scholarly journals Aplikasi Pelarut Eutektik K2CO3-Gliserol pada Ekstraksi Pigmen Antosianin dari Kulit Manggis (Garcinia mangostana Linn.)

2020 ◽  
Vol 9 (2) ◽  
pp. 64-69
Author(s):  
Hazima Asni ◽  
Renita Manurung ◽  
Dian Bonella
Keyword(s):  
Anthocyanin Content ◽  
Solvent Ratio ◽  
Synthetic Dyes ◽  
Anthocyanin Pigment ◽  
Color Intensity ◽  
Garcinia Mangostana ◽  
Extraction Technology ◽  
Extract Yield ◽  
Mangosteen Peel ◽  
Anthocyanin Pigments

Mangosteen peel (Garcinia mangostana Linn.) contains 593 ppm of anthocyanin. Anthocyanin pigment from mangosteen peel (Garcinia Mangostana Linn.) can be used as an alternative to synthetic dyes. Eutectic solvents are the latest development in extraction technology to extract anthocyanin from its source. The solvent used is pottasium carbonate-glycerol based eutectic solvent. The purpose of this study was to determine the effect of eutectic solvents on the extraction of anthocyanin pigments from mangosteen peel. This research consists of 2 treatment factors namely rmolar ratio of K2CO3: glycerol of 1: 5, 1: 6, and 1: 7 and material: solvent ratio of 1: 4, 1: 6 and 1: 8. Anthocyanin content and color intensity were analyzed using a Spectrophotometer UV-Vis.  Extraction using K2CO3 : glycerol eutectic solvent at a ratio of 1: 7 and the ratio of material: solvent 1: 8 produced the best treatment with extract yield of 46%; anthocyanin content of 263.976 mg/L, and color intensity value of 0.173.

scholarly journals Karakteristik Antosianin dari Kulit Buah Nipah (Nypa frutican) sebagai Pewarna Alami dengan Metode Soxhletasi

2020 ◽  
Vol 9 (1) ◽  
pp. 26-33
Author(s):  
Putri Herfayati ◽  
Setiaty Pandia ◽  
Halimatuddahliana Nasution
Keyword(s):  
Antioxidant Activity ◽  
Citric Acid ◽  
Extraction Time ◽  
Anthocyanin Content ◽  
Qualitative And Quantitative Analysis ◽  
Color Intensity ◽  
Natural Pigment ◽  
Total Anthocyanin ◽  
Qualitative And Quantitative ◽  
Extract Yield

Anthocyanin is a natural pigment that gives red colour on Nipah husk (Nypa fructican) extract. Extraction of anthocyanin compounds used the soxhletation method with independent variables were the type of solvent (aquadest and ethanol with citric acid 3% (w/v)) and extraction time (30, 45 and 60 minutes). This study aims to determine the best type of solvent and extraction time used for extraction of anthocyanin from Nipah husk. The parameters in this study include qualitative and quantitative analysis of anthocyanin (extract yield, total anthocyanin concentration, color intensity, antioxidant activity and analysis of toxicity) from Nipah husk extract. The results qualitatively and quantitatively indicate that Nipah husk extract had anthocyanin content with the highest extract yield was obtained using ethanol-citric acid 3% solvent at 60 minutes extraction time of 0.546 gram / gram. The highest total anthocyanin was obtained using ethanol-citric acid 3% solvent at 30 minutes extraction time of 226.36 mg / L. The highest color intensity was obtained using ethanol-citric acid 3% solvent at 30 minutes extraction time of 0.925. The strongest antioxidant activity (IC50) was obtained using 3% aquadest-citric acid solvent at 30 minutes extraction time of 3.569 ppm. The strongest toxicity activity (LC50) in ethanol-citric acid 3% solvent was 80.023 ppm.

scholarly journals ​Standardization of Cold Solvent Extraction Parameters for Natural Red Pigments

2021 ◽  
Author(s):  
C. Mini ◽  
S.S. Aparna Nath ◽  
S.G. Lekshmi
Keyword(s):  
Solvent Extraction ◽  
Raw Materials ◽  
Pigment Content ◽  
Raw Material ◽  
Anthocyanin Content ◽  
Solvent Ratio ◽  
Carotene Content ◽  
Ratio Requirement ◽  
Natural Colorant ◽  
Extract Yield

