New Features for Damage Detection and Their Temperature Stability

Author(s):  
Fahit Gharibnezhad ◽  
Luis Eduardo Mujica Delgado ◽  
Jose Rodellar

This chapter is devoted to present novel techniques in Structural Health Monitoring (SHM). These techniques are based on different statistical and signal processing methods that are used in other fields but their performance and capability in SHM is presented and tested for the first time in this work. This work is dedicated to the first level of SHM, which might be considered the main and most important level. Piezoceramic (PZT) devices are chosen in this work to capture the signals due to their special characteristics such as high performance, low energy consumption and reasonable price. Suggested techniques are tested on different laboratory and real scale test benchmarks. Moreover, this work considers the effect of environmental changes on performance of the presented techniques. This work shows that although those techniques have a significant result in normal conditions, their performance can be affected by any environmental discrepancy such as temperature change. As such, there is a vital need to consider their effect. In this work, temperature change is chosen, as it is one of the main environmental fluctuation factors.

2020 ◽  
pp. 659-696
Author(s):  
Fahit Gharibnezhad ◽  
Luis Eduardo Mujica Delgado ◽  
Jose Rodellar

This chapter is devoted to present novel techniques in Structural Health Monitoring (SHM). These techniques are based on different statistical and signal processing methods that are used in other fields but their performance and capability in SHM is presented and tested for the first time in this work. This work is dedicated to the first level of SHM, which might be considered the main and most important level. Piezoceramic (PZT) devices are chosen in this work to capture the signals due to their special characteristics such as high performance, low energy consumption and reasonable price. Suggested techniques are tested on different laboratory and real scale test benchmarks. Moreover, this work considers the effect of environmental changes on performance of the presented techniques. This work shows that although those techniques have a significant result in normal conditions, their performance can be affected by any environmental discrepancy such as temperature change. As such, there is a vital need to consider their effect. In this work, temperature change is chosen, as it is one of the main environmental fluctuation factors.


2019 ◽  
Author(s):  
Kent Griffith ◽  
Clare Grey

Nb18W8O69 (9Nb2O5×8WO3) is the tungsten-rich end-member of the Wadsley–Roth crystallographic shear (cs) structures within the Nb2O5–WO3 series. It has the largest block size of any known, stable Wadsley–Roth phase, comprising 5 ´ 5 units of corner-shared MO6 octahedra between the shear planes, giving rise to 2 nm ´ 2 nm blocks. Rapid lithium intercalation is observed in this new candidate battery material and 7Li pulsed field gradient nuclear magnetic resonance spectroscopy – measured in a battery electrode for the first time at room temperature – reveals superionic lithium conductivity. In addition to its promising rate capability, Nb18W8O69 adds a piece to the larger picture of our understanding of high-performance Wadsley–Roth complex metal oxides.


2019 ◽  
Vol 15 (6) ◽  
pp. 568-573
Author(s):  
Soheil Sedaghat ◽  
Ommoleila Molavi ◽  
Akram Faridi ◽  
Ali Shayanfar ◽  
Mohammad Reza Rashidi

Background: Signal transducer and activator of transcription 3 (STAT3), an oncogenic protein found constitutively active in many types of human malignancies, is considered to be a promising target for cancer therapy. Objective: In this study for the first time, a simple and accurate method has been developed for the determination of a STAT3 dimerization inhibitor called stattic in aqueous and plasma samples. Methods: A reverse-phase high-performance liquid chromatography (RP-HPLC) composed of C18 column as stationary phase, and the mixture of acetonitrile (60%) and water (40%) as mobile phase with a UV detection at 215 nm were applied for quantification of stattic. The developed method was validated by Food and Drug Administration (FDA) guideline. Results: The method provided a linear range between 1-40 and 2.5-40 µg mL-1 for aqueous and plasma samples, respectively, with a correlation coefficient of 0.999. The accuracy (as recovery) of the developed method was found to be between 95-105% for aqueous medium and 85-115% for plasma samples. The precision (as relative standard deviation) for aqueous and plasma samples was less than 6% and 15%, respectively. The sensitivity of the developed method based on FDA guideline was 1 µg mL-1 for aqueous and 2.5 µg mL-1 for plasma samples. Conclusion: These results show that the established method is a fast and accurate quantification for stattic in aqueous and plasma samples.


Molecules ◽  
2021 ◽  
Vol 26 (14) ◽  
pp. 4166
Author(s):  
Agata Konarska ◽  
Elżbieta Weryszko-Chmielewska ◽  
Anna Matysik-Woźniak ◽  
Aneta Sulborska ◽  
Beata Polak ◽  
...  

