Effect of Aging on Microstructure and Performance after Superplastic Deformation of Fine Grained 1420 Al-Li Alloy

2014 ◽  
Vol 936 ◽  
pp. 1647-1652
Author(s):  
Yan Ling Zhang ◽  
Hong Liang Hou ◽  
Yao Qi Wang

Superplastic forming (SPF) is an important process for forming fine grained 1420 Al-Li alloy. However, the mechanical properties will be decreased after deforming at high temperature. How to obtain the optimize relationship of strength and ductility after SPF is one of the key problems for the process. In this paper, a set of artificial aging tests including single and two-step aging were carried out, which are the typical strengthening process for Al-Li alloy. Based on experimental results, strength and elongation were studied by means of tensile tests at room temperature, and the effect of aging processes on mechanical properties was analyzed. Finally, the microstructures fore and after aging were examined by OM and TEM, and the strengthening mechanism of 1420 Al-Li alloy was further studied. It is found that artificial aging especially two-step aging can increase mechanical properties of post-SPF material obviously, and δ (Al3Li) is the primary strengthening phase.

2014 ◽  
Vol 697 ◽  
pp. 72-75
Author(s):  
De Liang Yin ◽  
Jian Qiao ◽  
Hong Liang Cui

An extruded ZK60 magnesium alloy was subjected to artificial aging at 180 oC for an investigation of the effect of aging time on its precipitation behavior and mechanical properties. Uniaxial tensile tests were conducted to obtain the mechanical properties. Optical microscopy and transmission electron microscopy (TEM) were employed to observe microstructure change before and after aging treatment. It is shown that, both tensile yield strength and ultimate tensile strength increases with aging time. The fracture elongation after aging for 20 h reaches up to 21.0%, and the yield strength increases to 269.5 MPa, 19.4% higher than that of extruded specimens (un-aged), showing a good match of strength and ductility. Three newly-formed precipitates were observed after aging for over 20 h, among which particulate and dispersive precipitates should be responsible for the good combination of strength and ductility.


Metals ◽  
2018 ◽  
Vol 8 (9) ◽  
pp. 658 ◽  
Author(s):  
Huan Liu ◽  
He Huang ◽  
Ce Wang ◽  
Jia Ju ◽  
Jiapeng Sun ◽  
...  

Developing high strength and high ductility magnesium alloys is an important issue for weight-reduction applications. In this work, we explored the feasibility of manipulating nanosized precipitates on LPSO-contained (long period stacking ordered phase) ultra-fine grained (UFG) magnesium alloy to obtain simultaneously improved strength and ductility. The effect of two aging treatments on microstructures and mechanical properties of an UFG Mg-10Y-6Gd-1.5Zn-0.5Zr alloy was systematically investigated and compared by a series of microstructure characterization techniques and tensile test. The results showed that nano γ’’ precipitates were successfully introduced in T5 peak aged alloy with no obvious increase in grain size. While T6 peak aging treatment stimulated the growth of α-Mg grains to 4.3 μm (fine grained, FG), together with the precipitation of γ’’ precipitates. Tensile tests revealed that both aging treatments remarkably improved the strengths but impaired the ductility slightly. The T5 peak aged alloy exhibited the optimum mechanical properties with ultimate strength of 431 MPa and elongation of 13.5%. This work provided a novel strategy to simultaneously improve the strength and ductility of magnesium alloys by integrating the intense precipitation strengthening with ductile LPSO-contained UFG/FG microstructure.


2021 ◽  
Vol 825 ◽  
pp. 141918
Author(s):  
Ziwei Zhang ◽  
Siqi Zhao ◽  
Yongqi Lv ◽  
Hongbo Zhang ◽  
Zhenwei Wang ◽  
...  

Materials ◽  
2022 ◽  
Vol 15 (2) ◽  
pp. 603
Author(s):  
Natalia Rońda ◽  
Krzysztof Grzelak ◽  
Marek Polański ◽  
Julita Dworecka-Wójcik

This work investigates the effect of layer thickness on the microstructure and mechanical properties of M300 maraging steel produced by Laser Engineered Net Shaping (LENS®) technique. The microstructure was characterized using light microscopy (LM) and scanning electron microscopy (SEM). The mechanical properties were characterized by tensile tests and microhardness measurements. The porosity and mechanical properties were found to be highly dependent on the layer thickness. Increasing the layer thickness increased the porosity of the manufactured parts while degrading their mechanical properties. Moreover, etched samples revealed a fine cellular dendritic microstructure; decreasing the layer thickness caused the microstructure to become fine-grained. Tests showed that for samples manufactured with the chosen laser power, a layer thickness of more than 0.75 mm is too high to maintain the structural integrity of the deposited material.


Metals ◽  
2022 ◽  
Vol 12 (1) ◽  
pp. 152
Author(s):  
Peng Peng ◽  
Shaosong Jiang ◽  
Zhonghuan Qin ◽  
Zhen Lu

This work fabricated a double hollow structural component of Mg-8.3Gd-2.9Y-0.8Zn-0.2Zr alloy by superplastic forming (SPF) and reaction-diffusion bonding (RDB). The superplastic characteristic and mechanical properties of Mg-8.3Gd-2.9Y-0.8Zn-0.2Zr alloy sheets at 250–450 °C were studied. Tensile tests showed that the maximum elongation of tensile specimens was about 1276.3% at 400 °C under a strain rate of 1 × 10−3 s−1. Besides, the effect of bonding temperature and interface roughness on microstructure and mechanical properties of the reaction diffusion-bonded joints with a Cu interlayer was investigated. With the increase of temperature, the diffusion coefficient of Cu increases, and the diffusion transition region becomes wider, leading to tightening bonding of the joint. However, the bonding quality of the joint will deteriorate due to grain size growth at higher temperatures. Shear tests showed that the highest strength of the joints was 152 MPa (joint efficiency = 98.7%), which was performed at 460 °C.


