scholarly journals High-Fluidization, Early Strength Cement Grouting Material Enhanced by Nano-SiO2: Formula and Mechanisms

Materials ◽  
2021 ◽  
Vol 14 (20) ◽  
pp. 6144
Author(s):  
Jiaolong Ren ◽  
Zedong Zhao ◽  
Yinshan Xu ◽  
Siyuan Wang ◽  
Haiwei Chen ◽  
...  
Keyword(s):  
Functional Requirements ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Rapid Repair ◽  
Nano Sio2 ◽  
Civil Infrastructures ◽  
Cement Grouting ◽  
Grouting Material ◽  
Early Strength ◽  
Grouting Materials

Cement grouting material is one of the most important materials in civil construction at present, for seepage prevention, rapid repair, and reinforcement. To achieve the ever-increasing functional requirements of civil infrastructures, cement grouting materials must have the specific performance of high fluidization, early strength, and low shrinkage. In recent years, nanomaterials have been widely used to improve the engineering performance of cement grouting materials. However, the mechanisms of nanomaterials in grouting materials are not clear. Hence, a high-fluidization, early strength cement grouting material, enhanced by nano-SiO2, is developed via the orthogonal experimental method in this study. The mechanisms of nano-SiO2 on the microstructure and hydration products of the HCGA, in the case of different curing ages and nano-SiO2 contents, are analyzed through scanning electron microscopy tests, X-ray diffraction tests, differential scanning calorimetry tests, and Fourier transform infrared spectroscopy tests.

Study of Rheological Properties of Carbon Nanotube-Reinforced Ultrafine Cement Grouting Materials

2021 ◽  
pp. 1-44
Author(s):  
Yunxiao Liu ◽  
Jiahang Zhang ◽  
Yinyin Chi
Keyword(s):  
Carbon Nanotubes ◽  
Rheological Properties ◽  
Polyvinyl Pyrrolidone ◽  
Cement Grouting ◽  
Grouting Material ◽  
Multi Walled Carbon Nanotubes ◽  
Different Diameters ◽  
Grouting Materials ◽  
Walled Carbon Nanotubes ◽  
Ultrafine Cement

In this study, three different diameters of multi-walled carbon nanotubes (MWCNTs) dispersed by polyvinyl pyrrolidone (PVP) were used to reinforce superfine cement grouting materials. The effect of MWCNTs and polyvinyl pyrrolidone (PVP) on the rheological properties of grouting material were accordingly studied. It was found that the yield stress (τ0) and plastic viscosity (η) were slightly decreased when PVP content was low and increased when the PVP content increased. The effect of MWCNT diameter on τ0 was not found to be clear but was more significant on η. The smaller MWCNT diameter was, the more quickly η increase. It was also found that the thixotropic ring area was increased as the MWCNTs content increased. The addition of PVP and MWCNTs caused an increase in the number of entanglement points in different scales, which was the main reason for the viscosity and thixotropy increase. Therefore, the rheological properties of superfine cement grouting material should be adjusted when MWCNTs were added as a reinforcing component. Due to the wrapping of PVP on cement particles which isolates the contacting part between the water and the cement particles, it slows down the cement's hydration rate thus slows down the fluidity loss of the slurry.

Study on Microfine Cement Grouting Material for Silty Fine Sand Stratum

2013 ◽  
Vol 838-841 ◽  
pp. 1457-1462
Author(s):  
Chun Lei Xia ◽  
Ying Ye ◽  
Guan Ming Wang ◽  
Li Cui
Keyword(s):  
Portland Cement ◽  
Particle Diameter ◽  
Fine Sand ◽  
Cement Grouting ◽  
Grouting Material ◽  
Soluble Glass ◽  
Microfine Cement ◽  
Sand Flow ◽  
Sand Stratum ◽  
Grouting Materials

Silty fine sand is the second smallest sand with a particle diameter ranging from 0.0625 to 0.120 mm.This kind of sand exists in a large amount in Beijing subway excavation project. Due to the poor self-stabilization of this stratum,seeping , sand flow and collapse take place frequently. Grouting materials such as Portland cement and soluble glass (also called sodium silicate) are employed in most of excavation projects to reinforce this sand stratum. However, the reinforcement is not effective, leading to a large amount of accidents in the process of construction. The reason may be attributed to the fact that Portland cement is unable to penetrate into the stratum and the strength of soluble glass (0.6MPa) is too weak to resist the stratum pressure. To solve this problem, a modified microfine cement grouting material able to penetrate into silty fine sand stratum is developed in this paper. A combination of suspension and diluent is used to increase the penetration extension of the grouts,and the experimental results reveal that the addition of the mixture of suspension and diluent in microfine cement grouting materials improves the penetration property substantially.

