Thermal Analysis and Surface Morphology Study of Cholesterol: Β-Cyclodextrin Inclusion Complex

2013 ◽  
Vol 812 ◽  
pp. 221-225 ◽  
Author(s):  
Che In Fauziah ◽  
Abdul Haiyee Zaibunnisa ◽  
Hassan Osman ◽  
Wan Mustapha Wan Aida
Keyword(s):  
Electron Microscopy ◽  
Thermal Analysis ◽  
Inclusion Complex ◽  
Egg Yolk ◽  
Scanning Calorimetry ◽  
Cyclodextrin Inclusion ◽  
Cyclodextrin Inclusion Complex ◽  
The Difference ◽  
Pure Cholesterol ◽  
Scanning Electron

nclusion complex of cholesterol:β-cyclodextrin (CβIC) was characterized for thermal analysis by differential scanning calorimetry (DSC) and scanning electron microscopy (SEM). The difference of endothermic peak between inclusion compounds of cholesterol:β-cyclodextrin (CβIC) with pure cholesterol and β-cyclodextrin endothermic peaks confirmed the formation of inclusion complex. SEM results showed that of cholesterol:β-cyclodextrin inclusion complex (CβIC) observed in the form of irregular crystalline particles which has different morphology from CHO and βCD. The results obtained from this study will able to give valuable information about cholesterol-reduced egg yolk properties that could be useful to produce healthy-egg yolk based products.

Effects of Thermal Treatment on the Morphology and Properties of CSM/Poly(Urethane-Isocyanurate) Composites Formed by SRIM Process

2008 ◽  
Vol 575-578 ◽  
pp. 941-946
Author(s):  
Hong Yan Tang ◽  
Ji Hui Wang ◽  
Guo Qiang Gao ◽  
Wen Xing Chen
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Mechanical Property ◽  
Thermal Analysis ◽  
Scanning Electron Microscopy ◽  
Treatment Time ◽  
Microphase Separation ◽  
Scanning Calorimetry ◽  
Transmission Electron ◽  
Scanning Electron

Fiberglass continuous strand mat(CSM)/poly(urethane-isocyanurate) composites were formed by SRIM process, treated under different conditions and then characterized based on dynamic mechanical thermal analysis (DMTA), differential scanning calorimetry (DSC), scanning electron microscopy (SEM) ,transmission electron microscopy (TEM) and the mechanical property tests. The results show that the mechanical properties of the composites could be increased with improving the degree of microphase separation. At a given temperature (120°C), the degree of microphase separation is the highest for 4h and decreases gradually with prolonging treatment time. For a given time (4h), the well microphase-separated morphology is obtained and the degree of microphase mixing is increased at 120°C and 140°C treatments, respectively. The degree of microphase separation of the composites decreases with enhancing the temperature to 140°C.

Synthesis, Characterization and Magnetism of Nanosized Copper Ferrite

2008 ◽  
Vol 368-372 ◽  
pp. 604-606 ◽  
Author(s):  
Wei Zhong Lv ◽  
Zhong Kuang Luo ◽  
Bo Liu ◽  
Xiang Zhong Ren ◽  
Hong Hua Cai ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Thermal Analysis ◽  
Copper Ferrite ◽  
Sonochemical Method ◽  
Thermal Gravimetric ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Ft Ir ◽  
Scanning Electron

Copper ferrite powders were successfully synthesized by sonochemical method. The resultant powders were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), FT-IR, differential thermal analysis-thermal gravimetric (DTA-TG), differential scanning calorimetry (DSC) and VSM. The particle saturation magnetization (Ms) is 66 emu/g and an intrinsic coercive force (iHc) is 2100 Oe when the precursor calcined at 950 °C for 15 h.

Thermal analysis and gas chromatography coupled mass spectrometry analyses of hydroxypropyl-β-cyclodextrin inclusion complex containing Lippia gracilis essential oil

2008 ◽  
Vol 475 (1-2) ◽  
pp. 53-58 ◽  
Author(s):  
Ricardo N. Marreto ◽  
Elis E.C.V. Almeida ◽  
Péricles B. Alves ◽  
Edenilson S. Niculau ◽  
Rogéria S. Nunes ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Thermal Analysis ◽  
Gas Chromatography ◽  
Essential Oil ◽  
Inclusion Complex ◽  
Cyclodextrin Inclusion ◽  
Cyclodextrin Inclusion Complex

scholarly journals Controlled Release Profile of Imidacloprid-β-Cyclodextrin Inclusion Complex Embedded Polypropylene Filament Yarns

