasticity gradually decrease.


2011 ◽  
Vol 299-300 ◽  
pp. 460-465 ◽  
Author(s):  
Li Zhang ◽  
Xiu Ping Dong ◽  
Hao Chen

By designing different formulations of composites and adopting optimized technology including extrusion and molding, the different composites with various content microcapsules were prepared. The results of the tensile tests show that with the increasing content of self-healing microcapsules in the glass fiber reinforced nylon composites, the mechanical properties of the composites will change, i.e. tensile strength, elastic modulus will decrease. But there is little effect on the mechanical properties of the composite gears if the content of self-healing microcapsules is less than 3.5%, and the technology of self-healing microcapsules used in the polymer composite gear is feasible.


Author(s):  
Matteo Benedetti ◽  
Cinzia Menapace ◽  
Vigilio Fontanari ◽  
Ciro Santus

The present paper investigates the variability in the static and cyclic properties of two nominally identical supplies of the aeronautical Al grade 7075-T6. Samples were extracted from extruded bars of 15 mm and 60 mm diameter and with slightly different chemical composition. Noticeable differences were found in tensile strength, total elongation, low- and high-cycle fatigue strength, despite the nearly identical hardness value. The diverse mechanical behavior has been imputed to different extrusion ratio and therefore work hardening along with a more or less fine distribution of precipitates and dispersoids. The high-cycle fatigue strength was found to be in direct correlation with the monotonic yield strength and the size of the largest intermetallic precipitate. A simple equation based on Murakami sqrt(area) parameter is proposed to predict the fatigue endurance. Tensile tests and microstructural analyses are recommended instead of conventional hardness tests to have a tighter quality control on the mechanical properties of semifinished products.


2010 ◽  
Vol 148-149 ◽  
pp. 332-337 ◽  
Author(s):  
Yong Xue ◽  
Zhi Min Zhang ◽  
Li Hui Lang

In the present research, the influences of different extrusion ratios (15, 30, 45, 60, and 75), extrusion temperatures (300 , 340 , 380 , 420 , and 460 ), and subsequent heat treatment on the mechanical properties and microstructure of as-cast ZK60 magnesium alloy have been investigated through the tensile tests and via metallographic observation. The results show that forward extrusion process can refine the microstructure of as-cast ZK60 alloy effectively. If as-cast ZK60 alloys have been extruded with the extrusion ratio 45 at 380 ,420 and 460 , respectively, and then post-heat treatment was conducted, the ZK60 alloy’s strength is higher under T5 than T6 treatment. For as-cast ZK60 alloy processed by extrusion and T5 method, the most appropriate temperature for extrusion processing is 300 , at which its tensile strength are highest provided the extrusion ratio is 30 but yet its plasticity is best provided the extrusion ratio is 45. If forward extrusions were conducted at 380 , mechanical properties of ZK60 alloy have little difference as the extrusion ratio varies. When T6 treatment was conducted for the extruded bars, their mechanical properties were improved little, moreover, the bigger the extrusion ratio is, the higher the tensile strength and elongation of the extruded bars become.


2017 ◽  
Vol 17 (4) ◽  
pp. 179-184
Author(s):  
Xuesong Fu ◽  
Yan Yang ◽  
QuanYang Ma ◽  
Xiaodong Peng ◽  
Tiancai Xu

AbstractMg-0.5Si-xSn (x=0.95, 2.9, 5.02wt.%) alloys were cast and extruded at 593K (320oC) with an extrusion ratio of 25. The microstructure and mechanical properties of as-cast and extruded test alloys were investigated by OM, SEM, XRD and tensile tests. The experimental results indicate that the microstructure of the Mg-0.5Si-xSn alloys consists of primary α-Mg dendrites and an interdendritic eutectic containing α-Mg, Mg2Si and Mg2Sn. There is no coarse primary Mg2Si phase in the test alloys due to low Si content. With the increase in the Sn content, the Mg2Si phase was refined. The shape of Mg2Si phase was changed from branch to short bar, and the size of them were reduced. The ultimate tensile strength and yield strength of Mg-0.52Si-2.9Sn alloy at the temperature of 473K (200oC) reach 133MPa and 112MPa respectively. Refined eutectic Mg2Si phase and dispersed Mg2Sn phase with good elevated temperature stability are beneficial to improve the elevated temperature performance of the alloys. However, with the excess addition of Sn, large block-like Mg2Sn appears around the grain boundary leading to lower mechanical properties.


