Glass-Crystalline Materials of a Cellular Structure, Formed by Vibration Foaming Technology

2021 ◽  
Vol 410 ◽  
pp. 823-828
Author(s):  
Vitaly A. Beregovoi ◽  
Dmitry S. Sorokin ◽  
Aleksandr M. Beregovoi
Keyword(s):  
Cellular Structure ◽  
Raw Material ◽  
Crystalline Materials ◽  
Vibration Effect ◽  
Glass Forming ◽  
Gas Formation ◽  
Joint Influence ◽  
Plastic Strength ◽  
Main Component ◽  
Foaming Technology

A method for producing cellular materials on a glass-crystalline matrix has been developed. The formation of a porous structure is ensured by the process of gas formation, combined with a vibration effect on the raw mass. The possibility of gaining the plastic strength of the raw mass, sufficient for fixing the cellular structure of the raw material without adding binders, has been established. The main component of the raw material mixture is a finely ground filler, obtained after grinding glass-crystalline frit of a specially selected composition. For its formation pre-compacted raw masses, containing natural silica and glass-forming additives, are heated. There was investigated the joint influence of the compositions formulation and the roasting parameters on the properties indicators of the glass composite.

Hyper-Pressed Composites from Recycling Products of Aerated Concrete Waste

2021 ◽  
Vol 410 ◽  
pp. 784-789
Author(s):  
Vitaly A. Beregovoi ◽  
Aleksandr M. Beregovoi
Keyword(s):  
Material Properties ◽  
Water Resistance ◽  
Physical And Mechanical Properties ◽  
Raw Material ◽  
Pressing Method ◽  
Joint Influence ◽  
Aerated Concrete ◽  
The Individual ◽  
Main Component ◽  
Concrete Recycling

A technology has been developed for obtaining wall materials by the hyper-pressing method, including the recycling of large-tonnage waste from the production of autoclaved aerated concrete. The main component of the raw mixture is finely ground filler fractions, obtained by crushing substandard fragments of aerated concrete. The joint influence of raw mixture, the parameters of pressing and the conditions of hardening on the indicators of material properties has been investigated. There was given a quantitative assessment of the individual components contribution of the raw material composition to the indicators of the physical and mechanical properties of the material. The mechanism is disclosed of the constructive effect of aerated concrete recycling waste and plasticizing additives on the water resistance and strength of samples. The promising areas of application of hyper-pressed materials in modern construction are presented.

scholarly journals Qualitative terpene profiling of Cannabis varieties cultivated for medical purposes

Rodriguésia ◽  
2020 ◽  
Vol 71 ◽  
Author(s):  
Ernesto Diaz Rocha ◽  
Vitória EA Silva ◽  
Fernanda CS Pereira ◽  
Valery M Jean ◽  
Fabio L Costa Souza ◽  
...  
Keyword(s):  
Raw Material ◽  
Control Methods ◽  
Intermediate Type ◽  
Spectral Library ◽  
Medical Cannabis ◽  
Two Samples ◽  
Different Strains ◽  
Main Component ◽  
Non Destructive

Abstract With the upcoming medical Cannabis regulation, quality control methods on raw material will be required. Besides testing for contaminants and potency, there are also pharmaceutical and forensic interests in the determination of the terpene profile in different strains of Cannabis as complementary identification methods. A simple non-destructive HS-SPME GC-MS method was used to identify the terpene content in twelve Cannabis samples, four of them were of the hemp type (Harle-tsu), seven from various marihuana types and one of the intermediate type. They all were previously analyzed by HPLC to determine the potency (THC and CBD content). Spectral library matching was used to identify the terpenes compounds. Thirty terpenes compounds were detected, nine of them were present in all Cannabis samples and used to find their terpene profile: α-pinene, β-pinene, β-myrcene, D-limonene, terpinolene, linalool, caryophyllene, α-bergamotene and humulene. Three of them, caryophyllene, α-pinene and β-myrcene were found as larger components in most of samples. A principal components analyses (PCA) was performed. The four hemp type samples showed two different profiles, two samples showed caryophyllene as main component and the others two with β-myrcene as such. The marihuana type samples showed wider profiles with no clear patterns at all, which is not surprising because of the low number of samples. The simple methodology shows viable to set the terpenes profile for analyses of raw Cannabis material. Suitability for differentiation between different sorts of types needs more studies, with increasing numbers of samples.

