Study of Preparation on the Flake Silver Coating over Copper Powder for Electronic Industry

2011 ◽  
Vol 275 ◽  
pp. 165-169
Author(s):  
Xiao Yun Zhu ◽  
Man Dong
Keyword(s):  
Electric Conductivity ◽  
Copper Powder ◽  
Silver Content ◽  
Copper Particle ◽  
Silver Coating ◽  
Electronic Industry ◽  
Dispersing Agent ◽  
Intermediate Phases ◽  
Xrd Patterns ◽  
Individual Particles

Flake copper powder is coated with silver by using a solution containing [Ag(NH3)]+. Factors such as copper particle size distribution, [Ag(NH3)]+ concentrations and the dispersing agent are studied and correlated with the silver content of coated copper and electric conductivity. At the condition of silver concentration of 0.8 mol/L and dispersing agent of 1.0g/L a powder of copper coated with silver with electric conductivity of 0.8×10-3Ω•cm is obtained. XRD patterns indicate that the powder consists of only the Cu and Ag phases without other intermediate phases. SEM results with different silver contents reveal that when Ag content rises, its surface topography transforms through the steps: individual particles →small islands→continuous 2D layers →multi-layers.

Preparation of Flake Silver Coated over Copper Powder

2011 ◽  
Vol 412 ◽  
pp. 251-254 ◽  
Author(s):  
Xiao Yun Zhu ◽  
Man Dong ◽  
Xu Xiao Yi
Keyword(s):  
Particle Size ◽  
Electric Conductivity ◽  
Copper Powder ◽  
Silver Content ◽  
Copper Particle ◽  
Small Islands ◽  
Dispersing Agent ◽  
Intermediate Phases ◽  
Xrd Patterns ◽  
Individual Particles

Flake copper powder is coated with silver by using a solution containing [Ag (NH3)]+. Factors such as copper particle size distribution, [Ag (NH3)]+ concentrations and the dispersing agent are studied and correlated with the silver content of coated copper and electric conductivity. At the condition of silver concentration of 0.8 mol/L and dispersing agent of 1.0g/L a powder of copper coated with silver with electric conductivity of 0.8×10-3Ω·cm is obtained. XRD patterns indicate that the powder consists of only the Cu and Ag phases without other intermediate phases. SEM results with different silver contents reveal that when Ag content rises, its surface topography transforms through the steps: individual particles → small islands → continuous 2D layers → multi-layers.

Facile Synthesis of Flake Copper Powder Loaded With Silver Particles

2011 ◽  
Vol 109 ◽  
pp. 91-95
Author(s):  
Xiao Feng Tian ◽  
Wei Ke Zhang
Keyword(s):  
Copper Powder ◽  
Composite Particle ◽  
Copper Particle ◽  
Composite Particles ◽  
Silver Particles ◽  
Facile Synthesis ◽  
Wet Chemistry ◽  
Dispersing Agent ◽  
Copper Composite ◽  
Individual Particles

A fast and facile wet chemistry method has been developed for preparing monodispersed silver coated copper composite particles. Copper powder is coated using a solution containing [Ag (NH3)] +. The effect of the copper particle size distribution, the concentrations of [Ag (NH3)] + on composite particles conductivity were investigated. The composite particle with electric conductivity of 0.8×10-3 Ω•cm is obtained at 0.8 mol/L of Ag+ and1.0 g/L of dispersing agent. Copper powder loaded with silver particles morphologies range from individual particles to small islands, to the continuous multi-layers structure with Ag+ concentration increases.

