scholarly journals DEPOSITION Ti-Sn ON AISI 316L SUBSTRATE WITH SURFACE MECHANICAL ALLOYING TREATMENT (SMAT) FOR BIOMATERIAL APPLICATION IN SIMULATED BODY FLUID

2021 ◽  
Vol 14 (3) ◽  
Author(s):  
Febriyanto Wijaya Pangestu ◽  
Talitha Ratna D. ◽  
Djoko Hadi Prajitno

The properties of biomaterials such as biocompatibility, which is non-allergic and non-toxic to be the main requirements that must be owned by the biomaterials because of the presence of direct contact between the biomaterial with body parts. Therefore the study of biomaterials is constantly carried to repair the biocompatibility. In this research, the improvement of the properties the compatibility of the metal alloy AISI 316L with superimposed ideal bio-inert Ti-Sn with the method of Surface Mechanical Alloying Treatment. Manufacture of the alloy with bio-inert Ti-Sn using a variation of the composition of Sn of 10% and Sn 20% done using Mechanosynthesis process. The results of the process are sintered with the variation of temperature of 800oC and 900oC for 2 hours and then were characterized by an optical microscope. Corrosion testing of the alloy was carried out with Polarization Tafel System Three Electrode method for 10 minutes. The results of characterization with an optical microscope shows there is a layer of bio-inert Ti-Sn the results of the process of SMAT of AISI 316L. The results of corrosion testing on alloy AISI 316L Ti-Sn in a solution of SBF showed that the content of Ti-10%Sn with a temperature of 800oC the obtained corrosion rate 4.785 MPY and at 900oC amounted to 4.155 MPY as well as on the content of Ti-20%Sn with a temperature of 800oC the obtained corrosion rate 3.525 MPY and at 900oC amounted to 3.234 MPY. Keywords: Biocompatible; Biomaterial; AISI 316L; Ti-Sn; Corrosion Rate; Allergic Reaction; Deposition.      

1994 ◽  
Vol 367 ◽  
Author(s):  
M. Hinojosa ◽  
R. Rodréguez ◽  
U. Ortiz

AbstractFractal dimension of the microstructure of AISI 316L steel (17 Cr, 12.7 Ni, 2.1 Mo, 1. 5 Mn, 0.01 C) with different degrees of strain were obtained from Richardson plots of grain boundary perimeter against magnification. Grain boundaries were revealed using conventional metallographic techniques and measurements were taken with the aid of an automatic image analizer (Quantimet 520) attached to an optical microscope. The magnifications used were 50, 100, 200, 400, and 1000X. The samples were obtained from a 4” diameter tubing, machined according to ASTM A370 standard test method and deformed to 5, 10, 15, and 20 % tensile strain. The results show that the fractal dimension of the grain boundaries changes as deformation is imparted to the material.These results suggest that fractal dimension may be used to describe microstructural evolution of metals during deformation processes.


Author(s):  
Abdul Ghofur ◽  
Dhonie Adetya Rachman ◽  
Muhammad Mochtar Lutfi ◽  
Fathur Rahman

<p class="02abstracttext">Leachate water from final waste landfill (Tempat Pembuangan Akhir, TPA) contains harmful substances for the environment and living organisms. Furthermore, the leachate water can deteriorate equipment buried near TPA, e.g. buried water pipe. This work investigated the corrosion rate of mild steel SPCC SD after immersion in leachate water of TPA Gunung Kupang and Cahaya Kencana located in South Kalimantan. The steel plate immersion into leachate water was worked out in 3 different cases. The first case was 2 weeks immersion in leachate water followed by 1 week contact with ambient air. In the second case, steel plate was immersed in leachate water for 1 week and then 2 weeks in direct contact with ambient air. The last one was steel plate immersion in leachate water for 3 weeks without any direct contact with ambient air. The investigation shows that longer contact duration between wet steel surface, after immersion in leachate water, with ambient air increases the corrosion rate. The investigation shows also that the corrosion rate due to leachate water from Gunung Kupang landfill is higher than that of Cahaya Kencana landfill. Corrosion rate for TPA Gunung Kupang case varies from 0.441 to 0.718 mmpy. Meanwhile, corrosion rate for TPA Cahaya Kencana varies from 0.131 to 0.495 mmpy. This is due to lower pH of leachate water from TPA Mount Kupang.</p>


Author(s):  
D. T. Oloruntoba ◽  
O. S. Adesina ◽  
O. F. Abraham ◽  
K. J. Akinluwade

This research focused on the corrosion behavior of gray cast iron and aluminum in alkaline medium (0.5 M NaOH) with and without inhibitor (water hyacinth Eichhornia crassipes extract) of varying concentrations of 5%, 10%, 15%, 20% and 25%. The corrosion rates of the metal samples were investigated using the weight loss and electrochemical methods alongside the formulation of a dispersant using readily available chemicals to develop a colloidal solution of the extract produced by hot water digestion of the water hyacinth plant leaves. The metallography tests of control samples as well as the most and least corroded samples were carried out using Optical Microscope (OM). The results revealed that the aluminum resulted in minimum corrosion rate of 0.000483 mg/mm2/yr with inhibitor efficiency of 98.93% obtained for sample A5 (25% extract from water hyacinth) while for the gray cast iron, a minimum corrosion rate of -4.4E-05 mg/mm2/yr with inhibitor efficiency of 566.6% obtained for sample C3 (15% extract from water hyacinth). The electrochemical result of aluminum showed increase in corrosion potential from -1.494 VAg/AgCl to -1.482 V Ag/AgCl and that of gray cast iron from -0.5436 VAg/AgCl to -0.2839 VAg/AgCl upon increase in inhibitor concentration. Therefore, the use of water hyacinth (Eichhornia crassipes)extract reduced the corrosion or dissolution rate of gray cast iron and aluminum in (NaOH) sodium hydroxide medium.