scholarly journals Melt-Quenched Porous Organic Cage Glasses

2021 ◽  
Author(s):  
Michael C. Brand ◽  
Francesca Greenwell ◽  
Rob Clowes ◽  
Benjamin Egleston ◽  
Aiting Kai ◽  
...  
Keyword(s):  
Crystal Engineering ◽  
Molecular Glasses ◽  
Crystalline Materials ◽  
Gas Uptake ◽  
Glass Forming ◽  
Soluble Glass ◽  
Alternative Approach ◽  
Liquid States ◽  
Forming Behaviour ◽  
Molecular Nature

The discrete molecular nature of porous organic cages (POCs) has allowed us to direct the formation of crystalline materials by crystal engineering. It has also been possible to create porous amorphous solids by deliberately disrupting the crystalline packing, either with chemical modification or by processing. More recently, organic cages were used to form isotropic porous liquids. However, the connection between solid and liquid states of POCs, and the glass state, are almost completely unexplored. Here, we investigate the melting and glass-forming behaviour of a range of organic cages, including both shape-persistent POCs formed by imine condensation, and reduced and synthetically post-modified amine POCs that are more flexible and lack shape-persistence. The organic cages exhibited melting and quenching of the resultant liquids provides molecular glasses. One of these molecular glasses exhibited improved gas uptake for both CO2 and CH4 compared to the starting amorphous cage. In addition, foaming of the liquid in one case resulted in a more stable and less soluble glass, which demonstrates the potential for an alternative approach to forming materials such as membranes without solution processing.

scholarly journals Karakterisasi Minyak Atsiri dari Simplisia Basah Ranting dan Daun sebagai Alternatif Subtitusi Kulit Batang Cinnamomum burmannii Blume

2018 ◽  
pp. 125-136
Author(s):  
Mery Budiarti ◽  
Wahyu Jokopriambodo ◽  
Ani Isnawati
Keyword(s):  
Refractive Index ◽  
Essential Oil ◽  
Chemical Constituent ◽  
Raw Material ◽  
Alternative Source ◽  
Water Distillation ◽  
Marker Compound ◽  
Cinnamomum Burmannii ◽  
Main Component ◽  
Material Scarcity

The bark of Cinnamomum burmannii Blume is the main raw material of Cinnamomum oil because its cinnamaldehyde content is higher than in the other parts. This condition lead to the exploitation of Cinnamomum burmannii Blume bark without any cultivation effort, thus it can cause the raw material scarcity. Twigs and leaves of Cinnamomum burmannii Blume are also known to contain cinnamaldehyde therefore it provide a potential alternative source of cinnamaldehyde. The purpose of this research is to investigate the characteristic of Cinnamomum burmannii Blume essential oil which includes refractive index, profiling of chemical constituent and percentage of cinnamaldehyde as a marker compound. This research used three fresh Cinnamomum burmannii Blume simplicia of bark, twigs and leaves from two selected growing locations: Tawangmangu and Purwokerto. Simple water distillation method was conducted, together with characterization and refractive index using refractometer, followed by qualitative and quantitative analysis with Thin Layer Chromatography (TLC) and Gas Chromatography (GC). The results showed Cinnamomum burmannii Blume oil derived from bark, twig and leaf have different profiles, but all have cinnamaldehyde as the main component. The leaf produces higher essential oil yield percentage compared to the twig with a cinnamaldehyde content that is comparable to the bark by 50% of cinnamaldehyde content in cinnamomum bark oil.

scholarly journals Mineralogical and physico-chemical characterizations of clay from Keur Saër (Senegal)

Clay Minerals ◽  
2012 ◽  
Vol 47 (4) ◽  
pp. 499-511 ◽  
Author(s):  
A. Mbaye ◽  
C. A. K. Diop ◽  
B. Rhouta ◽  
J. M. Brendle ◽  
F. Senocq ◽  
...  
Keyword(s):  
Cation Exchange ◽  
Cation Exchange Capacity ◽  
Clay Fraction ◽  
Exchange Capacity ◽  
Raw Material ◽  
Basic Knowledge ◽  
Mineral Mixture ◽  
Fine Clay ◽  
Main Component ◽  
Adsorption Desorption

