Application of Texture Analysis for Optimizing Thermo-Mechanical Treatment of a High Mn TWIP Steel

2014 ◽  
Vol 922 ◽  
pp. 213-218 ◽  
Author(s):  
Christian Haase ◽  
Luis Antonio Barrales-Mora ◽  
Dmitri A. Molodov ◽  
Günter Gottstein
Keyword(s):  
Cold Rolling ◽  
Texture Analysis ◽  
Twip Steel ◽  
Uniform Elongation ◽  
High Yield ◽  
Processing Route ◽  
Recrystallization Annealing ◽  
Deformation Degree ◽  
Texture Measurement ◽  
Wide Range

A recently introduced processing route consisting of cold rolling and recovery annealing allows the production of TWIP steels with high yield strength along with appreciable uniform elongation due to the thermal stability of mechanically induced nanoscale twins. A wide range of strength-ductility combinations was obtained using recovery and recrystallization annealing of 30%, 40%, and 50% cold-rolled Fe-23Mn-1.5Al-0.3C TWIP steel. Texture measurement during cold rolling and annealing was proven to be a suitable tool to determine the optimal deformation degree and annealing time for this processing method. As a consequence, texture analysis can be used to predict the final materials properties.

scholarly journals Tailoring Strength and Ductility of a Cr-Containing High Carbon Steel by Cold-Working and Annealing

Materials ◽  
2019 ◽  
Vol 12 (24) ◽  
pp. 4136
Author(s):  
Jing Wang ◽  
Yongfeng Shen ◽  
Yan Liu ◽  
Fuguo Wang ◽  
Nan Jia
Keyword(s):  
Carbon Steel ◽  
Cold Rolling ◽  
High Carbon Steel ◽  
Cold Drawing ◽  
High Yield ◽  
Recrystallization Annealing ◽  
Stress And Strain ◽  
High Carbon ◽  
Fe Method ◽  
Good Ductility

SEM, TEM characterizations, in combination with tensile tests, provided an intriguing observation that ultra-high-strength and good ductility could be achieved simultaneously by changing the ratio of large and small precipitates in high-carbon steel (1.0C-1.5Cr-0.31Mn-0.20Si, wt %). The high yield strength of 670 MPa, tensile-stress of 740 MPa, and good ductility (elongation of 26%) were obtained by adopting spheroidization annealing, cold rolling, recrystallization annealing, and cold drawing. This led to nanosized precipitates with a large ratio of big size to the small size of 0.28, promoting high dislocation storage of 1.39 × 1014 m−2. In addition, the finite element (FE) method was used to simulate the cold-rolling process, and the largest stress and strain were 830 MPa and 0.6 at a depth of 3 mm after the fourth pass of the 0.10C-1.50Cr steel, respectively. The stress and strain accumulation in the top layer was potentially caused by severe plastic deformation, as well as attrition rendered by the rollers. This explained the emergence of dense low-angle grain boundaries in the region close to the surface of the cold rolled steel.

Synchrotron texture analysis with area detectors

2003 ◽  
Vol 36 (4) ◽  
pp. 1040-1049 ◽  
Author(s):  
H.-R. Wenk ◽  
S. Grigull
Keyword(s):  
Texture Analysis ◽  
Standard Technique ◽  
Orientation Distribution ◽  
Polycrystalline Materials ◽  
Texture Measurement ◽  
X Ray ◽  
Texture Information ◽  
Reconstruction Methods ◽  
Special Cases ◽  
Wide Range

The wide availability of X-ray area detectors provides an opportunity for using synchrotron radiation based X-ray diffraction for the determination of preferred crystallite orientation in polycrystalline materials. These measurements are very fast compared to other techniques. Texture is immediately recognized as intensity variations along Debye rings in diffraction images, yet in many cases this information is not used because the quantitative treatment of texture information has not yet been developed into a standard technique. In special cases it is possible to interpret the texture information contained in these intensity variations intuitively. However, diffraction studies focused on the effects of texture on materials properties often require the full orientation distribution function (ODF) which can be obtained from spherical tomography analysis. In cases of high crystal symmetry (cubic and hexagonal) an approximation to the full ODF can be reconstructed from single diffraction images, as is demonstrated for textures in rolled copper and titanium sheets. Combined with area detectors, the reconstruction methods make the measurements fast enough to study orientation changes during phase transformations, recrystallization and deformationin situ, and even in real time, at a wide range of temperature and pressure conditions. The present work focuses on practical aspects of texture measurement and data processing procedures to make the latter available for the growing community of synchrotron users. It reviews previous applications and highlights some opportunities for synchrotron texture analysis based on case studies on different materials.