Background: Selecting an appropriate extraction technique and optimization of extraction conditions must be done to improve the efficiency and productivity of natural colorant. Methods: Flesh and peels of four different raw materials viz., beetroot, carrot, pomegranate and grape were extracted independently using 100% ethyl alcohol using cold solvent extraction method adopting 1: 1 and 1: 2 w/v solid to solvent ratio for 24 and 48 hrs, forming 8 treatments replicated thrice in three factorial CRD. The collected extracts were evaporated at 60oC; per cent yield and pigment content were calculated. Result: Extract yield and pigment content were significantly influenced by raw material, solid to solvent ratio and duration of extraction. Extract yield was higher in flesh of carrot and beetroot as well as in peels of grape and pomegranate. Anthocyanin content in grape and pomegranate and betalain content in beetroot were high in peel where as β-carotene content was higher in carrot flesh extract. Per cent yield and pigment content increased with increased duration of extraction and solid to solvent ratio. Requirement of more solvent and longer extraction time are the drawback of conventional extraction methods and there is a growing demand for non-conventional techniques to enhance yield and maintain pigment stability.

scholarly journals EXTRACTION OF ANTHOCYANIN PIGMENTS FROM MALABAR SPINACH FRUITS AS A POTENTIAL PHOTOSENSITIZER FOR DYE-SENSITIZED SOLAR CELL

2020 ◽  
pp. 5-9
Author(s):  
GLENNISE FAYE C. MEJICA ◽  
YUWALEE UNPAPROM ◽  
PIYAPIT KHONKAEN ◽  
RAMESHPRABU RAMARAJ
Keyword(s):  
Dye Sensitized Solar Cells ◽  
Natural Dyes ◽  
Synthetic Dyes ◽  
Anthocyanin Pigment ◽  
Dye Sensitized ◽  
Harvesting Efficiency ◽  
Anthocyanin Pigments ◽  
Pure Methanol ◽  
Sensitized Solar Cells ◽  
High Absorption

The implementation of synthetic dyes gives a better efficiency with higher durability; however, the production process of synthesizing these dyes is more complex, expensive, and involves the use of toxic materials. For these reasons, the production of such dyes can pose harm not only to humans but also to the environment. An alternative for the synthetic dyes is the natural dyes or pigment extracted from plants such as anthocyanin, carotenoid, chlorophyll and many others. These natural dyes are easily extracted from various parts of plants, such as from the fruits, flowers, leaves, and seeds. Regardless of the limited performance of natural dyes, the natural dyes exhibit advantages, including high absorption coefficients, highlight-harvesting efficiency, inexpensive, ecologically friendly, non-toxic, and are easily extractable. Moreover, this research paper is mainly focused on about extraction of anthocyanin dye pigments from Malabar spinach fruits for Dye-sensitized solar cells (DSSC). The experiment was conducted using three different methods; extraction of anthocyanin pigments from Malabar spinach fruits: a.) using pure methanol solvent, b.) using 50% methanol solvent, and c.) using 50% methanol & 1% HCl solvent, and the resulted data were 160.81 mg/L, 64.62 mg/L and 77.65 mg/L respectively. It can be concluded that the extraction of anthocyanin pigments from Malabar spinach fruits using pure methanol solvent has the highest amount of extracted anthocyanin pigment, which is 160.81 mg/L.

scholarly journals Study on the extraction of anthocyanin from mangosteen peel Vietnam using supramolecular method

2019 ◽  
Vol 2 (2) ◽  
pp. 130
Author(s):  
Nguyen Hien ◽  
Nguyen Thi Hien ◽  
Hoang Dinh Hoa ◽  
Nguyen Thi Minh Tu
Keyword(s):  
Antioxidant Activity ◽  
Aluminum Chloride ◽  
Solvent Mixture ◽  
Anthocyanin Content ◽  
Garcinia Mangostana ◽  
Scientific Publications ◽  
Tropical Plants ◽  
Practical Applications ◽  
Mangosteen Peel

