Tribological Behaviour of Ceramic Coatings Formed on Titanium Alloy through Miro-Arc Oxidation Technique

2007 ◽  
Vol 353-358 ◽  
pp. 898-901 ◽  
Author(s):  
Xue Tong Sun ◽  
Cheng Xin Lin

In the present work, the wear behaviour of coatings produced on Ti-6Al-4V alloy by micro-arc oxidation method was studied. The wear tests were performed using a pin-on-disc wear machine under dry sliding conditions. It is found that the MAO coating can efficiently improve the wear-resistant performance of Ti alloy in the test range of this paper. The coated samples demonstrated wear rates up to 5-12 times lower than that of the uncoated substrates tested. The wear behaviours are deeply characterized by the variations of coating structure and composition.

Author(s):  
L. Jacobs ◽  
M. Hyland ◽  
Μ. De Bonte

Abstract The tribological behaviour of WC-Co-Cr coatings deposited by HVOF and HVAF and WC-Co coating deposited by HVAF was investigated in pin-on-disc tests. Wear rates were determined and wear tracks on the coatings and counterbodies were investigated in SEM. The HVAF sprayed coatings showed greater wear resistance compared to the HVOF coatings. The main wear mechanism in the WC-Co coatings was adhesive wear. The cobalt matrix is lubricious, resulting in very low wear rates and low debris generation. The main wear mechanisms in the WC-Co-Cr coatings were adhesive and abrasive wear. Adhesive wear results in pull-outs that are trapped in the contact zone and act as a third-body abrasive. Particle pull-out of the coating significantly increases the wear rate of the coated specimen. The HVAF/WC-Co-Cr coatings proved to have a better resistance to particle pull-out which reflected in a considerably lower wear rate than the HVOFIWC-Co-Cr coatings.


Materials ◽  
2021 ◽  
Vol 14 (12) ◽  
pp. 3281
Author(s):  
Chiara Soffritti ◽  
Annalisa Fortini ◽  
Anna Nastruzzi ◽  
Ramona Sola ◽  
Mattia Merlin ◽  
...  

This work evaluates the dry sliding behavior of anodic aluminum oxides (AAO) formed during one traditional hard anodizing treatment (HA) and two golden hard anodizing treatments (named G and GP, respectively) on a EN AW-6060 aluminum alloy. Three different thicknesses of AAO layers were selected: 25, 50, and 100 μm. Prior to wear tests, microstructure and mechanical properties were determined by scanning electron microscopy (VPSEM/EDS), X-ray diffractometry, diffuse reflectance infrared Fourier transform (DRIFT-FTIR) spectroscopy, roughness, microhardness, and scratch tests. Wear tests were carried out by a pin-on-disc tribometer using a steel disc as the counterpart material. The friction coefficient was provided by the equipment. Anodized pins were weighed before and after tests to assess the wear rate. Worn surfaces were analyzed by VPSEM/EDS and DRITF-FTIR. Based on the results, the GP-treated surfaces with a thickness of 50 μm exhibit the lowest friction coefficients and wear rates. In any case, a tribofilm is observed on the wear tracks. During sliding, its detachment leads to delamination of the underlying anodic aluminum oxides and to abrasion of the aluminum substrate. Finally, the best tribological performance of G- and GP-treated surfaces may be related to the existence of a thin Ag-rich film at the coating/aluminum substrate interfaces.


Metals ◽  
2018 ◽  
Vol 8 (11) ◽  
pp. 895 ◽  
Author(s):  
Luca Boccarusso ◽  
Fabio Scherillo ◽  
Umberto Prisco

Microstructure, hardness, transverse rupture strength, and abrasion resistance of WC-10 wt% Co cemented carbides modified with the addition of different mass fraction of Cr3C2, in the range of 0–3 wt%, are studied. The influence of the microstructure, composition and hardness on the mechanical properties and wear resistance is analysed. Considering that the material under investigation can be used as die for the extrusion process of hard ceramic materials, the tribological behaviour was evaluated by performing sliding wear tests in wet conditions using a block-on-ring tribometer. Wear mechanism principally based on binder removal and subsequent fragmentation and microabrasion of the WC grains is proposed. Carbide grain size and bulk hardness can be tuned as function of specific applications by adding different amounts of Cr3C2. In particular, increasing hardness and reducing grain size by the addition of Cr3C2 are demonstrated to considerably enhance the wear performance of these carbides.