Ultrafine-Grained Structure and Mechanical Properties of a High-Mn Twinning Induced Plasticity Steel

2016 ◽  
Vol 838-839 ◽  
pp. 392-397 ◽  
Author(s):  
Pavel Kusakin ◽  
Andrey Belyakov ◽  
Rustam Kaibyshev ◽  
Dmitri Molodov
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Tensile Strength ◽  
Ultimate Tensile Strength ◽  
Yield Strength ◽  
Cold Rolling ◽  
Twip Steel ◽  
True Strain ◽  
Total Elongation ◽  
Recrystallization Annealing

The influence of thermo-mechanical treatment consisting of cold rolling followed by recrystallization annealing on the grain size and mechanical properties of a high-Mn TWIP steel was studied. An Fe-23Mn-0.3C-1.5Al TWIP steel (wt. %) was subjected to extensive cold rolling with a reduction of 80% (true strain of ∼1.6) and then annealed in the temperature interval ranging from 400 to 900 °C during 20 minutes. Recovery processes took place below 500 °C, partial recrystallization was evident at ~550°C and fully recrystallized structure evolved after annealing at 600 °C and higher. The static recovery resulted in a slight decrease in the yield strength from 1400 MPa to 1250 MPa and the ultimate tensile strength from 1540 MPa to 1400 MPa whereas the total elongation of 4% did not changed. The recrystallization development led to a drastic drop of strength and an increase in ductility. The yield strength of 225 MPa, the ultimate tensile strength of 700 MPa and the total elongation of 79% was obtained after annealing at 900 °C. Correspondingly, the grain size increased from 0.2 μm to 6.2 μm with increase in anneal temperature from 550 to 900°C.

Dynamic energy absorption of ultrafine-grained TWIP steel under axial impact loading

2018 ◽  
Vol 1 (1) ◽  
pp. 51-64 ◽  
Author(s):  
Mahmoud H. A. Gadelhaq ◽  
Atef S. Hamada ◽  
Mohsen A. Hassan ◽  
Jukka Kömi
Keyword(s):  
Energy Absorption ◽  
Twip Steel ◽  
Cast Steel ◽  
Tensile Tests ◽  
High Yield ◽  
Ultrafine Grain ◽  
Recrystallization Annealing ◽  
Ultrafine Grained ◽  
Cold Worked ◽  
The Impact

This research focuses on studying the dynamic energy absorption property of a micro-alloyed TWIP steel, which was proposed to act as a connection part between car front bumper and chassis in middle-class cars for vehicle safety. The studied TWIP steel was designed based on stacking fault energy of 25mJ/m2. The as-cast steel was deformed in hot and cold rolling to 2 mm thick sheets. Subsequently, recrystallization annealing was applied to the heavily cold-worked steel at different temperatures to obtain different ultrafine grain structures. The mechanical properties were determined using tensile tests. It was observed that at 900°C, the optimal temperature for strengthening by vanadium carbide precipitation, it was too low to complete recrystallization. However, at 1000°C, an ultrafine-grained structure was formed with high yield, tensile strengths and elongation of about 700MPa, 1100MPa and 30% respectively. Accordingly, TWIP steel was used for crash analysis simulation using ANSYS Workbench R14.5. Thin-walled square columns of that steel were employed for energy absorbance during a collision regarding progressive plastic deformation. The crashworthiness criteria were studied under different impact conditions with thicknesses of 0.25, 0.5, 0.75 and 1 mm. Simulation results showed high initial peak force during the impact. Hence, a trigger mechanism of an external tapered plunger was proposed to reduce it. This combination of new material and innovative design promises enhancement car safety.

scholarly journals Effect of Processing Parameters on Mechanical Properties of Deformed and Partitioned (D&P) Medium Mn Steels

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 356
Author(s):  
Chengpeng Huang ◽  
Mingxin Huang
Keyword(s):  
Mechanical Properties ◽  
Cold Rolling ◽  
Large Scale ◽  
Intercritical Annealing ◽  
Uniform Elongation ◽  
High Strength ◽  
Processing Parameters ◽  
Annealing Process ◽  
Processing Route ◽  
Trip Effect