Mangosteen (Garcinia mangostana Linn) is one of the tropical plants grown in many countries, including Vietnam. This is a fruit of high nutrition value and its fruit peels have been used in many traditional remedies. Many scientific publications showed that mangosteen peel contains active ingredients such as xanthone, anthocynin and tannins in this study, we investigated extraction of anthocyanin from fresh mangosteens’ peel of Vietnam in organic solvent and then isolation by supramolecular method. Antioxidant activity was determined in vitro using DPPH reagent. Using 90% acetonitrile acidified with 1% HCl as a solvent, with a ratio of material to solvent of 3 (v/w) at 4°C for 3.5 hours. Anthocyanin content in the extract reached 0.41% dry matter, antioxidant activity DPPH was 51.28 nmol Trolox/mg. Next, anthocyanin was separated by liquid liquid extraction with a solvent mixture (1 water and 2 dichloromethane) and then isolated by supramolecular method with flavocomelin and aluminum chloride. The results of the anthocyanin isolation test by supersymmetry showed that anthocyanin complexes are formed with flavocomelin and aluminum chloride. That way could separate high purity anthocyanins without sophisticate instruments. The antioxidant activity of the super molar complex was 25.39 nmol Trolox/mg. Practical applications Anthocyanin extracted from peels of mangosteen, can be used afterward for additive in some food application as natural coloring substance and antioxidants for preservation.

scholarly journals Physicochemical Study of Mangosteen (Garcinia mangostana L.) peel Extract as Coloring Agent in Tablet Formulation

2020 ◽  
Vol 3 (1) ◽  
pp. 22-32
Author(s):  
RIDHO ASRA ◽  
Rusdi Rusdi ◽  
Riri Nofrianti
Keyword(s):  
Pharmaceutical Preparations ◽  
Ash Content ◽  
Water Soluble ◽  
Anthocyanin Content ◽  
Garcinia Mangostana ◽  
Total Anthocyanin ◽  
Mangosteen Peel ◽  
Extract Content ◽  
Ftir Spectrophotometry ◽  
Peel Extract

The mangosteen peel (Garcinia mangostana L.) contains anthocyanin pigments, which has an important role in coloring. This study aims to determine the physicochemical properties of mangosteen peel extract (Garcinia mangostana L.) with two methods, which is an examination with UV-Vis and FTIR spectrophotometry. Then the extract was characterized, identified, and analyzed for its stability against temperature, pH, and applied as a coloring agent in the formulation of pharmaceutical preparations (tablets). The results showed that the yield of mangosteen peel extract obtained 13.0975 %, drying losses 5.2822 %, total ash content 14.488 %, acid insoluble ash content 0.684 %, water-soluble extract content 29.58 %, extract content dissolved in ethanol 37.78 %, total anthocyanin content with λmax = 367 nm which is = 9.58 mg / 100 g and with λmax = 289 nm which is = 52.43 mg / 100 g. In this study, the anthocyanin pigment content in mangosteen peel extract cannot be used as an alternative to natural dyes for pharmaceutical preparations (tablets).

scholarly journals EKSTRAKSI PIGMEN ANTOSIANIN DARI KULIT BUAH NAGA MERAH (Hylocereus polyrhizus)

2014 ◽  
Vol 3 (2) ◽  
pp. 25-29
Author(s):  
Lidya Simanjuntak ◽  
Chairina Sinaga ◽  
Fatimah
Keyword(s):  
Citric Acid ◽  
Ph Value ◽  
Extraction Process ◽  
Solvent Mixture ◽  
Extraction Time ◽  
Solvent Ratio ◽  
Distilled Water ◽  
Anthocyanin Pigment ◽  
Anthocyanin Pigments ◽  
Hylocereus Polyrhizus

Extraction of anthocyanin pigments from the red pitaya’s peel (Hylocereus polyrhizus) has been done. Anthocyanin pigment from the red pitaya’s peel (Hylocereus polyrhizus) can be used as an alternative for sinthetys dye. Extraction of anthocyanin pigments in this experiment is using maceration method. There are three independent variables used in this experiment, they are the type of solvent (distilled water, 95% ethanol, ethyl acetate and 10% citric acid), solvent ratios (1:2, 1:3 and 1:4,) and the time of extraction process (1, 2 and 3 days). This experiment aims to determine the right type of solvent, better solvent ratio and better extraction time that used to get anthocyanin pigments from red pitaya’s peel. The measurements in this experiment are based on the pH value, the absorbance value and anthocyanin pigment yield. The experimental results shows that the levels of anthocyanin pigments of red pitaya’s peel dissolved in a solvent mixture of distilled water plus 10% citric acid produce the highest level of anthocyanin pigment yield is 62.68% at pH 2 and the extraction time are 3 days.