2017 ◽  
Vol 12 (1) ◽  
pp. 155892501701200 ◽  
Author(s):  
Ahmet C. Turan ◽  
İlhan Özen ◽  
Hüsnü K. Gürakın ◽  
Enrico Fatarella
Keyword(s):  
Thermal Stability ◽  
Differential Scanning Calorimetry ◽  
Fourier Transform ◽  
Inclusion Complex ◽  
High Performance ◽  
Release Profile ◽  
Dissolution Time ◽  
Scanning Calorimetry ◽  
Cyclodextrin Inclusion ◽  
Cyclodextrin Inclusion Complex

Imidacloprid-β-cyclodextrin (IMI-β-CD) inclusion complex was synthesized and effectively incorporated into filament yarns of polypropylene. The physical and thermal properties of IMI-β-CD inclusion complex were determined by Fourier transform infrared spectroscopy, thermogravimetric analysis, and differential scanning calorimetry. According to the results, formation of the inclusion complex was achieved along with enhanced thermal stability. The release profile of imidacloprid was monitored by high-performance chromatography measurements. Dissolution time of the IMI-β-CD inclusion complex was increased to 5 times that of the neat imidacloprid (from 9 h to 48 h). Poylpropylene filament yarns containing 3 wt.% IMI-β-CD inclusion complex released 84 wt.% of IMI within 21 days.

The Preparation and Characterization of Inclusion Complex of Ursolic Acid with γ-Cyclodextrin

2011 ◽  
Vol 403-408 ◽  
pp. 712-716 ◽  
Author(s):  
Wei Zong ◽  
Su Mei Bi
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Inclusion Complex ◽  
Inclusion Complexes ◽  
Ursolic Acid ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Grinding Method ◽  
Scanning Electron

In order to increase the solubility of ursolic acid, the inclusion complexes of ursolic acid with γ-cyclodextrin were prepared by grinding, ultrasonic and stirring methods. The characterizations of the inclusion complexes were proved by x-ray powder diffraction, fourier transform infrared spectroscopy, differential scanning calorimetry and scanning electron microscopy. The results confirmed the interactions of ursolic acid with γ-cyclodextrin, indicating the formation of the inclusion complexes. In addition, grinding method is a better way of preparing inclusion complex of ursolic acid with γ-cyclodextrin.

New Patent on Electrospinning for Increasing Rutin Loading in Nanofibers

2020 ◽  
Vol 14 (1) ◽  
pp. 35-41
Author(s):  
Na Li ◽  
Yongfang Qian ◽  
Zhen Zhang ◽  
Ying Wang ◽  
Lihua Lve ◽  
...  
Keyword(s):  
Fourier Transform ◽  
Inclusion Complex ◽  
Inclusion Complexes ◽  
Electrospun Nanofibers ◽  
Cyclodextrin Inclusion ◽  
Cyclodextrin Inclusion Complex ◽  
Loading Amount ◽  
Functional Nanofibers ◽  
Surface Morphologies ◽  
Scanning Electron

Background: The electrospinning and the bubble electrospinning provide facile ways for the fabrication of functional nanofibers by incorporating rutin/hydroxypropyl-β-cyclodextrin inclusion complex (RT/HP-β-CD-IC) in Polyvinyl Alcohol (PVA). Few patents on incorporation of rutin and cyclodextrin in nanofibers has been reported. Objective: The study aimed at increasing the loading amount of rutin in the electrospun nanofibers to obtain ultraviolet resistant property. Methods: Rutin was encapsulated in the cavity of RT/HP-β-CD and formed an inclusion complex. Fourier Transform Infrared Spectroscopy (FTIR) and Differential Scanning Calorimeter (DSC) was used to verify the formation of inclusion complexes. Results: The results showed that the inclusion between rutin and HP-β-CD had been successfully formed. The surface morphologies of nanofibrous membranes were characterized by Scanning Electron Microscope (SEM), which indicated that adding RT/HP-β-CD inclusion complexes had little influence on the morphologies and diameters of the fibers. Ultraviolet resistant results also confirmed the inclusion complex had increased the loading amount in the final nanofibrous mats, and thus had good ultraviolet resistant properties. Conclusion: The formed inclusion complexes had obviously enhanced the loading amount of rutin in electrospun PVA nanofibers, indicating that encapsulation of rutin in the cavity of HP-β-CD is a good way to increase the loading amount.

