scholarly journals Facile bacterial cellulose nanofibrillation for the development of plasmonic paper sensor

2020 ◽  
Author(s):  
Agnes Purwidyantri ◽  
Myrtha Karina ◽  
Chih-Hsien Hsu ◽  
Yoice Srikandace ◽  
Briliant Adhi Prabowo ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Bacterial Cellulose ◽  
Limit Of Detection ◽  
High Surface ◽  
Textural Properties ◽  
Food Product ◽  
Casting Process ◽  
Sers Substrate ◽  
Paper Sheet ◽  
Plasmonic Sensor

In this present work, a plasmonic sensor is developed through an extremely cheap cellulose-based source, widely known as a food product, nata de coco (NDC). Capturing its interesting features, such as innate surface roughness from naturally grown cellulose during its fermentation period, the engineering and modulation of NDC fibril size and properties were attempted through a high-pressure homogenization (HPH) treatment to obtain highly dense nanofibrils. After the transformation into a thin, paper-sheet form through a casting process, the homogenized bacterial cellulose (HBC) resulting from HPH was compared with the normally agitated bacterial cellulose (BC) pulp and decorated with silver nanoparticles (AgNPs) to produce plasmonic papers, for further application as surface-enhanced Raman scattering (SERS) substrate. As demonstrated in the measurement of Rhodamine 6G (R6G) molecule, the plasmonic HBC paper sheet provided more prominent SERS signals than the plasmonic BC due to its high surface roughness and improved textural properties from the nanofibrillation process favoring better adsorption of AgNPs and effective SERS hotspots generation. The plasmonic HBC obtained a 2 order higher estimated SERS enhancement factor over the plasmonic BC with a limit of detection of approximately 92 fM. Results denote that the proposed approach provides a new, green-synthesis route toward the exploration of biodegradable sources integrated into an inexpensive and simple nanostructuring process for the production of flexible, paper-based, plasmonic sensors.

scholarly journals Evaluation and optimisation of a slurry-based layer casting process in additive manufacturing using multiphase simulations and spatial reconstruction

2021 ◽  
Author(s):  
P. Erhard ◽  
A. Seidel ◽  
J. Vogt ◽  
W. Volk ◽  
D. Günther
Keyword(s):  
Surface Roughness ◽  
3D Printing ◽  
Fine Particles ◽  
High Surface ◽  
Casting Process ◽  
Spatial Reconstruction ◽  
Novel Method ◽  
Slurry Layer ◽  
High Level

AbstractSlurry-based 3D printing allows ceramic green bodies to be fabricated at high packing densities. In contrast to powder-based binder jetting, full densification of printed parts can be achieved in a subsequent sintering step as fine particles dispersed in a suspension are cast and compacted. Slurry-based 3D printing is thus expected to overcome the application limits of the powder-based alternative in metal casting in terms of unfavorable properties like high surface roughness, low density and low mechanical strength. To ensure stress-free drying and therefore high qualities of the compounds made in layers, it is crucial to fabricate single layers with a high level of homogeneity. This paper presents a CFD model based on the open-source simulation environment OpenFOAM to predict the resulting homogeneity of a cast slurry layer with defined parameter sets or coater geometries using the Volume-Of-Fluid method. Moreover, a novel method of spatial reconstruction is proposed to evaluate the surface quality of layers on a minimised computional demand. By comparing the results of the simulation with the real macroscopic behaviour determined in experiments, the approach is found to be a useful tool for suggesting suitable parameters and coater geometries for processing slurries. A precise reconstruction of the outline of the coating area with different process parameters and an approximate prediction of the effect on surface roughness was achieved.

OPTIMISATION OF SAND CASTING PROCESS FOR IMPELLER USING TAGUCHI METHODOLOGY

2020 ◽  
Vol XVII (2) ◽  
pp. 23-33
Author(s):  
Faisal Hafeez ◽  
Salman Hussain ◽  
Wasim Ahmad ◽  
Mirza Jahanzaib
Keyword(s):  
Surface Roughness ◽  
Surface Defects ◽  
A356 Alloy ◽  
Casting Process ◽  
Sand Casting ◽  
Gate Length ◽  
Taguchi Methodology ◽  
Confirmatory Tests ◽  
Binder Ratio ◽  
Response Measures

