Estimation of Elastic Constants of Restoration Mortars, Used on Historic Masonries Restoration Interventions, VIA Ultrasonic Technique and Correlation to their Mechanical and Microstructure Parameters

2004 ◽  
Vol 852 ◽  
Author(s):  
Antonia Moropoulou ◽  
Asterios Bakolas ◽  
Eleni Aggelakopoulou ◽  
Anastasia Odatzidou ◽  
Christos Teas ◽  
...  

ABSTRACTEight syntheses of mortars used for restoration interventions in historic masonry were produced using the traditional materials of aerial lime and artificial pozzolanic additives. The mortars were aged over a 15-month period and then tested for properties related to chemical and mechanical stabilization using the following four analytical techniques: ultrasonic velocity propagation and the mortars' dynamic modulus of elasticity (Ed), mercury intrusion porosimetry for evaluation of microstructural characteristics (percentage open porosity, bulk density, average pore radius, total cumulative volume, and specific surface area), water capillary rise tests for the determination of total cumulative volume accessible to water and capillary rise coefficients of the mortars, and conventional mechanical tests for the determination of the mortars' flexural and compressive strength. Performance is correlated to the mortars' chemical composition, microstructural characteristics (as measure by average pore radius) and mechanical characteristics as measured by dynamic modulus of elasticity (Ed) and flexural and compressive strength (Fc).

Buildings ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 104
Author(s):  
Fernando A. N. Silva ◽  
João M. P. Q. Delgado ◽  
António C. Azevedo ◽  
Tahlaiti Mahfoud ◽  
Abdelhafid Khelidj ◽  
...  

Early deterioration of reinforced concrete foundations has been often reported in recent years. This process is usually characterized by an extensive mapping cracking process on concrete surfaces that results from several types of Internal Swelling Reaction (ISR). In this paper, a real case study of a tall reinforced concrete building with a severe deterioration process installed in its deep foundations is discussed. Laboratory tests were performed in concrete drilled cores extracted from a deep pile cap block 19 years after the beginning of construction. Tests to assess the compressive strength, the static and the dynamic modulus of elasticity, the gas permeability, and electron microscopy scanning to find out the primary mechanism responsible for the deterioration observed during in situ inspections. Chemical alterations of materials were observed in concrete cores, mainly due to Delayed Ettringite Formation (DEF), which significantly affected the integrity and durability of the structure. Dynamic modulus of elasticity showed to be a better indicator of damage induced by ISR in concrete than compressive strength. Procedures to strengthen the deteriorated elements using prestressing proved to be an efficient strategy to recover the structural integrity of pile caps deteriorated due to expansions due to ISR.


Holzforschung ◽  
2007 ◽  
Vol 61 (4) ◽  
pp. 414-418 ◽  
Author(s):  
Cheng-Jung Lin ◽  
Ming-Jer Tsai ◽  
Chia-Ju Lee ◽  
Song-Yung Wang ◽  
Lang-Dong Lin

Abstract The effects of ring characteristics on the compressive strength and dynamic modulus of elasticity of seven softwood species in Taiwan were examined. The results revealed good correlation between compressive strength and dynamic modulus of elasticity obtained using an ultrasonic wave technique (correlation coefficient r=0.77–0.86). Overall, compressive strength increased with decreasing ring width parameters and increasing ring density parameters. Ring density was related to compressive strength, but was not the sole factor affecting the wood strength. According to our statistical analysis, compressive strength was affected by various ring characteristics. Relationships between ring characteristics and compressive strength are influenced by the anatomic direction. Results revealed that earlywood density and minimum density in a ring are equally important variables for evaluating the compressive strength of wood.


2010 ◽  
Vol 5 (3) ◽  
pp. 261-268 ◽  
Author(s):  
Rodiansono Rodiansono ◽  
Wega Trisunaryanti

Activity test and regeneration of NiMo/active natural zeolite catalyst for hydrocracking of waste plastic fraction of polyprophylene (PP) type have been carried out. The catalysts was prepared by loading Mo followed by Ni Metals onto the natural zeolite (Z) sample, then calcined at 500oC, oxidized and reduced at 400oC under nitrogen, oxygen and hydrogen stream, respectively. The characterization of catalysts including spesific surface area, average pore radius, and total pore volume were performed by gas sorption analyzer, amount of total acid sites was determined by gas sorption method, and acid site strength was confirmed by IR spectroscopy. The hydrocracking process was carried out in a semi-flow reactor system at 360 oC and catalyst:feed ratio 0.5 under hydrogen stream (150 mL/hour). The feed was vaporized from the pyrolisis reactor into the hydrocracking reactor. A liquid product was collected and analyzed by gas chromatography (GC) and gas chromatography-mass spectroscopy (GC-MS). The characterization results showed that spesific surface area, average pore radius, and total pore volume of the Z sample decreased after loading of the Ni and Mo metals. Amount of total acid sites of the NiMo/Z catalyst was higher than that of the Z sample. The activity of NiMo/Z catalyst decreased after several continously runs. Its regeneration produced the NiMo/Z reg catalyst with similar activity and selectivity to the fresh catalyst (NiMo/Z). The activity of catalysts at the optimum condition followed the order of NiMo/Z reg>NiMo/Z>Z (conversion of hydrocarbon C>12) and NiMo/Z reg>NiMo/Z>Z (total yield of gasoline fraction). The selectivity of catalysts for C7-C8 product followed the order of Z>NiMo/Z>NiMo/Z reg. Keywords: activity, polyprophylene, catalyst, gasoline fraction.