Deformed and partitioned (D&P) medium Mn steels exhibiting high strength, large ductility, and excellent fracture toughness have been developed recently. The ultra-high dislocation density and transformation-induced plasticity (TRIP) effect are the main mechanisms for their exceptional mechanical properties. The simple processing route to manufacturing D&P steel makes it promising for large-scale industrial applications. However, the exact effect of each processing step on the final mechanical properties of D&P steel is not yet fully understood. In the present work, the effects of processing parameters on the mechanical properties of D&P steels are systematically investigated. The evolution of microstructure, tensile behavior and austenite fraction of warm rolled samples and D&P samples are revealed. Two D&P steels, with and without the intercritical annealing process, are both produced for comparison. It is revealed that the intercritical annealing process plays an insignificant role to the mechanical properties of D&P steel. The partitioning process is extremely important for obtaining large uniform elongation via slow but sustaining strain hardening by the TRIP effect in the partitioned austenite. The cold rolling process is also significant for acquiring high strength, and the cold rolling thickness reduction (CRTR) is extremely critical for the strength–ductility synergy of D&P steels.

scholarly journals Ultrasonic Assessment of the Influence of Cold Rolling and Recrystallization Annealing on the Elastic Constants in a TWIP Steel

Materials ◽  
2021 ◽  
Vol 14 (21) ◽  
pp. 6559
Author(s):  
Linton Carvajal ◽  
María Sosa ◽  
Alfredo Artigas ◽  
Nelson Luco ◽  
Alberto Monsalve
Keyword(s):  
Cold Rolling ◽  
Elastic Constants ◽  
Poisson’S Ratio ◽  
Twip Steel ◽  
Ultrasonic Waves ◽  
Poisson's Ratio ◽  
Recrystallization Annealing ◽  
Acoustic Birefringence ◽  
The Times ◽  
High Level

The evolution of the elastic constants, , and Poisson’s ratio and acoustic birefringence of a Fe-0.5 wt% C-21.5 wt% Mn twinning-induced plasticity (TWIP) steel with reduction by cold rolling and recrystallization annealing was assessed from measurements of the times of flight of ultrasonic waves propagating along the thickness of the rolled plates. As the reduction increased, changes in the elastic constants resulted in a steadily increasing orthotropy, which was clearly shown by Poisson’s ratio and acoustic birefringence. Although optical metallography and hardness measurements showed that partial or full recrystallization is attained after annealing at 600 °C and 700 °C, the ultrasonic measurements revealed that a high level of orthotropy remains.

Microstructure Refinement of a Low Interstitial Ferritic Stainless Steel by Cold Rolling and Annealing of Martensite

2007 ◽  
Vol 558-559 ◽  
pp. 113-118
Author(s):  
H. Azizi-Alizamini ◽  
Chad W. Sinclair ◽  
Matthias Militzer ◽  
J.D. Mithieux
Keyword(s):  
Stainless Steel ◽  
Cold Rolling ◽  
Uniform Elongation ◽  
Carbon Steels ◽  
Processing Route ◽  
Low Carbon ◽  
Low Carbon Steels ◽  
Microstructure Refinement ◽  
Cold Rolling And Annealing ◽  
Cold Rolled

Several studies have shown that recrystallization of cold rolled martensite results in low carbon steels with very fine microstructures. Correspondingly, these materials exhibit promising combinations of strength and elongation. Most of the work on this processing route has focused on low carbon steels (0.1-0.2wt% carbon) where the interstitial content may play an important role in the microstructure refinement. In this note we describe experiments performed on a low interstitial stainless steel containing 0.02wt%C. It has been possible to achieve materials with high strengths (UTS > 1 GPa) and significant uniform elongation (> 8%), however, the microstructures associated with these properties are very different from those previously reported for low carbon steels.