AbstractThere is interest in exploiting and developing natural resources, particularly deposits of natural clays. Senegal has several clay mineral deposits for which chemical and mineralogical compositions have been little studied. Some of these natural materials are nowadays used in pottery and ceramics. To extend applications, a better basic knowledge is required and, for this objective, the raw clay and separated <2 μm clay fraction from Keur Saër (Senegal) were subjected to chemical and mineralogical studies. Several techniques including X-ray diffraction (XRD), thermal analysis (TG-DTA), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), N2 adsorption-desorption isotherms, cation exchange capacity (CEC) measurements and solid state nuclear magnetic resonance (NMR) have been used to characterize the material. It was found that the raw clay and the separated clay fraction consist of a mineral mixture in which kaolinite is the main component. 29Si and 27Al MAS-NMR spectra show the presence of silicon atoms linked to three other silicon atoms via an oxygen atom and six coordinated Al atoms. Significant increases in the specific surface area and cation exchange capacity were observed on purification, reaching a maximum of about 73.2 m2g–1 and 9.5 meq/100 g for the separated fine clay fraction while the values for the raw material were around 28.9 m2g–1 and 7.3 meq/100 g.

scholarly journals Temperature, Solid Loading and Time Effects on Recovery of Sugar from OPEFB

2018 ◽  
Vol 156 ◽  
pp. 03022 ◽  
Author(s):  
Diah Meilany ◽  
MTAP Kresnowati ◽  
Tjandra Setiadi
Keyword(s):  
Lignocellulosic Biomass ◽  
Treatment Process ◽  
Hydrothermal Process ◽  
Raw Material ◽  
Effect Of Temperature ◽  
Solid Loading ◽  
Time Effects ◽  
Glucose Recovery ◽  
Pre Treatment ◽  
Main Component

Biorefinery industry used lignocellulosic biomass as the raw material. Oil Palm Empty Fruit Bunch (OPEFB) is one of Indonesian potential lignocellulosic biomass, which consists of hemicellulose with xylan as the main component. Xylitol production via fermentation could use this xylan since it can be converted into xylose. However, the structure of OPEFB is such that hemicellulose is protected in a way that will hinder hydrolysis enzyme to access it. Considering that hemicellulose is more susceptible to heat than cellulose, a hydrothermal process was applied to pre-treat OPEFB before it was hydrolyzed enzymatically. The aim of the research is to map the effect of temperature, solid loading and time of pre-treatment process to obtain and recover as much as possible accessible hemicellulose from OPEFB. The results showed that temperature gave more significant effect than time and solid loading for glucose recovery of OPEFB residues. While xylose recovery varies greatly with temperature, but solid loading and time gave less significant effect.

scholarly journals Low-Mass Liquid Crystalline Materials Blended in Recycled Thermoplastic Polyester Elastomer for Corrosion Inhibitor Application

Polymers ◽  
2021 ◽  
Vol 13 (18) ◽  
pp. 3188
Author(s):  
Chun-Jui Chen ◽  
Bo-Wei Huang ◽  
Po-Jung Tseng ◽  
Zhi-Yu Yang ◽  
Xiang Huang ◽  
...  
Keyword(s):  
Liquid Crystalline ◽  
Electrochemical Corrosion ◽  
Raw Material ◽  
Pet Waste ◽  
Crystalline Materials ◽  
Iron Plate ◽  
Anticorrosion Coatings ◽  
Adhesion Behavior ◽  
Low Mass ◽  
Liquid Crystalline Materials

In this work, the development and application of multicomponents obtained from recycled polyethylene terephthalate (r-PET) waste and monotropic liquid crystals as anticorrosion coatings are reported. The r-PET raw material was alcoholyzed and reproduced as a thermoplastic polyester elastomer (TPEE) with different amounts (n%, n = 0, 1, 3, and 5) of 1,6-hexanediamine (HDA). Then, a fluorine-containing liquid crystal (4-cyano-3-fluorophenyl 4-ethylbenzoate (4CFE)) was incorporated into the TPEE mixture via solvent blending to modify and enhance the water resistance. The adhesion behavior of the coating on glass and iron substrates was evaluated by cross-cut tests and immersion tests in aqueous NaCl. In the corrosion resistance measurements, all of the coating samples fabricated with 10 ± 1 mm thickness were less active toward electrochemical corrosion (PEF% > 99%) than the bare iron plate, indicating that our work provided better protection against corrosion of the iron plate.

scholarly journals Production and characterization of sophorolipids by Candida bombicola using catfish fat