This paper presents the study to investigate the effects of binder ratio, in-gate length and pouring height on hardness, surface roughness and casting defects of sand casting process. Taguchi methodology with L9 orthogonal array was employed to design the experimentation. Sand casting of six blade impeller using A356 alloy was performed and empirical models for all the above response measures were formulated. Confirmatory tests and analysis of variance results confirmed the accuracy of the model. Binder ratio was found to be the most significant parameter affecting casting surface defects and surface roughness. This was followed by pouring height and in-gate length.

scholarly journals Geometric correction for thermographic images of asteroid 162173 Ryugu by TIR (thermal infrared imager) onboard Hayabusa2

2021 ◽  
Vol 73 (1) ◽  
Author(s):  
Takehiko Arai ◽  
Tatsuaki Okada ◽  
Satoshi Tanaka ◽  
Tetsuya Fukuhara ◽  
Hirohide Demura ◽  
...  
Keyword(s):  
Surface Roughness ◽  
High Surface ◽  
Thermal Inertia ◽  
Thermal Infrared ◽  
Shape Model ◽  
Infrared Imager ◽  
Least Squares Fit ◽  
Temperature Maps ◽  
Pixel Scale ◽  
Thermal Infrared Imager

AbstractThe thermal infrared imager (TIR) onboard the Hayabusa2 spacecraft performed thermographic observations of the asteroid 162173 Ryugu (1999 JU$$_3$$ 3 ) from June 2018 to November 2019. Our previous reports revealed that the surface of Ryugu was globally filled with porous materials and had high surface roughness. These results were derived from making the observed temperature maps of TIR using a projection method onto the shape model of Ryugu as geometric corrections. The pointing directions of TIR were calculated using an interpolation of data from the SPICE kernels (NASA/NAIF) during the periods when the optical navigation camera (ONC) and the light detection and ranging (LIDAR) observations were performed. However, the mapping accuracy of the observed TIR images was degraded when the ONC and LIDAR were not performed with TIR. Also, the orbital and attitudinal fluctuations of Hayabusa2 increased the error of the temperature maps. In this paper, to solve the temperature image mapping problems, we improved the correction method by fitting all of the observed TIR images with the surface coordinate addressed on the high-definition shape model of Ryugu (SFM 800k v20180804). This correction adjusted the pointing direction of TIR by rotating the TIR frame relative to the Hayabusa2 frame using a least squares fit. As a result, the temperature maps spatially spreading areas were converged within high-resolved $$0.5^\circ$$ 0 . 5 ∘ by $$0.5^\circ$$ 0 . 5 ∘ maps. The estimated thermal inertia, for instance, was approximately 300$$\sim$$ ∼ 350 Jm$$^{-2}$$ - 2 s$$^{-0.5}$$ - 0.5 K$$^{-1}$$ - 1 at the hot area of the Ejima Saxum. This estimation was succeeded in case that the surface topographic features were larger than the pixel scale of TIR. However, the thermal inertia estimation of smooth terrains, such as the Urashima crater, was difficult because of surface roughness effects, where roughness was probably much smaller than the pixel scale of TIR.

scholarly journals Mechanical Characterization and Thermodynamic Analysis of Laser-Polished Landscape Design Products Using 3D Printing

Materials ◽  
2021 ◽  
Vol 14 (10) ◽  
pp. 2601
Author(s):  
Yue Ba ◽  
Yu Wen ◽  
Shibin Wu
Keyword(s):  
Surface Roughness ◽  
3D Printing ◽  
Fused Deposition Modeling ◽  
High Surface ◽  
Landscape Design ◽  
Laser Polishing ◽  
Fused Deposition ◽  
Design Structure ◽  
3D Printed ◽  
Stability And Accuracy

Recent innovations in 3D printing technologies and processes have influenced how landscape products are designed, built, and developed. In landscape architecture, reduced-size models are 3D-printed to replicate full-size structures. However, high surface roughness usually occurs on the surfaces of such 3D-printed components, which requires additional post-treatment. In this work, we develop a new type of landscape design structure based on the fused deposition modeling (FDM) technique and present a laser polishing method for FDM-fabricated polylactic acid (PLA) mechanical components, whereby the surface roughness of the laser-polished surfaces is reduced from over Ra 15 µm to less than 0.25 µm. The detailed results of thermodynamics and microstructure evolution are further analyzed during laser polishing. The stability and accuracy of the results are evaluated based on the standard deviation. Additionally, the superior tensile and flexural properties are examined in the laser-polished layer, in which the ultimate tensile strength (UTS) is increased by up to 46.6% and the flexural strength is increased by up to 74.5% compared with the as-fabricated components. Finally, a real polished landscape model is simulated and optimized using a series of scales.