Microstructural Evolution of Mg-4Al-2.5Ca Alloy during Solidification

2015 ◽  
Vol 816 ◽  
pp. 486-491 ◽  
Author(s):  
Zhong Tao Jiang ◽  
Bin Jiang ◽  
Jian Yue Zhang ◽  
Xiang Sheng Xia ◽  
Fu Sheng Pan
Keyword(s):  
Electron Microscopy ◽  
Thermal Analysis ◽  
Energy Dispersive Spectrometer ◽  
Dendritic Structure ◽  
Eutectic Phase ◽  
Scanning Calorimetry ◽  
Phase Separation Temperature ◽  
Separation Temperature ◽  
Scanning Electron ◽  
Cast Microstructure

In the present work, the microstructure evolution of Mg-4Al-2.5Ca alloy during solidification was investigated by means of scanning electron microscopy (SEM), energy dispersive spectrometer (EDS) and differential scanning calorimetry (DSC). The results showed that the as-cast microstructure was typical dendritic structure, consisting of α-Mg and the Al2Ca with a C15 structure formed at inter-dendritic regions. But during slow solidification, the sequence of phase formation of this alloy consisted of following stages: L→ L + α-Mg → L + α-Mg + (Mg, Al)2Ca → α-Mg + (Mg, Al)2Ca + Al2Ca → α-Mg + Al2Ca. Thermal analysis showed that the (Mg, Al)2Ca and Al2Ca phase separation temperature was about 520°C and 510°C respectively, which is different from thermodynamic calculation. With the temperature decreasing, the liquid (Mg, Al)2Ca phase with thick and continuous morphology transformed into lamellar-shaped eutectic phase, and parts of (Mg, Al)2Ca phase translated into Al2Ca phase with bone-shaped and needle-like.

Effect of Cooling Rates on the Solidification and Microstructure of Rapidly Solidified Mg70.8Zn28Nd1.2 Quasicrystal Alloy

2017 ◽  
Vol 898 ◽  
pp. 246-253
Author(s):  
Xing Jing Ge ◽  
Xin Ying Teng ◽  
Shu Min Xu ◽  
Jin Yang Zhang
Keyword(s):  
Electron Microscopy ◽  
Phase Transition ◽  
Thermal Analysis ◽  
Energy Dispersive Spectrometer ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Cooling Rates ◽  
X Ray ◽  
Rapidly Solidified ◽  
Scanning Electron

The influence of cooling rates on the solidification and microstructure of rapidly solidified quasicrystal alloy Mg70.8Zn28Nd1.2(at.%) was investigated. The microstructure, phase constitution, phase transition and phase structure of the alloys were examined by means of scanning electron microscopy, x-ray diffraction, energy dispersive spectrometer, differential scanning calorimetry. The experimental results showed that the phase composition of as-cast Mg70.8Zn28Nd1.2 alloy includes quasicrystal I-phase and Mg7Zn3 phase. For the rapidly solidified alloy ribbons, when the speed is not higher than 400 r/min, the microstructure includes I-phase, Mg7Zn3 phase and α-Mg phase. When the speed is at the range of 400-2000r/min, the Mg7Zn3 phase disappears and only quasicrystal with α-Mg phase exist. With the increase of cooling rate, the grain size decreases and there are a large number of microcrystals in the microstructure. When the speed reaches higher than 2500 r/min, amorphous phase appeared. Differential thermal analysis showed that quasicrystal exist at about 340°C.

Effect of Ultra-High Pressure on the Characterization of Ursolic Acid/β-Cyclodextrin Inclusion Complex

2012 ◽  
Vol 424-425 ◽  
pp. 999-1002
Author(s):  
Feng Zhu Liu ◽  
Wei Zong
Keyword(s):  
High Pressure ◽  
Inclusion Complex ◽  
Ursolic Acid ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Ultra High Pressure ◽  
Cyclodextrin Inclusion ◽  
Cyclodextrin Inclusion Complex

To study the characterization of ursolic acid (UA) and β- cyclodextrin(β-CD) inclusion complex which prepared by ultra-high pressure method. Inclusion complex of UA /β-CD was prepared at 100MPa and 500MPa. The inclusion complex was characterized by IR spectra, X-ray diffraction, Differential scanning calorimetry and Scanning electron microscope. It was testified that the inclusion complex was formed between β-CD and UA at ultra-high pressure conditions.

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