2019 ◽  
Vol 14 (9) ◽  
pp. 152
Author(s):  
Nguyen Luong Hieu Hoa ◽  
Le Quynh Loan ◽  
Vo Thanh Sang ◽  
Le Van Minh ◽  
Le Viet Dung ◽  
...  
Keyword(s):  
Low Cost ◽  
Radical Scavenging ◽  
Raw Material ◽  
Dependent Manner ◽  
Candida Bombicola ◽  
Main Component ◽  
Seafood Processing ◽  
Layer Chromatography ◽  
Dose Dependent

Catfish fat is a high nutrition by-product of seafood processing industry. In this work, catfish fat has been used as a sustainable and economical raw material for sophorolipids production by Candida bombicola. Sophorolipids yield was maximum as 21.8g/L after 7 days of fermentation at 25oC, pH 6, 180 rpm. The obtained sophorolipids was to contained the main component as lactonic sophorolipids, which has been confirmed by Thin layer chromatography (TLC). Sophorolipids also exhibited the ability to resistant Staphylococcus aureus, Bacillus subtilis, Escherichia coli, Pseudomonas aeruginosa and showed the ability of free radical scavenging the dose dependent manner with IC50 was 4.45 mg/ml. These results suggested that sophorolipids could be used in health care products and cosmetic. Catfish fat could be used as the low cost hydrophobic carbon source to replace fatty acid for sophorolipids production.

Application of Improved BP Neural Network in the Preparation Processing of the CaCO3 Nanocrystalline

2017 ◽  
Vol 726 ◽  
pp. 338-342 ◽  
Author(s):  
Qiang Luo ◽  
Qing Li Ren
Keyword(s):  
Bp Neural Network ◽  
Layer Structure ◽  
Back Propagation ◽  
Raw Material ◽  
Technological Factors ◽  
Learning Speed ◽  
Main Component Analysis ◽  
Input Variables ◽  
Main Component ◽  
Propagation Network

A three-layer structure back-propagation network model based on the non-linear relationship between the size of the CaCO3 nanocrystalline and the technological factors, such as reaction time, reaction temperature, raw material adding amount of NaCO3 and CaCl2, was established. Moreover, in order to accelerate the converging rate and avoid the non-converging situation, the momentum terms are introduced. Besides, the variable learning speed is adopted. At the same time, the input variables were pretreated by using the main component analysis firstly. And the results show that the improved back propagation neural networks model is very efficient for predication of the CaCO3 nanocrystalline size.

scholarly journals Improving Mildew Resistance of Soy Meal by Nano-Ag/TiO2, Zinc Pyrithione and 4-Cumylphenol

Polymers ◽  
2020 ◽  
Vol 12 (1) ◽  
pp. 169 ◽  
Author(s):  
Wenping Li ◽  
Mingsong Chen ◽  
Yanchen Li ◽  
Jingmeng Sun ◽  
Yi Liu ◽  
...  
Keyword(s):  
Soy Protein ◽  
Cellular Structure ◽  
Value Added ◽  
Oil Industry ◽  
Raw Material ◽  
Zinc Pyrithione ◽  
Mildew Resistance ◽  
Soy Meal ◽  
Mold Resistance ◽  
Value Added Products

As a byproduct from the soybean oil industry, soy meal can be reproduced into value-added products to replace formaldehyde as a plywood adhesive. However, the use of soy meal has been limited by its poor antifungal and antiseptic properties. In this work, three kinds of material, namely nano-Ag/TiO2, zinc pyrithione, and 4-cumylphenol were applied to enhance the mildew resistance of soy meal via breakdown of the cellular structure of mildew. The fungi and mold resistance, morphology, thermal properties, and mechanism of the modified soy meal were evaluated. The success of the antifungal and antiseptic properties was confirmed by Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy. The results indicated that all three kinds of material improved the fungi and mold resistance of soy meal, and sample B, which was modified with a compound of nano-Ag/TiO2 and zinc pyrithione, was the effective antifungal raw material for the soy-based adhesives. FTIR indicated that the great improvement of antifungal properties of soy meal modified with 4-cumylphenol might be caused by the reaction between COO– groups of soy protein. This research can help understand the effects of the chemical modification of nano-Ag/TiO2, zinc pyrithione, and 4-cumylphenol on soy meal, and the modified soy meal exhibits potential for utilization in the plywood adhesive industry.

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