scholarly journals Effects of Austenitizing Temperature on Tensile and Impact Properties of a Martensitic Stainless Steel Containing Metastable Retained Austenite

Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 1000
Author(s):  
Biao Deng ◽  
Dapeng Yang ◽  
Guodong Wang ◽  
Ziyong Hou ◽  
Hongliang Yi

Austenitizing temperature is one decisive factor for the mechanical properties of medium carbon martensitic stainless steels (MCMSSs). In the present work, the effects of austenitizing temperature (1000, 1020, 1040 and 1060 °C) on the microstructure and mechanical properties of MCMSSs containing metastable retained austenite (RA) were investigated by means of electron microscopy, X-ray diffraction (XRD), as well as tensile and impact toughness tests. Results suggest that the microstructure including an area fraction of undissolved M23C6, carbon and chromium content in matrix, prior austenite grain size (PAGS), fraction and composition of RA in studied MCMSSs varies with employed austenitizing temperature. By optimizing austenitizing temperature (1060 °C for 40 min) and tempering (250 °C for 30 min) heat treatments, the MCMSS demonstrates excellent mechanical properties with the ultimate tensile strength of 1740 ± 8 MPa, a yield strength of 1237 ± 19 MPa, total elongation (ductility) of 10.3 ± 0.7% and impact toughness of 94.6 ± 8.0 Jcm−2 at room temperature. The increased ductility of alloys is mainly attributed to the RA with a suitable stability via a transformation-induced plasticity (TRIP) effect, and a matrix containing reduced carbon and chromium content. However, the impact toughness of MCMSSs largely depends on M23C6 carbides.

Metals ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 978 ◽  
Author(s):  
Pengfei Wang ◽  
Zhaodong Li ◽  
Guobiao Lin ◽  
Shitong Zhou ◽  
Caifu Yang ◽  
...  

Steels used for high-speed train wheels require a combination of high strength, toughness, and wear resistance. In 0.54% C-0.9% Si wheel steel, the addition of 0.075 or 0.12 wt % V can refine grains and increase the ferrite content and toughness, although the influence on the microstructure and toughness is complex and poorly understood. We investigated the effect of 0.03, 0.12, and 0.23 wt % V on the microstructure and mechanical properties of medium-carbon steels (0.54% C-0.9% Si) for train wheels. As the V content increased, the precipitation strengthening increased, whereas the grain refinement initially increased, and then it remained unchanged. The increase in strength and hardness was mainly due to V(C,N) precipitation strengthening. Increasing the V content to 0.12 wt % refined the austenite grain size and pearlite block size, and increased the density of high-angle ferrite boundaries and ferrite volume fraction. The grain refinement improved the impact toughness. However, the impact toughness then reduced as the V content was increased to 0.23 wt %, because grain refinement did not further increase, whereas precipitation strengthening and ferrite hardening occurred.


2019 ◽  
Vol 9 (20) ◽  
pp. 4231
Author(s):  
Oskari Haiko ◽  
Antti Kaijalainen ◽  
Sakari Pallaspuro ◽  
Jaakko Hannula ◽  
David Porter ◽  
...  

In this paper, the effects of different tempering temperatures on a recently developed ultrahigh-strength steel with 0.4 wt.% carbon content were studied. The steel is designed to be used in press-hardening for different wear applications, which require high surface hardness (650 HV/58 HRC). Hot-rolled steel sheet from a hot strip mill was austenitized, water quenched and subjected to 2-h tempering at different temperatures ranging from 150 °C to 400 °C. Mechanical properties, microstructure, dislocation densities, and fracture surfaces of the steels were characterized. Tensile strength greater than 2200 MPa and hardness above 650 HV/58 HRC were measured for the as-quenched variant. Tempering decreased the tensile strength and hardness, but yield strength increased with low-temperature tempering (150 °C and 200 °C). Charpy-V impact toughness improved with low-temperature tempering, but tempered martensite embrittlement at 300 °C and 400 °C decreased the impact toughness at −40 °C. Dislocation densities as estimated using X-ray diffraction showed a linear decrease with increasing tempering temperature. Retained austenite was present in the water quenched and low-temperature tempered samples, but no retained austenite was found in samples subjected to tempering at 300 °C or higher. The substantial changes in the microstructure of the steels caused by the tempering are discussed.