scholarly journals Kadar Polifenol Total Ekstrak Etanol Kulit Buah Manggis (Garcinia mangostana) Pada Variasi Asal Daerah

2017 ◽  
Vol 3 (1) ◽  
pp. 22 ◽  
Author(s):  
Any Guntarti
Keyword(s):  
Ethanol Extract ◽  
Total Phenol Content ◽  
Ammonia Vapor ◽  
Phenol Content ◽  
Garcinia Mangostana ◽  
Mangosteen Peel ◽  
Fruit Skin ◽  
Specific Parameter ◽  
Qualitative Test ◽  
Parameter Test

Background:Mangosteen peel is one of the waste of mangosteen, that nowadays have already utilized much to manage health problems. One of the ingredients in the mangosteen fruit skin is a polyphenols. Objective: to determine the polyphenols content of the ethanol extract of mangosteen peel variations based on different regions. Methods: Powder of dried mangosteen peel that come from 3 difference areas, Sumatera (Pekanbaru), Jawa (Yogyakarta) and Kalimantan (Martapura) extracted with ethanol 70% by multilevel maceration. Extract that obtained than tested specific parameter form of qualitative test of polyphenols compounds with FeCl3, AlCl3, ammonia vapor, Folin Ciucalteau and tannin test. Determination level of polyphenols (Gallic acid) with visible spectrophotometri after reacted with Folin Ciucalteau reagent. Results: The result of this research was quality test of extract etanol 70% Specific parameter test total phenol content (mg GAE/g ekstrak) from Sumatera, Jawa and Kalimantan are :824.13 (mg GAE/g ekstrak); 155,86 (mg GAE/g ekstrak); 688,9 (mg GAE/g ekstrak). Conclusions: There were difference in contents of polyphenol of mangosteen peel origin among Sumatera, Jawa and Kalimantan. 

scholarly journals FORMULASI NANOEMULGEL EKSTRAK KULIT MANGGIS (Garcinia Mangostana L.)

2019 ◽  
Vol 1 (3) ◽  
pp. 166-176
Author(s):  
Hilda Damayanti ◽  
Saleh Wikarsa ◽  
Garnadi Jafar
Keyword(s):  
Antioxidant Activity ◽  
Particle Size ◽  
Particle Size Analysis ◽  
Size Analysis ◽  
Garcinia Mangostana ◽  
Mangosteen Peel ◽  
Dpph Method ◽  
Nanoemulsion Gel ◽  
Materials Used ◽  
Peel Extract

Antioxidant-containing cosmetic has antiaging therapy that can inhibit the free radical formation. Mangosteen peel extract has very strong antioxidant activity. To enhance the effect and comfortness of mangosteen peel extract use on the skin, it could be made into nanoemulgel. The article provides the information about method of preparation and evaluation of nanoemulsion-gel. The purpose of this study was to formulate a stable microemulgel of mangosteen peel extractusing halal materials declared halal according to Islamic Shari’a.  the materials used don’t contain carrion, blood, pig and/ animals that don’t conform to Islamic Shari’a. Microemulgel mangosteen peel extract was made by varying plantacare® 1200 UP concentration as cosurfactant (5, 10, 15, 20 and 25%) in the microemulsion and it was incorporated into the gel base. Evaluations were included the antioxidant activity test and organoleptic, pH, viscosity, stability, particle size analysis and panelist test. The antioxidant activity determined by DPPH method showed that IC50 value of mangosteen peel extract was 5.54 ppm. The third microemulsion formula containing cosurfactant of 15% resulted in the best results in that the parameter of the product can be penetrated by ray laser was at particle size of  23.65 nm, was determined by tranmission Electron Microscopy (TEM). Microemulgel containing Viscolam® MAC 10 of seven percent gave the stable formula proofed by freeze thaw and sentrifuga test. The five microemulgel formulations were stable.    