scholarly journals Effect of Optical and Morphological Control of Single-Structured LEC Device

Micromachines ◽  
2021 ◽  
Vol 12 (7) ◽  
pp. 843
Author(s):  
Woo Jin Jeong ◽  
Jong Ik Lee ◽  
Hee Jung Kwak ◽  
Jae Min Jeon ◽  
Dong Yeol Shin ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Surface Roughness ◽  
Surface Properties ◽  
High Efficiency ◽  
High Surface ◽  
Reduction Rate ◽  
Operating Characteristics ◽  
Emission Layer ◽  
Light Emitting ◽  
Stable Operating

We investigated the performance of single-structured light-emitting electrochemical cell (LEC) devices with Ru(bpy)3(PF6)2 polymer composite as an emission layer by controlling thickness and heat treatment. When the thickness was smaller than 120–150 nm, the device performance decreased because of the low optical properties and non-dense surface properties. On the other hand, when the thickness was over than 150 nm, the device had too high surface roughness, resulting in high-efficiency roll-off and poor device stability. With 150 nm thickness, the absorbance increased, and the surface roughness was low and dense, resulting in increased device characteristics and better stability. The heat treatment effect further improved the surface properties, thus improving the device characteristics. In particular, the external quantum efficiency (EQE) reduction rate was shallow at 100 °C, which indicates that the LEC device has stable operating characteristics. The LEC device exhibited a maximum luminance of 3532 cd/m2 and an EQE of 1.14% under 150 nm thickness and 100 °C heat treatment.

scholarly journals A Brief Overview of Recent Progress in Porous Silica as Catalyst Supports

2021 ◽  
Vol 5 (3) ◽  
pp. 75
Author(s):  
Preeti S. Shinde ◽  
Pradnya S. Suryawanshi ◽  
Kanchan K. Patil ◽  
Vedika M. Belekar ◽  
Sandeep A. Sankpal ◽  
...  
Keyword(s):  
Heterogeneous Catalysis ◽  
High Surface ◽  
High Surface Area ◽  
Porous Silica ◽  
Textural Properties ◽  
Silica Particles ◽  
Catalyst Supports ◽  
Silica Supports ◽  
Low Degree ◽  
Transfer Properties

Porous silica particles have shown applications in various technological fields including their use as catalyst supports in heterogeneous catalysis. The mesoporous silica particles have ordered porosity, high surface area, and good chemical stability. These interesting structural or textural properties make porous silica an attractive material for use as catalyst supports in various heterogeneous catalysis reactions. The colloidal nature of the porous silica particles is highly useful in catalytic applications as it guarantees better mass transfer properties and uniform distribution of the various metal or metal oxide nanocatalysts in solution. The catalysts show high activity, low degree of metal leaching, and ease in recycling when supported or immobilized on porous silica-based materials. In this overview, we have pointed out the importance of porous silica as catalyst supports. A variety of chemical reactions catalyzed by different catalysts loaded or embedded in porous silica supports are studied. The latest reports from the literature about the use of porous silica-based materials as catalyst supports are listed and analyzed. The new and continued trends are discussed with examples.

scholarly journals Post-Processing and Surface Characterization of Additively Manufactured Stainless Steel 316L Lattice: Implications for BioMedical Use

Materials ◽  
2021 ◽  
Vol 14 (6) ◽  
pp. 1376
Author(s):  
Alex Quok An Teo ◽  
Lina Yan ◽  
Akshay Chaudhari ◽  
Gavin Kane O’Neill
Keyword(s):  
Surface Roughness ◽  
Stainless Steel ◽  
Surface Characterization ◽  
High Surface ◽  
Surface Characteristics ◽  
Post Processing ◽  
Stainless Steel 316L ◽  
Processing Methods ◽  
Particulate Debris

Additive manufacturing of stainless steel is becoming increasingly accessible, allowing for the customisation of structure and surface characteristics; there is little guidance for the post-processing of these metals. We carried out this study to ascertain the effects of various combinations of post-processing methods on the surface of an additively manufactured stainless steel 316L lattice. We also characterized the nature of residual surface particles found after these processes via energy-dispersive X-ray spectroscopy. Finally, we measured the surface roughness of the post-processing lattices via digital microscopy. The native lattices had a predictably high surface roughness from partially molten particles. Sandblasting effectively removed this but damaged the surface, introducing a peel-off layer, as well as leaving surface residue from the glass beads used. The addition of either abrasive polishing or electropolishing removed the peel-off layer but introduced other surface deficiencies making it more susceptible to corrosion. Finally, when electropolishing was performed after the above processes, there was a significant reduction in residual surface particles. The constitution of the particulate debris as well as the lattice surface roughness following each post-processing method varied, with potential implications for clinical use. The work provides a good base for future development of post-processing methods for additively manufactured stainless steel.