2009 ◽  
Vol 618-619 ◽  
pp. 551-554 ◽  
Author(s):  
O. Al-Buhamad ◽  
M. Zakaria Quadir ◽  
Michael Ferry

A multilayered sheet composite of commercial purity Al and Al-0.3%Sc alloys was produced by accumulative roll bonding. The final sheet material consisted of 64 ultra fine grained layers, each of ~7.8mm in thickness. The as-deformed material was annealed at temperatures ranging from 250 to 350°C to study the changes in microstructure and their associated influence on mechanical properties. The as-deformed structures largely comprised of high angle grain boundaries in the Al layers and low angle grain boundaries in the Al(Sc) layers. During annealing, the structures in the Al(Sc) layers remained unaltered, whereas the Al layers recrystallized rapidly to the full layer thickness. The mechanical properties of the Al-Al(Sc) composite were measured and found to be unique in strength and ductility with annealing temperature having a significant influence on these properties.


2010 ◽  
Vol 638-642 ◽  
pp. 3128-3133 ◽  
Author(s):  
Felix Peñalba ◽  
Xabier Gómez ◽  
R. Allende ◽  
Manuel Carsí ◽  
Oscar A. Ruano

The possibilities to improve the properties of steels for tubes exposed at high temperatures are explored. The mechanical properties and forming behavior of an experimental casting of type 9Cr-ferritic steels, P92, containing 2%W, are studied. The hardenability was determined by means of continuous cooling diagrams associated with hardness measurements and microstructure observations. Tensile tests from room temperature to 650°C were carried out to determine the variation of the strength and ductility in this temperature range. In addition, Charpy impact tests were conducted to characterize the toughness of the steel and the ductile-brittle transition temperature. Finally, hot torsion tests at various temperatures and strain rates were carried out and the generalized stresses and strains to rupture for each test are determined. With these data forming stability maps were generated to characterize the best forming conditions.


2021 ◽  
Vol 1016 ◽  
pp. 917-921
Author(s):  
Haruka Miyano ◽  
Keisuke Takemoto ◽  
Hiromoto Kitahara ◽  
Shinji Ando

In this study, tensile tests of rolled Mg-Li alloy and Mg-Ce alloy sheets were carried out at room temperature to investigate effects of alloying additions on the relationship between mechanical properties and activities of slip systems in magnesium polycrystals. In Mg-Li alloy, ductility increased while strength decreased by lithium addition. Frequency of non-basal slips increased with increasing lithium content. In Mg-Ce alloy, strength and ductility were similar pure magnesium, and non-basal slips were hardly activated. Since critical resolved shear stress of non-basal slips were decreased by lithium addition, ductility of magnesium was increased while its strength was decreased.


2015 ◽  
Vol 641 ◽  
pp. 3-9
Author(s):  
Anna Kula ◽  
Ludwik Blaz ◽  
Makoto Sugamata

Experiments on Al-1Fe-1Ni-5Mg alloy were performed to determine the effect of rapid solidification (RS) on the material strengthening, which result from the refining of the grain size and intermetallic compounds. Additionally, an enhancement of the material strengthening due to magnesium addition was also observed. RS procedure was performed using spray deposition of the molten alloy on the rotating water-cooled copper roll. As a result, highly refined structure of rapidly solidified flakes was obtained. Using common powder metallurgy (PM) techniques, i.e. cold pressing, vacuum degassing and hot extrusion, as received RS-flakes were consolidated to the bulk PM materials. For comparison purposes, the conventionally cast and hot extruded Al-1Fe-1Ni-5Mg alloy was studied as well. RS process combined with hot pressing and extrusion procedure was found to be very effective method for the manufacture of fine grained material and effective refinement of intermetallic compounds. However some inhomogenity of particles distribution was observed, which was ascribed to varied cooling rate dependent on the particular spray-drop size. Mechanical properties of as-extruded material were examined using compression test at 293K – 873K. High strength and ductility of as-extruded RS material with respect to conventionally produced alloy were observed. However, the effect of enhanced mechanical properties of RS material is observed only at low deformation temperatures. It was found that increasing deformation temperature above 400K results in negligible hardening of RS samples if compared to conventionally produced material.


2011 ◽  
Vol 287-290 ◽  
pp. 420-423
Author(s):  
Jin Song Chen

Jet electrodeposition orientated by rapid fabrication were introduced , The nanocrystalline nickel parts were fabricated using jet electrodeposition . The microstructure and phase transformation of nanocrystalline nickel were observed under the scanning microscope and X-ray diffraction instrument . The results show that the jet electrodeposition can greatly enhance the limited current density, fine crystalline particles and improve deposition quality. The nickel parts prepared by jet electrodeposition own a fine-grained structure with a smooth surface and high dimensional accuracy under the optimum processing parameters.


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