The aim of this study was to conduct a histochemical analysis to localize lipids, terpenes, essential oil, and iridoids in the trichomes of the L. album subsp. album corolla. Morphometric examinations of individual trichome types were performed. Light and scanning electron microscopy techniques were used to show the micromorphology and localization of lipophilic compounds and iridoids in secretory trichomes with the use of histochemical tests. Additionally, the content of essential oil and its components were determined using gas chromatography-mass spectrometry (GC-MS). Qualitative analyses of triterpenes carried out using high-performance thin-layer chromatography (HPTLC) coupled with densitometric detection, and the iridoid content expressed as aucubin was examined with spectrophotometric techniques. We showed the presence of iridoids and different lipophilic compounds in papillae and glandular and non-glandular trichomes. On average, the flowers of L. album subsp. album yielded 0.04 mL/kg of essential oil, which was dominated by aldehydes, sesquiterpenes, and alkanes. The extract of the L. album subsp. album corolla contained 1.5 × 10−3 ± 4.3 × 10−4 mg/mL of iridoid aucubin and three triterpenes: oleanolic acid, β-amyrin, and β-amyrin acetate. Aucubin and β-amyrin acetate were detected for the first time. We suggest the use of L. album subsp. album flowers as supplements in human nutrition.


Author(s):  
Irshad Mohammad ◽  
Lucie Blondeau ◽  
Eddy Foy ◽  
Jocelyne Leroy ◽  
Eric Leroy ◽  
...  

Following the trends of alloys as negative electrodes for Na-ion batteries, the sodiation of the InSb intermetallic compound was investigated for the first time. The benefit of coupling Sb with...


Author(s):  
Ling Zhang ◽  
Chunlin Zhao ◽  
Ting Zheng ◽  
Jiagang Wu

Electrocaloric refrigeration emerges as a newly-developing technology with potential to be the next generation of coolers. However, the combination of large adiabatic temperature change (ΔT) and good temperature stability remains...


Nutrients ◽  
2020 ◽  
Vol 13 (1) ◽  
pp. 129
Author(s):  
Charlotte Cuerq ◽  
Claire Bordat ◽  
Charlotte Halimi ◽  
Emilie Blond ◽  
Marion Nowicki ◽  
...  

(1) Background: vitamin E is often supplemented in the form of tocopherol acetate, but it has poor bioavailability and can fail to correct blood tocopherol concentrations in some patients with severe cholestasis. In this context, α-tocopheryl polyethylene glycol succinate 1000 (TPGS) has been of value, but very little is known about the mechanisms of its absorption. The aim of our work was to evaluate the mechanisms of absorption/secretion of TPGS compared to tocopherol acetate (TAC) and α-tocopherol by human enterocyte-like Caco-2 TC7 cells. (2) Methods: two weeks post-confluence Caco-2 cells were incubated with tocopherol- or TAC- or TPGS-rich mixed micelles up to 24 h and, following lipid extraction, TAC and tocopherol amounts were measured by high performance liquid chromatography (HPLC) in apical, cellular, and basolateral compartments. (3) Results: at equivalent concentrations of tocopherol in the apical side, the amounts of tocopherol secreted at the basolateral pole of Caco-2 cells are (i) significantly greater when the tocopherol is in the free form in the micelles; (ii) intermediate when it is in the TAC form in the micelles (p < 0.001); and (iii) significantly lower with the TPGS form (p < 0.0001). Interestingly, our results show, for the first time, that Caco-2 cells secrete one or more esterified forms of the vitamin contained in TPGS at the basolateral side.


2014 ◽  
Vol 2 (15) ◽  
pp. 5427-5433 ◽  
Author(s):  
Shugang Li ◽  
Zhongcheng Yuan ◽  
Jianyu Yuan ◽  
Ping Deng ◽  
Qing Zhang ◽  
...  

An expanded isoindigo unit (IBTI) has been incorporated into a donor–acceptor conjugated polymer for the first time. The PCE of the solar cell device based on the new polymer reached 6.41% with a fill factor of 0.71.


RSC Advances ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 6798-6803
Author(s):  
Linchao Zeng ◽  
Jianhui Zhu ◽  
Minsu Liu ◽  
Peixin Zhang

Antimony nanosheet modified separator is prepared for high performance Li–S batteries for the first time.


2000 ◽  
Vol 655 ◽  
Author(s):  
Jung-Hyuk Koh ◽  
S.I. Khartsev ◽  
Alex Grishin ◽  
Vladimir Petrovsky

AbstractFor the first time AgTa0.38Nb0.62O3 (ATN) films have been grown on the La0.7Sr0.3CoO3 (LSCO)/LaAlO3 single crystal as well as onto Pt80Ir20 (PtIr) polycrystalline substrate. Comprehensive X-ray diffraction analyses reveal epitaxial quality of ATN and LSCO films on the LaAlO3(001) substrate, while ATN/PtIr films have been found to be (001) preferentially oriented. Dielectric spectroscopy performed for ATN films and bulk ceramics in a wide temperature range 77 to 420 K shows the structural monoclinic M1-to-monoclinic M2 phase transition occurs in films at the temperature 60 °C lower than in ceramics. The tracing of the ferroelectric hysteresis P-E loops indicates the ferroelectric state in ATN films at temperatures below 125 K and yields remnant polarization of 0.4 μC/cm2 @ 77 K. Weak frequency dispersion, high temperature stability of dielectric properties as well as low processing temperature of 550 °C make ATN films to be attractive for various applications.


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