Synthesis and Characterization of Silver-Coated Copper Powder Layer

2012 ◽  
Vol 512-515 ◽  
pp. 141-146
Author(s):  
Xiao Yun Zhu ◽  
Lie Hu ◽  
Man Dong
Keyword(s):  
Copper Powder ◽  
Silver Content ◽  
Chemical Reduction ◽  
Surface Topology ◽  
Powder Layer ◽  
Silver Coating ◽  
Complete Coverage ◽  
Thermal Analyser ◽  
Differential Thermal Analyser

This paper presents the process of preparing spherical silver-coated copper powder with a silver content of 30-50%, using chemical reduction and by adjusting the silver-coating process. By means of SEM, XRD, grain size analyser, digital ohmmeter and differential thermal analyser, the surface topology, structure and conductivity of silver-coated copper powder and raw copper powder are characterised. The results show that the spherical silver-coated copper powder has superior compact surface, complete coverage, a coated layer reaching a thickness of 336nm and excellent conductivity and anti-oxidation property.

Electrical Conductivity of Chloro(phenyl)glyoxime and Its Co(II), Ni(II) and Cu(II) Complexes

2003 ◽  
Vol 68 (7) ◽  
pp. 1233-1242 ◽  
Author(s):  
Orhan Turkoglu ◽  
Mustafa Soylak ◽  
Ibrahim Belenli
Keyword(s):  
Electrical Conductivity ◽  
Temperature Dependence ◽  
Electric Conductivity ◽  
Crystal Structures ◽  
Elemental Analysis ◽  
Analysis Data ◽  
Elemental Analysis Data ◽  
The Stability ◽  
Xrd Patterns ◽  
Metal Ligand

Chloro(phenyl)glyoxime, a vicinal dioxime, and its Ni(II), Cu(II) and Co(II) complexes were prepared. XRD patterns of the complexes point to similar crystal structures. IR and elemental analysis data revealed the 1:2 metal-ligand ratio in the complexes. The Co(II) complex is a dihydrate. Temperature dependence of electrical conductivity of the solid ligand and its complexes was measured in the temperature range 25-250 °C; it ranged between 10-14-10-6 Ω-1 cm-1 and increased with rising temperature. The activation energies were between 0.61-0.80 eV. The Co(II) complex has lower electric conductivity than the Ni(II) and Cu(II) complexes. This difference in the conductivity has been attributed to differences in the stability of the complexes.

A Simple Dissolved Metals Mixing Route to Prepare Nanostructured Mg0.8Zn0.2TiO3 Solid Solution

2015 ◽  
Vol 1112 ◽  
pp. 47-52 ◽  
Author(s):  
Frida Ulfah Ermawati ◽  
Suasmoro Suasmoro ◽  
Suminar Pratapa
Keyword(s):  
Solid Solution ◽  
Particle Size ◽  
Rietveld Analysis ◽  
Dissolved Metals ◽  
Intermediate Phases ◽  
Particle Size Analyzer ◽  
Ft Ir ◽  
Xrd Patterns ◽  
Zn Ions

A study of liquid mixing route to synthesize high purity Mg0.8Zn0.2TiO3 nanopowder, a candidate dielectric ceramics, has been successfully performed. Formation of the phases on the dried powder was studied using TG/DTA, XRD and FT-IR data. Rietveld analysis on the collected XRD patterns confirmed the formation of solid solution in the system. Such solid solution can be obtained from the powder calcined at 500 °C, but calcination at 550 °C gave rise to the most optimum molar purity up to 98.5% without intermediate phases. The role of Zn ions on the formation of solid solution was also discussed. Homogeneity of particle size distribution and nano-crystallinity of the system was verified from the particle size analyzer data, TEM image and the Rietveld analysis output.

Electric conductivity of compressed copper powder. Ageing and influence of electric field strength

1980 ◽  
Vol 27 (1) ◽  
pp. 53-59 ◽  
Author(s):  
Karl-Joachim Euler ◽  
Paul Herger ◽  
Heinrich Metzendorf ◽  
Bernd Sperlich
Keyword(s):  
Field Strength ◽  
Electric Field ◽  
Electric Field Strength ◽  
Electric Conductivity ◽  
Copper Powder