Research on Multivariate Composite Super early Strength Grouting Materials

2013 ◽  
Vol 477-478 ◽  
pp. 990-995
Author(s):  
Xiao Ping Zhang ◽  
Chang Zheng Sun ◽  
Tong Feng Zhao
Keyword(s):  
Compressive Strength ◽  
High Performance ◽  
Ordinary Portland Cement ◽  
High Alumina ◽  
Flow Ratio ◽  
Initial Flow ◽  
Growth Structure ◽  
Grouting Material ◽  
Early Strength ◽  
Grouting Materials

Super early strength high performance grouting material was produced using high alumina cement, ordinary portland cement, gypsum and silica fume. The different glue sand ratio and the cement sand ratio 1.0 mix microstructure were studied systematically. The results showed that the system with a variety of admixture using hingh mortar ratio can be prepared for the initial flow ratio greater than 325{mm},, 30min flow greater than 280{mm}, 2h compressive strength 34.80{MPa}, 24h bending over 13.82{MPa}, 28d compressive strength greater than 99.90{MPa}, 28d compressive strength greater than 56d compressive strength. The system of early SEM microstructures showed good crystal growth, structure compact.

scholarly journals Effects of Aluminum Sulfate and Quicklime/Fluorgypsum Ratio on the Properties of Calcium Sulfoaluminate (CSA) Cement-Based Double Liquid Grouting Materials

Materials ◽  
2019 ◽  
Vol 12 (8) ◽  
pp. 1222 ◽  
Author(s):  
Yuli Wang ◽  
Jie Yu ◽  
Junjie Wang ◽  
Xuemao Guan
Keyword(s):  
Compressive Strength ◽  
Aluminum Sulfate ◽  
Setting Time ◽  
Strength Properties ◽  
X Ray Diffraction ◽  
Cement Slurry ◽  
Calcium Sulfoaluminate ◽  
Optimum Content ◽  
Grouting Material ◽  
Grouting Materials

Grouting materials are used frequently in grouting reinforcement projects, such as mining and coastal engineering. Double liquid grouting materials are mostly used because of the fast setting and high early strength properties when the two slurries are mixed together but high fluidity when the two slurries are separated. In our study, double liquid grouting materials were developed from CSA cement (slurry A), quicklime and fluorgypsum (slurry B). Aluminum sulfate was added in slurry B in order to counteract any adverse effects caused by the fluorgypsum, such as the decreased early compressive strength and the prolonged setting time. The effects of aluminum sulfate content and the quicklime/fluorgypsum ratio on the setting time, hydration heat, and compressive strength of the double liquid grouting materials were investigated, and the hydration products were characterized through thermogravimetry-differential thermal analysis (TG-DTA), X-ray Diffraction (XRD), and Scanning Electron Microscope (SEM) tests. The results show that the addition of aluminum sulfate can shorten the setting time and increase compressive strength at both early and later ages. Considering the setting time and compressive strength of double liquid grouting material at the same time, the optimum content of aluminum sulfate was found to be 2%, and the optimum ratio of quicklime/fluorgypsum was found to be 2:8. The values of the optimum content of aluminum sulfate and ratio of quicklime/fluorgypsum were verified from theoretical analysis.

scholarly journals Experimental Study of Cement Alkali-Resistant Glass Fiber (C-ARGF) Grouting Material

Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 605 ◽  
Author(s):  
Zhenyue Shi ◽  
Qingbiao Wang ◽  
Lei Xu
Keyword(s):  
Tensile Strength ◽  
Compressive Strength ◽  
Flexural Strength ◽  
Glass Fiber ◽  
High Strength ◽  
Strength Ratio ◽  
Karst Tunnel ◽  
Grouting Material ◽  
Early Strength ◽  
Grouting Materials

Mixing alkali-resistant glass fiber (ARGF) into grouting slurry can prevent the development of cracks; thus, understanding the properties of ARGF grouting material is important for applications in engineering. Two types of ARGFs (Cem-FIL®60 and Anti-Crak®HD) were selected as mixing materials, and their performance was tested in four areas, namely, compressive strength, tensile strength, flexural strength, and impervious performance, under four different mixing amounts of fiber (0%, 0.25%, 0.5%, and 1.0%). Results demonstrate that the addition of ARGF increased the compressive strength and tensile strength of the grouting slurry, and the best performance was at 0.5%. The effect on the flexural strength and impervious performance was related to the mixing amount, and the fiber may have induced a counter-effect for certain amounts of added ARGF. Mixing ARGF could increase the early strength ratio of grout; however, a high early strength ratio did not necessarily result in high strength, as the flexural strength did not change synchronously with the early strength ratio; a similar pattern was found for the impermeability. Cem-FIL®60 had a better effect on the properties of grouting materials than Anti-Crak®HD. These results were successfully applied in the water-plugging and reinforcement engineering of a karst tunnel.