Metals ◽  
2019 ◽  
Vol 9 (10) ◽  
pp. 1066 ◽  
Author(s):  
Koh-ichi Sugimoto ◽  
Sho-hei Sato ◽  
Junya Kobayashi ◽  
Ashok Kumar Srivastava

In this study, the effects of Cr and Mo additions on mechanical properties of hot-forged medium carbon TRIP-aided bainitic ferrite (TBF) steel were investigated. If 0.5%Cr was added to the base steel with a chemical composition of 0.4%C, 1.5%Si, 1.5%Mn, 0.5%Al, and 0.05%Nb in mass%, the developed steel achieved the best combination of strength and total elongation. The best combination of strength and impact toughness was attained by multiple additions of 0.5%Cr and 0.2%Mo to the base steel. The excellent combination of strength and impact toughness substantially exceeded those of quenched and tempered JIS-SCM420 and 440 steels, although it was as high as those of 0.2%C TBF steels with 1.0%Cr and 0.2%Mo. The good impact toughness was mainly caused by uniform fine bainitic ferrite matrix structure and a large amount of metastable retained austenite.


2017 ◽  
Vol 898 ◽  
pp. 772-777
Author(s):  
Jia Xing Wang ◽  
Xu Ming Wang ◽  
Hui Guo ◽  
Ai Min Zhao ◽  
Liu Wei

The tensile and impact tests were used to study the mechanical properties under different temperatures of 300 mm large-scale angle steel at different positions, especially the tensile strength, yield strength, total elongation and impact toughness in the range of-40 oC to 20 oC. The results showed that different regions had great differences in the microstructures and impact toughness, in which the size of edge region was the smallest and the impact toughness was the best. However, the coarsened grain of heat affected zone at weld region had deteriorated to the low temperature impact toughness. When the impact energy was 34 J, the ductile-brittle transition temperature of weld, center, vertex and edge were-7.2 oC, -33.0 oC, -31.5 oC and far less than-40 oC, respectively. Meanwhile, because the banded structure was detrimental to the ductility, the elongation of rolling direction was lower than vertical direction. The strength of weld region was higher than other locations, but the elongation was obviously decreased.


2011 ◽  
Vol 299-300 ◽  
pp. 57-60
Author(s):  
De Qiang Wei ◽  
Ke Liu

The low alloyed bainite ductile iron is obtained by alloying and austempering in room-temperature machine oil. The microstructure is investigated. The mechanical properties are discussed. In general, the number of white-bright zones and segregation is increasing with the increasing in the content of Mn, but the impact toughness is decreased. Therefore, the content of Mn is no more than 0.5 wt.%. The microstructure of bainite, martensite and a little retained austenite in the matrix of the ductile iron was investigated by scanning electron microscope (SEM). The hardness and impact toughness of the ductile iron subjected to heat-treatment are 54~56 HRC and 14.2 J/cm2, respectively. The substitution of 0.3~0.5wt.% Mo by 0.7~1.0 wt.% Mn can be realized in the bainite ductile iron.


Metals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1133 ◽  
Author(s):  
Zhang ◽  
Zhao ◽  
Tan ◽  
Ji ◽  
Xiang

The relationship between microstructure parameters and mechanical properties was studied in this paper. The steel was heat-treated at different austenitizing temperatures to acquire varying microstructure. The results showed that austenite grain size increases with austenitizing temperature, while the pearlite colony size was relatively constant. The strength followed a Hall–Petch relationship with the austenite grain size, but the austenite grain size has nothing to do with the impact toughness. The control unit for determining the impact toughness of pearlitic steel is the pearlite colony size using a comparison method. Further studies have found that, in the hypoeutectoid steel and hypereutectoid steel, the pearlite colony size changes with the austenitizing temperature. However, when the eutectoid steel with a carbon content of 0.81% undergoes the isothermal transformation, the number of grain boundary precipitates is very few. There are many nucleation sites at the grain boundary. The pearlite colonies randomly nucleate at the grain boundaries and grow into the interior of the grains. Simultaneously, new pearlite colonies nucleate by the side of the existing pearlite colony. The intragranular pearlite colonies are also randomly nucleated. These nucleation sites increase the chance of the growing pearlite colonies colliding with each other, eventually resulting in a constant pearlite colony size.