Electroless Silver Plating Process on Al-Ag Alloy Powder

2013 ◽  
Vol 800 ◽  
pp. 256-259
Author(s):  
Wang Qun ◽  
Ye Fan Li ◽  
Dong Mei Li ◽  
Zhi Xue Qu
Keyword(s):  
Electroless Plating ◽  
Alloy Powder ◽  
Glucose Solution ◽  
Silver Content ◽  
Silver Coating ◽  
Chemical Compositions ◽  
Composite Powders ◽  
Plating Bath ◽  
Thiourea Solution ◽  
Electroless Silver Plating

The Ag coating was deposited on the surface of Al-Ag alloy powder by electroless plating process. 10 wt% of AgNO3 was put in the powder for precursor replacement reaction, and then added the powder into electroless plating bath which contained glucose solution, solution of silver ammonia, thiourea solution, tartaric acid solution and absolute ethanol. The effects of formula components were analyzed. The surface morphology of the prepared composite particles was studied with SEM and their chemical compositions were confirmed by XRD. With the chemical etching method, silver content of the powder was determined. The studies have shown that an uniform, complete and dense silver coating for the Al-Ag composite powders was generated by this method, with the silver content being 20wt%, and the conductivity was favorable.

Conversion of Strontium Hydroxyapatite Nanopowders to Porous Scaffolds for Bone Implant Application

2014 ◽  
Vol 607 ◽  
pp. 3-6
Author(s):  
Che Murad Mardziah ◽  
Iis Sopyan ◽  
Koay Mei Hyie ◽  
N.R. Nik Roselina
Keyword(s):  
Compressive Strength ◽  
Cancellous Bone ◽  
Compression Test ◽  
Ambient Air ◽  
Porous Scaffolds ◽  
Distilled Water ◽  
Bone Implant ◽  
Morphological Evaluation ◽  
Dispersing Agent ◽  
Xrd Patterns

The fabrication of Sr hydroxyapatite (HA) porous scaffolds was done by using polymeric sponge method. To prepare the porous samples, the synthesized SrHA nanopowders were mixed with distilled water and appropriate amount of dispersing agent followed by drying in the ambient air and sintering at 1300°C. The compressive strength of the materials was strongly influenced by the porosity, while there was almost no dependence on the crystallinity of the powders since XRD patterns showed high crystallinity of HA phase for all porous samples. Morphological evaluation by FESEM revealed that the SrHA scaffolds were characterized by macro-micro interconnected porosity, which replicates the morphology of the cancellous bone. Compression test on the porous scaffolds demonstrated that doping 10 mol% of strontium in HA has increased the compressive strength by a factor of two compared to the undoped HA with 1.81±0.26 MPa at 41% porosity.

Production and Characterization of Aluminium Metal Matrix Composite Reinforced with Al3Ni by Stir and Squeeze Casting

2015 ◽  
Vol 766-767 ◽  
pp. 315-319
Author(s):  
R. Ramesh ◽  
S. Suresh Kumar ◽  
S. Gowrishankar
Keyword(s):  
Squeeze Casting ◽  
Wear Behavior ◽  
Optical Microscope ◽  
Dry Sliding Wear ◽  
Mechanical And Tribological Properties ◽  
Intermediate Phases ◽  
Ni Powder ◽  
Xrd Patterns

In the present work AA1100/ Al3Ni MMC was successfully fabricated using the in-situ method of stirring and squeeze casting. The effects of amount of Ni powder on the formation and mechanical behavior of Al-Al3Ni MMC were investigated. The fabricated MMC was characterized using XRD and optical microscope. The XRD patterns clearly indicated the presence of Al3Ni particles without the formation of intermediate phases. The in-situ formed Al3Ni particles were found to have uniform distribution, good bonding and clear interface. The mechanical and tribological properties such as hardness, Ultimate Tensile Strength (UTS) and dry sliding wear behavior of AA1100/ Al3Ni MMC were compared for stir and squeeze casted MMCs with different percentage in weight of Al3Ni (5, 10 wt. %) and it was found that properties improved with increase in Al3Ni content and all properties of squeeze casted MMCs were superior to stir casted MMCs.

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