Holzforschung ◽  
2016 ◽  
Vol 70 (1) ◽  
pp. 79-85 ◽  
Author(s):  
Julia K. Denzler ◽  
Andreas Weidenhiller

AbstractThe possibility for pre-grading of logs throughout the year has been evaluated based on dynamic modulus of elasticity (MOEdynor simplifiedEdyn) by means of frequency-based nondestructive testing (NDTfreq). The challenge is thatEdynis variable in the frozen, partly frozen, and unfrozen states of logs (state of matter). In the unfrozen state, NDTfreqis reliable if the moisture content does not fall below fiber saturation. The state of the matter was tested via temperature measurements of air and log by means of an infrared technique and sensors, and information was evaluated from NDTfreq. The temperature measurements proved to be inefficient for industrial application because of unreliable data and long measurement times, whereas the NDTfreqmeasurements allowed the determination of meaningful damping factors. A sufficient level of predictability for more than 60% of the measurements was found. The log measurements in the partly frozen state are inconclusive becauseEdyndata fluctuate in the presence of both liquid and frozen water. For the completely frozen logs, a correction is introduced as a precaution that avoids an overestimation ofEdynin the unfrozen state.


2011 ◽  
Vol 243-249 ◽  
pp. 165-169 ◽  
Author(s):  
Iqbal Khan Mohammad

Nondestructive testing (NDT) is a technique to determine the integrity of a material, component or structure. The commonly NDT methods used for the concrete are dynamic modulus of elasticity and ultrasonic pulse velocity. The dynamic modulus of elasticity of concrete is related to the structural stiffness and deformation process of concrete structures, and is highly sensitive to the cracking. The velocity of ultrasonic pulses travelling in a solid material depends on the density and elastic properties of that material. Non-destructive testing namely, dynamic modulus of elasticity and ultrasonic pulse velocity was measured for high strength concrete incorporating cementitious composites. Results of dynamic modulus of elasticity and ultrasonic pulse velocity are reported and their relationships with compressive strength are presented. It has been found that NDT is reasonably good and reliable tool to measure the property of concrete which also gives the fair indication of the compressive strength development.


2010 ◽  
Vol 163-167 ◽  
pp. 1655-1660
Author(s):  
Jian Zhang ◽  
Bo Diao ◽  
Xiao Ning Zheng ◽  
Yan Dong Li

The mechanical properties of high strength concrete(HSC) were experimentally investigated under mixed erosion and freeze-thaw cycling according to ASTM C666(Procedure B), the erosion solution was mixed by weight of 3% sodium chloride and 5% sodium sulfate. The mass loss, relative dynamic modulus of elasticity, compressive strength, elastic modulus and other relative data were measured. The results showed that with the increasing number of freeze-thaw cycles, the surface scaled more seriously; the mass loss, compressive strength and elastic modulus continued to decrease; the relative dynamic modulus of elasticity increased slightly in the first 225 freeze-thaw cycles, then decreased in the following 75 cycles; the corresponding strain to peak stress decreased with the increase of freeze-thaw cycles. After 200 cycles, the rate of deterioration of concrete accelerated obviously.


2016 ◽  
Vol 138 (3) ◽  
Author(s):  
João Victor Staub de Melo ◽  
Glicério Trichês

This paper reports the results obtained in a study on the effect of the addition of TiO2 nanoparticles on the mechanical properties and microstructural characteristics of photocatalytic concretes. In the hardened state, tests to determine the compressive strength and modulus of elasticity were carried out. Also, microstructural aspects of the samples were investigated. In the fresh state, the influence of the addition of TiO2 on the concrete compaction and conduction calorimetry curves was evaluated. The results obtained indicated a better mechanical and microstructural behavior of concrete with addition of TiO2.


1996 ◽  
Vol 13 (6) ◽  
pp. 469-477 ◽  
Author(s):  
A.M. Youssef ◽  
G.E. Badr ◽  
Th. El-Nabarawy

CuO/Fe2O3 (1:1) was prepared by co-precipitation. Six thermal products (I–VI) were obtained by calcination in the temperature range 300–800°C. The structures of I–VI were determined from XRD patterns and they were also identified from electrical conductivity measurements in the temperature range 313–523 K. The textural properties were determined from nitrogen adsorption at 77 K and the acidities of the thermal product were measured by pyridine chemisorption at 423 K. The decomposition of H2O2 over the catalysts I–VI was followed in the temperature range 303–323 K. Conversion of 2-propanol was investigated at 523 K. Calcination of CuO/Fe2O3 at 600°C resulted in partial transformation to CuFe2O4, this transformation predominating at 700°C and being complete at 800°C. Two mechanisms of electrical conduction are involved for catalysts calcined at 600–800°C depending on the temperature at which σ is measured. The surface area decreases and the average pore radius increases with increasing calcination temperature due to sintering and spinel formation. A mechanism is suggested for H2O2 decomposition and the activity and selectivity of the catalysts towards the conversion of 2-propanol are discussed.


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