2013 ◽  
Vol 12 (3) ◽  
pp. 231-238
Author(s):  
Teresa Szymura ◽  
Wojciech Adamczyk

Corrosion testing was performed on structural steel of a cooling tower in the environment of cooling water containing ammonium sulfates and ammonium chloride. The test were performed using gravimetric and electrochemical methods with the application of a potentiostat. The analyses clearly showed that the corrosion rate is higher in solutions that contain ammonium sulfate and that the S235JRG2 steel exhibits higher corrosion resistance in this environment.


2019 ◽  
Vol 21 (3) ◽  
pp. 127
Author(s):  
Hardi Hidayat ◽  
Budi Setyahandana ◽  
Yohannes Sardjono ◽  
Yulwido Adi

The purpose of this study is to determine the value of corrosion rate influenced by coastal environment and seawater to nickel as a collimator base material for the application of boron neutron capture therapy (BNCT). In this research, the authors used 99.9% pure nickel as the reference material. Corrosion testing was carried out to determine the rate of corrosion of nickel as a base material for BNCT. After the specimens were formed, the test specimens were then corroded for 12 weeks, with various conditions such as indoor, outdoor environment, static seawater, and moving seawater. The results of this study indicated that in corrosion testing with indoor condition, the corrosion rate values are 0.61-1.00 mpy. For outdoor condition, the corrosion rate is 0.89-1.34 mpy. Meanwhile, at static seawater conditions, the corrosion rate is 0.97-1.24 mpy. Lastly, for moving seawater condition, the corrosion rate is 1.64-1.91 mpy. The results showed that corrosion resistance was relatively the same for all nickel exposed to corrosion in the coastal environment. Therefore, in regards to corrosion resistance, using nickel as a collimator base material for BNCT applications is considered as safe.Keywords: BNCT, Nickel, Corrosion, Coastal Environtment, Sea Water


2014 ◽  
Vol 522-524 ◽  
pp. 341-345
Author(s):  
Dan Dan Liu ◽  
Yan Ling Cui ◽  
Chang Feng Liu ◽  
Xin Lin Gao ◽  
Yin Yao Xia

In vitro test was used to determine the effect of acid stress on soil nematode (Meloidogyne incognita) J2 survival, behavior, individual development and fluid extravasations. The effects of acid stress on J2 survival is C2H2O4>C6H8O7>C4H6O5. Inhibition on J2 movement behavior increased with time prolonged. Effect on nematode body length, stylet length, tail transparent area length, body fluid extravasations: C2H2O4>C6H8O7>C4H6O5. At high magnification optical microscope can be clearly observed symptoms of poisoning J2. Compared with the control, acid inhibited the nematode survival, movement and individual development, promote the body fluid extravasations, destroyed the normal physiological metabolism of nematodes, even lead to death.


2012 ◽  
Vol 602-604 ◽  
pp. 1663-1666
Author(s):  
Zhong Qing Tian ◽  
Guo Xing Zhang ◽  
Wei Jiu Huang ◽  
Yu Kai Zhu

The mechanical alloying method process has been innovatively used to prepare Cu-Cr coating on the inner wall of steel pipe. The effect of the rotating speed on thickness, microhardness and friction coefficient of the Cu-Cr coating was investigated. The coating thickness was measured from all samples using optical microscope. The microhardness was analyzed by Digital Microhardness Tester. The friction coefficient was tested by high speed reciprocating friction testing machine. The results show that the coating thickness is 26, 29 and 31μm at the rotating speed of 200, 250 and 300 rpm. The microhardness of the Cu-Cr coating prepared at 200, 250 and 300 rpm are about 760, 780 and 830 Hv. The friction coefficient of the Cu-Cr coating prepared at 200 rpm are about 0.25, 0.40 and 0.38 at the frequencies of 3, 4 and 5 Hz. The friction coefficient of the Cu-Cr coating prepared at 250 rpm are about 0.30, 0.29 and 0.20 at the frequencies of 3, 4 and 5 Hz. The friction coefficient of the Cu-Cr coating prepared at 300 rpm are about 0.10, 0.13 and 0.09 at the frequencies of 3, 4 and 5 Hz.


Coatings ◽  
2020 ◽  
Vol 10 (3) ◽  
pp. 231
Author(s):  
Farzad Soleymani ◽  
Rahmatollah Emadi ◽  
Sorour Sadeghzade ◽  
Fariborz Tavangarian

Polymer–ceramic composite coatings on magnesium-based alloys have attracted lots of attention in recent years, to control the speed of degradability and to enhance bioactivity and biocompatibility. In this study, to decrease the corrosion rate in a simulated body fluid (SBF) solution for long periods, to control degradability, and to enhance bioactivity, polycaprolactone–chitosan composite coatings with different percentages of baghdadite (0 wt.%, 3 wt.%, and 5 wt.%) were applied to an anodized AZ91 alloy. According to the results of the immersion test of the composite coating containing 3 wt.% baghdadite in a phosphate buffer solution (PBS), the corrosion rate decreased from 0.45 (for the AZ91 sample) to 0.11 mg/cm2·h after seven days of immersion. To evaluate the apatite formation capability of specimens, samples were immersed in an SBF solution. The results showed that the samples were bioactive as apatite layers formed on the surface of specimens. The composite coating containing 3 wt.% baghdadite showed the highest apatite-formation capability, with a controlled release of ions, and the lowest corrosion rate in the SBF.


Sign in / Sign up

Export Citation Format

Share Document