2006 ◽  
Vol 519-521 ◽  
pp. 1479-1484 ◽  
Author(s):  
Hiroki Adachi ◽  
Kozo Osamura ◽  
Jun Kusui ◽  
Shigeru Okaniwa

The effect of extrusion rate and ratio on the Al3Zr induced dynamic recrystallization (DRX) that occurs during hot extrusion of RS-P/M Al-Zn-Mg-Cu-Zr alloys was investigated. An increase in the logarithm of extrusion rate promoted DRX and lead to a monotonic increase in the number of fine grains. Although DRX was also promoted and the grain size reduced by an increase in extrusion ratio from 10 to 20, the DRX behavior hardly changed, even when the extrusion ratio exceeded 20. However, with increasing extrusion ratio, the width of fibrous grain, i.e., the unrecrystallized region, decreased and the tensile strength increased to 879 MPa. When the extrusion rate and ratio exceeded 54 mm/min and 20, respectively, a marked grain coarsening occurred upon solution treatment, and the tensile strength tended to decrease, because of the high dislocation density induced by hot extrusion. By annealing at 563 K before solution treatment, it was possible to prevent grain coarsening, and thus prevent the strength decrease.


2014 ◽  
Vol 540 ◽  
pp. 356-359
Author(s):  
Hui Du ◽  
Zun Jie Wei

As-cast Mg-2Zn-1Mn-xCa (x=0.5 and 1.5 wt.%) alloys are extruded a 553K with an extrusion ratio of 11.3:1 as biomedical materials. The microstructures of the extruded Mg-2Zn-1Mn-xCa alloys are investigated. Microstructures show that the dynamic recrystallization (DRX) occurs after the extruded process. The grain size of the extruded Mg-2Zn-1Mn-1.5Ca alloy is significantly refined compared to that of Mg-2Zn-1Mn-0.5Ca alloy. The tensile strength increases and the elongation decreases with an increase of Ca content. The improvement of tensile strength can be attibuted to the pesence of Mg2Ca phase. However, Mg2Ca phase is bristle, which results in the elongation reducing.


2012 ◽  
Vol 706-709 ◽  
pp. 1261-1266 ◽  
Author(s):  
Wei Guo ◽  
Qu Dong Wang ◽  
Man Ping Liu ◽  
Xin Tao Liu ◽  
Hao Zhou

Repetitive upsetting (RU) was applied to a commercial AZ31 Mg alloy. The samples were processed at temperatures of 230 °C, 250 °C and 300 °C up to 3 passes. Effects of processing temperature on the microstructure and mechanical properties were investigated. The results indicate that the microstructure was effectively refined by RU and an average grain size of ~1.9 μm was obtained at 250 °C. Increasing the temperature resulted in larger mean grain size and higher microstructural homogeneity. Both the strength and hardness were significantly improved. It was also found that increasing the processing temperature led to increase in the strength but decrease in the ductility. The sample after RU 3 passes at 230 °C had tensile strength of 330 MPa compared with 173 MPa prior to the processing.


2009 ◽  
Vol 23 (06n07) ◽  
pp. 990-995 ◽  
Author(s):  
GUOQING CHEN ◽  
JUNHUI SONG ◽  
XUESONG FU ◽  
YUXIAN ZHAO ◽  
WENLONG ZHOU

This paper describes the effect of hot extrusion on the microstructure and mechanical properties of electromagnetic continuous cast (EMC) AZ31 alloy. The microstructure, mechanical properties and fracture surfaces of AZ31 alloy before and after extrusion were investigated. The results demonstrate that extrusion processing gives rise to a strong basal texture. The grains are significantly refined and the average grain size of localized fine grain area is 2μm. Compared with EMC ingots, as-extruded specimens have much finer grain size and more uniform microstructure, and the second phase ( Mg 17 Al 12) becomes smaller and distributes more uniformly. The mechanical properties of the deformed AZ31 were improved after hot-extrusion. When the extrusion ratio was 10, the yield strength, ultimate tensile strength and reduction in cross-sectional area of as-extruded AZ31 alloy were 248MPa, 306MPa and 28.44%, which were respectively enhanced by 78.4%, 41% and 45.25%, compared with those of as-cast samples. With the increase of extrusion ratio, the grain refining effect was more significant and the microstructure was more uniform. The yield strength, ultimate tensile strength and reduction in cross-sectional area increased obviously with increasing the extrusion ratio. The observation on fracture surfaces demonstrates that the fracture mode changes from ductile-brittle fracture to ductile fracture after extrusion.


2012 ◽  
Vol 57 (3) ◽  
pp. 863-867 ◽  
Author(s):  
K. Topolski ◽  
H. Garbacz ◽  
P. Wiecinski ◽  
W. Pachla ◽  
K.J. Kurzydłowski

The mechanical properties of titanium Grade 2 subjected to the hydrostatic extrusion technique (HE) were investigated. The hydrostatic extrusion technique is a method which refines the titanium grains to a nano-metric size. Compared with coarse grained titanium (CG-Ti), nanocrystalline titanium (NC-Ti) is characterized by a much higher yield stress, tensile strength and microhardness. The yield stress of NC-Ti determined in tensile tests is higher than that measured in compression test. The Young modulus of NC-Ti is slightly lower than that of CG-Ti.


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