scholarly journals High-quality net shape geometries from additively manufactured parts using closed-loop controlled ablation with ultrashort laser pulses

2020 ◽  
Vol 9 (1-2) ◽  
pp. 101-110 ◽  
Author(s):  
Daniel Holder ◽  
Artur Leis ◽  
Matthias Buser ◽  
Rudolf Weber ◽  
Thomas Graf
Keyword(s):  
Surface Roughness ◽  
Closed Loop ◽  
High Surface ◽  
Laser Pulses ◽  
Ultrashort Laser Pulses ◽  
Minimum Thickness ◽  
High Quality ◽  
Surface Optical ◽  
The Individual ◽  
Ultrashort Laser

AbstractAdditively manufactured parts typically deviate to some extent from the targeted net shape and exhibit high surface roughness due to the size of the powder grains that determines the minimum thickness of the individual slices and due to partially molten powder grains adhering on the surface. Optical coherence tomography (OCT)-based measurements and closed-loop controlled ablation with ultrashort laser pulses were utilized for the precise positioning of the LPBF-generated aluminum parts and for post-processing by selective laser ablation of the excessive material. As a result, high-quality net shape geometries were achieved with surface roughness, and deviation from the targeted net shape geometry reduced by 67% and 63%, respectively.

scholarly journals Investigation on the Surface Quality Obtained during Trochoidal Milling of 6082 Aluminum Alloy

Machines ◽  
2021 ◽  
Vol 9 (4) ◽  
pp. 75
Author(s):  
Nikolaos E. Karkalos ◽  
Panagiotis Karmiris-Obratański ◽  
Szymon Kurpiel ◽  
Krzysztof Zagórski ◽  
Angelos P. Markopoulos
Keyword(s):  
Surface Roughness ◽  
Surface Quality ◽  
Process Parameters ◽  
Manufacturing Industry ◽  
High Surface ◽  
Cutting Tools ◽  
Cutting Speed ◽  
Depth Of Cut ◽  
High Surface Quality ◽  
Trochoidal Milling

Surface quality has always been an important goal in the manufacturing industry, as it is not only related to the achievement of appropriate geometrical tolerances but also plays an important role in the tribological behavior of the surface as well as its resistance to fatigue and corrosion. Usually, in order to achieve sufficiently high surface quality, process parameters, such as cutting speed and feed, are regulated or special types of cutting tools are used. In the present work, an alternative strategy for slot milling is adopted, namely, trochoidal milling, which employs a more complex trajectory for the cutting tool. Two series of experiments were initially conducted with traditional and trochoidal milling under various feed and cutting speed values in order to evaluate the capabilities of trochoidal milling. The findings showed a clear difference between the two milling strategies, and it was shown that the trochoidal milling strategy is able to provide superior surface quality when the appropriate process parameters are also chosen. Finally, the effect of the depth of cut, coolant and trochoidal stepover on surface roughness during trochoidal milling was also investigated, and it was found that lower depths of cut, the use of coolant and low values of trochoidal stepover can lead to a considerable decrease in surface roughness.

Surface and Sub-Surface Integrity of Ultra- Machined BK7 Using Fine and Coarse Grained Diamond Wheels

2007 ◽  
Vol 359-360 ◽  
pp. 234-238 ◽  
Author(s):  
Qing Liang Zhao ◽  
Bo Wang ◽  
Ekkard Brinksmeier ◽  
Otmann Riemer ◽  
Kai Rickens ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Surface Integrity ◽  
High Surface ◽  
Coarse Grained ◽  
Nanometer Scale ◽  
Grinding Wheels ◽  
Fine Grained ◽  
Optical Glasses ◽  
Diamond Grinding ◽  
Surface Damages

This paper aims to evaluate the surface and sub-surface integrity of optical glasses which were correspondingly machined by coarse and fine-grained diamond grinding wheels on Tetraform ‘C’ and Nanotech 500FG. The experimental results show that coarse-grained diamond grinding wheels are capable of ductile grinding of optical glasses with high surface and sub-surface integrity. The surface roughness values are all in nanometer scale and the sub-surface damages are around several micros in depth, which is comparative to those machined by fine-grained diamond wheels.

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