Research on Grouting Materials for Underground Construction Projects

2021 ◽  
Vol 1036 ◽  
pp. 319-326
Author(s):  
Hao Ran Duan ◽  
Peng Zhao ◽  
Lei Qin ◽  
Feng Jiao Shi
Keyword(s):  
Environmental Pollution ◽  
Large Scale ◽  
Raw Materials ◽  
Development Trend ◽  
Engineering Practice ◽  
Underground Engineering ◽  
Chemical Grouting ◽  
Cement Grouting ◽  
Grouting Material ◽  
Grouting Materials

The engineering practice shows that the application of grouting technology to treat underground engineering has strong applicability and is one of the most commonly used technical means at present. Based on the underground engineering, this paper introduces the research achievements of grouting materials in recent years, including cement-based grouting materials, mixed grouting materials, anti-scouring grouting materials, and ultra-fine cement grouting materials. Current demand of grouting materials in underground engineering, there exists large dosage of cement, high content, high cost, serious environmental pollution problems, such as looking for alternatives or mixed with other raw materials for preparation of cementation material become the development trend, compared with the cement grouting material, chemical grouting material with higher performance, but in smaller projects within the scope of application. How to reduce the production cost of chemical grouting materials, simplify the production process, overcome the existing toxicity, reduce environmental pollution and improve the durability of solidified body has become the bottleneck of its popularization and application. Some achievements have been made in the modification of cement or chemical materials by nanometer components, but there is still a long way to go before the large-scale application of grouting engineering.

SEM and XRD Investigation on Mechanism of Expansion and High-Early-Strength of a Cementitious Composited Grouting Material

2011 ◽  
Vol 194-196 ◽  
pp. 1099-1102
Author(s):  
Guo Chen Sang ◽  
Hao Bo Zhang ◽  
Yi Yun Zhu
Keyword(s):  
Calcium Sulfate ◽  
Ordinary Portland Cement ◽  
Expansion Ratio ◽  
X Ray Diffraction ◽  
Microstructural Study ◽  
X Ray ◽  
Ettringite Formation ◽  
Grouting Material ◽  
Early Strength ◽  
Aluminate Cement

In this paper, an innovative research on mechanism of a non-shrinkage and high early strength composited cements-based grouting material is presented. A blend cements system of ordinary Portland cement (OPC), calcium aluminate cement (CAC) and calcium sulfate (CS) were used in the innovative grouting material. Through the systemic studies on the influence of the constituents on properties of the grouts and microstructural study by Scanning Electron Microscopy (SEM) and X-ray Diffraction (XRD), experimental results show that the development of the compressive strength and expansion ratio in hydrated cementitious grouts resulted from ettringite formation and quantity of ettringite crystals in the cementitious grouts.

Glibenclamide-Nicotinamide Cocrystals Synthesized by The Solvent Evaporation Method to Enhance Solubility and Dissolution Rate of Glibenclamide

2019 ◽  
Vol 9 (01) ◽  
pp. 21-26
Author(s):  
Arif Budiman ◽  
Ayu Apriliani ◽  
Tazyinul Qoriah ◽  
Sandra Megantara
Keyword(s):  
Solvent Evaporation ◽  
Physical Mixture ◽  
Dissolution Profile ◽  
Solvent Evaporation Method ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Evaporation Method ◽  
Dissolution Properties ◽  
Mixture Characterization

Purpose: To develop glibenclamide-nicotinamide cocrystals with the solvent evaporation method and evaluate their solubility and dissolution properties. Methods: Cocrystals of glibenclamide-nicotinamide (1:2) were prepared with the solvent evaporation method. The prediction of interactive cocrystals was observed using in silico method. The solubility and dissolution were performed as evaluation of cocrystals. The cocrystals also were characterized by differential scanning calorimetry (DSC), infrared spectrophotometry, and powder X-ray diffraction (PXRD). Result: The solubility and dissolution profile of glibenclamide-nicotinamide cocrystal (1:2) increased significantly compared to pure glibenclamide as well as its physical mixture. Characterization of cocrystal glibenclamide-nicotinamide (1:2) including infrared Fourier transform, DSC, and PXRD, indicated the formation of a new solid crystal phase differing from glibenclamide and nicotinamide. Conclusion: The confirmation of cocrystal glibenclamide-nicotinamide (1:2) indicated the formation of new solid crystalline phases that differ from pure glibenclamide and its physical mixture

Studies on the Preparation, Characterization and Solubility of -Cyclodextrin-Roxythromycin Inclusion Complexes

2009 ◽  
Vol 2 (2) ◽  
pp. 523-530
Author(s):  
D. Nagasamy Venkatesh ◽  
S. Karthick ◽  
M. Umesh ◽  
G. Vivek ◽  
R.M. Valliappan ◽  
...  
Keyword(s):  
Dissolution Rate ◽  
Inclusion Complexes ◽  
Phase Solubility ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Ir Studies ◽  
Poorly Soluble ◽  
Poorly Soluble Drug

Roxythromycin/ β-cyclodextrin (Roxy/ β-CD) dispersions were prepared with a view to study the influence of β-CD on the solubility and dissolution rate of this poorly soluble drug. Phase-solubility profile indicated that the solubility of roxythromycin was significantly increased in the presence of β-cyclodextrin and was classified as AL-type, indicating the 1:1 stoichiometric inclusion complexes. Physical characterization of the prepared systems was carried out by differential scanning calorimetry (DSC), X-ray diffraction studies (XRD) and IR studies. Solid state characterization of the drug β-CD binary system using XRD, FTIR and DSC revealed distinct loss of drug crystallinity in the formulation, ostensibly accounting for enhancement of dissolution rate.

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