2012 ◽  
Vol 445 ◽  
pp. 195-200
Author(s):  
Murat Aydin ◽  
Yakup Heyal

The mechanical properties mainly tensile properties, impact toughness and high-cycle fatigue properties, of two-phase Al-20Zn alloy subjected to severe plastic deformation (SPD) via equal-channel angular extrusion (ECAE) using route A up to 2 passes were studied. The ECAE almost completely eliminated as-cast dendritic microstructure including casting defects such as micro porosities. A refined microstructure consisting of elongated micro constituents, α and α+η eutectic phases, formed after ECAE via route A. As a result of this microstructural change, mechanical properties mainly the impact toughness and fatigue performance of the as-cast Al-20Zn alloy increased significantly through the ECAE. The rates of increase in fatigue endurance limit are approximately 74 % after one pass and 89 % after two passes while the increase in impact toughness is 122 %. Also the yield and tensile strengths of the alloy increase with ECAE. However, no considerable change occurred in hardness and percentage elongation of the alloy. It was also observed that the ECAE changed the nature of the fatigue fracture characteristics of the as-cast Al-20Zn alloy.


2013 ◽  
Vol 762 ◽  
pp. 551-555 ◽  
Author(s):  
Marek Stanislaw Węglowski ◽  
Marian Zeman ◽  
Miroslaw Lomozik

In the present study, the investigation of weldability of new ultra-high strength - Weldox 1300 steel has been presented. The thermal simulated samples were used to investigate the effect of welding cooling time t8/5 on the microstructure and mechanical properties of the heat affected zone (HAZ). In the frame of these investigation the microstructure was studied by the light (LM) and transmission electron microscopies (TEM). It has been shown that the microstructure of the Weldox 1300 steel is composed of tempered martensite, and inside the laths the minor precipitations mainly V(CN) and molybdenum carbide Mo2C were observed. Mechanical properties of parent material were analysed by the tensile, impact and hardness tests. In details the influence of cooling time in the range of 2,5 - 300 s. on hardness, impact toughness and microstructure of simulated HAZ was studied by using welding thermal simulation test. The results show that the impact toughness and hardness decrease with the increase of t8/5 under the condition of a single thermal cycle in simulated HAZ. The continuous cooling transformation diagrams (CCT-W for welding conditions) of Weldox 1300 steel for welding purposes was also elaborated. The steel Weldox 1300 for cooling time in the range of 2,5 - 4 s showed martensite microstructure, for time from 4 s to 60 s mixture of martensite and bainite, and for longer cooling time mixture of ferrite, bainite and martensite. The results indicated that the weldability of Weldox 1300 steel is limited and to avoid the cold cracking the preheating procedure or medium net linear heat input should be used.


2014 ◽  
Vol 1082 ◽  
pp. 202-207 ◽  
Author(s):  
Shu Yan ◽  
Xiang Hua Liu

A low carbon steel was treated by quenching and partitioning (Q&P) process, and a detailed characterization of the microstructural evolution and testing of mechanical properties were carried out. The resulted mechanical properties indicate that with the partitioning time increasing, the tensile strength decreases rapidly first and then remains stable, and the total elongation increases first then decreases. The investigated steel subjected to Q&P process exhibits excellent products of strength and elongation (17.8-20.6 GPa•%). The microstructural evolution of martensite matrix during the partitioning step was observed, and the morphology and content of retained austenite were characterized. The working hardening behavior of the samples was analyzed, and the retained austenite with higher carbon content contributes to the uniform elongation more effectively.


2011 ◽  
Vol 239-242 ◽  
pp. 1092-1095
Author(s):  
Xu Tao Gao ◽  
Ai Min Zhao ◽  
Zheng Zhi Zhao ◽  
Ming Ming Zhang ◽  
Di Tang

By means of optical microscopy(OM), scanning electron microscopy(SEM),X-ray diffraction(XRD),And tensile test, Mechanical Properties of hot rolled transformation -induced plasticity (TRIP) steels which were prepared through three different coiling temperature was investigated. Result reveals that the formability index of the experimental steel descends when the coiling temperature becomes low. Different coiling temperature has greater impact on retained austenite. Amount and carbon content of retained austenite in the experimental steel get less with lower coiling temperature.


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