scholarly journals Methanol extract of mangosteen peel (Garcinia mangostana L.) increase activity acetylcholinesterase and glutathione peroxidase and reduce MDA in diazinon exposed rat

2018 ◽  
Vol 7 (3) ◽  
Author(s):  
I Gusti Ayu Kunti Sri Panca Dewi ◽  
Ida Bagus Putra Manuaba ◽  
I Wayan Putu Sutirta Yasa ◽  
Bagus Komang Satriyasa
Keyword(s):  
Glutathione Peroxidase ◽  
Methanol Extract ◽  
Garcinia Mangostana ◽  
Mangosteen Peel

scholarly journals PRODUKSI ANTOSIANIN DARI DAUN MIANA (Plectranthus scutellarioides) SEBAGAI PEWARNA ALAMI

Pro Food ◽  
2018 ◽  
Vol 4 (1) ◽  
pp. 298-303
Author(s):  
Dhanang Puspita ◽  
Yosephine Diana Tjahyono ◽  
Yunius Samalukang ◽  
Binerd Anthon Im Toy ◽  
Norson Willem Totoda
Keyword(s):  
Food Industry ◽  
Heat Exposure ◽  
Ornamental Plant ◽  
Anthocyanin Pigment ◽  
Natural Pigment ◽  
Single Leaf ◽  
Maximum Absorbance ◽  
Exposure Temperature ◽  
Anthocyanin Pigments ◽  
Purple Color

Miana (Coleus scutellaroides) is an ornamental plant of single leaf a purple color. The purple color found from miana leaves is an indicator of the presence of anthocyanin pigments. Anthocyanin from miana leaves can be utilized as a natural pigment for various staining purposes especially in the food industry, anthocyanin harvesting on miana leaves can be done at any time and does not depend on the season due to its abundant availability in nature.The aims of this study were to isolate, identify, and microencapsulated anthocyanin pigments of miana leaves. The result, pigment extracted from miana leaves had characteristic of purple color and having maximum absorbance at wavelength 529 nm, suspected as anthocyanin derivative (cyanidin-3-routosida).The total microcapsulated anthocyanim was 0.149542 mg / g. Thermostability of encapsulated anthocyanin pigment from miana leaves stable with heat exposure temperature 100C up to 60 minutes. Based on those collected information, encapsulated miana leaves pigment could be used as an additional natural coloring in food industries.Keywords: anthocyanin, miana, microencapsulation, pigment, thermostability. ABSTRAKMiana (Coleus scutellaroides) termasuk ke dalam tanaman hias yang berdaun tunggal dan berwarna ungu. Warna ungu yang terdapat pada daun miana adalah indikator keberadaan pigmen antosianin.Pemanfaatan daun miana sebagai sumber antosianin dapat dimanfaatkan sebagai pigmen alami untuk berbagai keperluan pewarna terutama dalam industri pangan, pemanenan antosianin pada daun miana dapat dilakukan setiap saat dan tidak bergantung pada musim dikarenakan ketersediannya yang selalu melimpah di alam.Tujuan dari penelitian ini adalah untuk mengisolasi, mengidentifikasi, dan mikroenkapsulasi pigmen antosianin dari daun miana.Berdasarkan hasil analisis didapati bahwa ekstrak pigmen daun miana memiliki karakteristik warna nampak ungu dan serapan maksimum absorbansinya berada pada panjang gelombang 529 nm, pigmen diduga sebagai turunan antosianin yaitu sianidin-3-rutinosida.Total antosianim yang sudah dimikroenkapsulasi sebesar 0.149542 mg/g. Dari hasil uji thermostabilitas pigmen terenkapsulasi maltodekstrin, stabilitas pigmen antosianin dari daun miana cenderung stabil dengan adanya pemaparan panas suhu 100C hingga 60 menit.Berdasarkan hasil dan pengujian, pigmen daun miana terenkapsulasi dapat menjadi pertimbangan produk untuk digunakan sebagai bahan tambahan pewarna dalam industri pangan.Kata kunci: antosianin, miana, mikroenkapsulasi, pigmen, termostabilitas.

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