Facile Synthesis of a Diverse Library of Mono-3-substituted β-Cyclodextrin Analogues

2018 ◽  
Author(s):  
Kathryn Kellett ◽  
Brendan M. Duggan ◽  
Michael Gilson
Keyword(s):  
High Yield ◽  
Facile Synthesis ◽  
Wide Range

We have described simple, high-yield, protocols, which require only commonly accessible equipment, to synthesize a wide range of β-CD derivatives mono-substituted at the secondary face. These derivatives may be useful in their own right, and they are also scaffolds for further modification, and examples of the far broader array of derivatives that may be accessed by these procedures.

scholarly journals MXenes for future nanophotonic device applications

Nanophotonics ◽  
2020 ◽  
Vol 9 (7) ◽  
pp. 1831-1853
Author(s):  
Jaeho Jeon ◽  
Yajie Yang ◽  
Haeju Choi ◽  
Jin-Hong Park ◽  
Byoung Hun Lee ◽  
...  
Keyword(s):  
Solar Cells ◽  
Transition Metal ◽  
Wide Spectrum ◽  
Building Blocks ◽  
Optoelectronic Device ◽  
High Yield ◽  
Saturable Absorption ◽  
Nanophotonic Device ◽  
Wide Range ◽  
Device Applications

AbstractTwo-dimensional (2D) layers of transition metal carbides, nitrides, or carbonitrides, collectively referred to as MXenes, are considered as the new family of 2D materials for the development of functional building blocks for optoelectronic and photonic device applications. Their advantages are based on their unique and tunable electronic and optical properties, which depend on the modulation of transition metal elements or surface functional groups. In this paper, we have presented a comprehensive review of MXenes to suggest an insightful perspective on future nanophotonic and optoelectronic device applications based on advanced synthesis processes and theoretically predicted or experimentally verified material properties. Recently developed optoelectronic and photonic devices, such as photodetectors, solar cells, fiber lasers, and light-emitting diodes are summarized in this review. Wide-spectrum photodetection with high photoresponsivity, high-yield solar cells, and effective saturable absorption were achieved by exploiting different MXenes. Further, the great potential of MXenes as an electrode material is predicted with a controllable work function in a wide range (1.6–8 eV) and high conductivity (~104 S/cm), and their potential as active channel material by generating a tunable energy bandgap is likewise shown. MXene can provide new functional building blocks for future generation nanophotonic device applications.

scholarly journals Multiparametric MRI Texture Analysis in Prediction of Glioma Biomarker Status: Added Value of MR Diffusion

2021 ◽  
Author(s):  
Shingo Kihira ◽  
Nadejda Tsankova ◽  
Adam Bauer ◽  
Yu Sakai ◽  
Keon Mahmoudi ◽  
...  
Keyword(s):  
Texture Analysis ◽  
Diffusion Mri ◽  
Test Group ◽  
Multiparametric Mri ◽  
Added Value ◽  
Conventional Mri ◽  
Mri Features ◽  
Wide Range ◽  
Mr Diffusion ◽  
And Diffusion

Abstract Background Early identification of glioma molecular phenotypes can lead to understanding of patient prognosis and treatment guidance. We aimed to develop a multiparametric MRI texture analysis model using a combination of conventional and diffusion MRI to predict a wide range of biomarkers in patients with glioma. Methods In this retrospective study, patients were included if they 1) had diagnosis of gliomas with known IDH1, EGFR, MGMT, ATRX, TP53 and PTEN status from surgical pathology and 2) had preoperative MRI including FLAIR, T1c+ and diffusion for radiomic texture analysis. Statistical analysis included logistic regression and receiver-operating characteristic (ROC) curve analysis to determine the optimal model for predicting glioma biomarkers. A comparative analysis between ROCs (conventional only vs. conventional + diffusion) was performed. Results From a total of 111 patients included, 91 (82%) were categorized to training and 20 (18%) to test datasets. Constructed cross-validated model using a combination of texture features from conventional and diffusion MRI resulted in overall AUC/accuracy of 1/79% for IDH1, 0.99/80% for ATRX, 0.79/67% for MGMT, and 0.77/66% for EGFR. The addition of diffusion data to conventional MRI features significantly (p<0.05) increased predictive performance for IDH1, MGMT and ATRX. The overall accuracy of the final model in predicting biomarkers in the test group was 80% (IDH1), 70% (ATRX), 70% (MGMT) and 75% (EGFR). Conclusion Addition of MR diffusion to conventional MRI features provides added diagnostic value in preoperative determination of IDH1, MGMT, and ATRX in patients with glioma.

Sign in / Sign up

Export Citation Format

Share Document