2016 ◽  
Vol 1137 ◽  
pp. 24-38
Author(s):  
Jasmaninder Singh Grewal ◽  
Buta Singh Sidhu ◽  
Satya Prakash

In the present work TiAlN coatings were deposited by plasma spray process as titanium aluminium based nitride (Ti, Al)N coatings possess excellent tribological behaviour with respect to metal cutting and polymer forming contacts. Three coatings of TiAlN were deposited on AISI-304 grade boiler steel substrate out of which two were thin nanocoatings deposited at different temperatures of 500°C and 200°C and one conventional coating was deposited by plasma spraying. The as sprayed coatings were characterized with relative to coating thickness, microhardness, porosity and microstructure. The optical microscopy (OM), the XRD analysis and field mission scanning electron microscope (FESEM with EDAX attachment) techniques have been used to identify various phases formed after coating deposited on the surface of the substrate. Subsequently the sliding wear behaviour of uncoated, PVD sprayed nanostructured thin TiAlN coatings deposited at 500°C and 200°C and plasma sprayed conventional coated AISI-304 grade boiler steel were investigated according to ASTM standard G99-03 using pin on disk wear test rig. Cumulative wear volume loss and coefficient of friction, μ were calculated for the coated as well as uncoated specimens for 0.5, 1 and 2 m/sec sliding velocities at a constant normal load of 10 N. The worn out samples were analysed with SEM/EDAX. Wear rates in terms of volumetric loss (mm3/g) for uncoated and coated alloys were compared. The nanostructured TiAlN coatings deposited at 500°C and 200°C has shown minimum wear rate as compared to conventional TiAlN coating and uncoated AISI-304 grade boiler steel. Nanostructured TiAlN coatings were found to be successful in retaining surface contact with the substrate after the wear tests.


2012 ◽  
Vol 19 (04) ◽  
pp. 1250038 ◽  
Author(s):  
H. X. LI ◽  
H. H. ZHU ◽  
X. WU ◽  
Z. G. JI

Ceramic coatings have been synthesized on 6063 aluminum alloy by micro-arc oxidation (MAO) technique in the solution of Na2B4O7 electrolyte with and without α- Al2O3 nanoadditive. Effects of α- Al2O3 nanoadditive on the phase composition, micro-structure, micro-hardness, adhesion and wear resistance of the prepared ceramic coatings have been investigated in this paper. The phase composition and microstructure of the MAO coatings were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDX) analyses, respectively. Micro-hardness, adhesion and tribological and wear tests were also performed. The results showed that the α- Al2O3 nanoadditive doped in the electrolyte had great influence on the structural and mechanical properties of the ceramic coatings.


2012 ◽  
Vol 512-515 ◽  
pp. 1066-1069
Author(s):  
Jin Xue Zhang

Compound ceramic coatings with the main crystal phase of Al2TiO5 (as-coated samples) were prepared in situ on the surface of Ti-6Al-4V alloy by means of pulsed bi-polar micro-arc oxidation (MAO) in an NaAlO2 solution. The coated samples were calcined in argon and air at 1000 oC, respectively. The phase composition, surface and section morphology, and element contents of the ceramic coatings were investigated by X-ray diffractometry (XRD), Scanning electron microscopy (SEM) and X-ray fluorescence spectroscopy (XRF). The samples were treated in argon and the as-coated ones were calcined in air at 1000 oC to study the anti-oxidation properties of the samples. The results show that Al2TiO5 had been decomposed in an hour and transformed into α-Al2O3 and rutile TiO2 in air. However, Al2TiO5 had been decomposed in four hours in argon and the final coating surface was completely composed of α-Al2O3. The content of Al2O3 was decreased from outside to inside layers and Ti2O3 was formed in the coating. Furthermore, the morphology of the ceramic coatings after the calcination was different. The coatings calcined in argon were finer; the grains and pores were smaller than those in air.


2010 ◽  
Vol 97-101 ◽  
pp. 1554-1557
Author(s):  
Guo Dong Hao ◽  
Nai Wu Zhang ◽  
Tao Yun ◽  
Jin Wang ◽  
Bo Lian ◽  
...  

Compound ceramic coatings with the main crystalline of Al2TiO5 (as-coated samples) were prepared in situ on the surface Ti-6Al-4V alloy by means of pulsed bi-polar micro-arc oxidation (MAO) in a NaAlO2 solution. The coated samples were calcined in argon and air at 1000 oC, respectively. The phase composition, surface morphology of the ceramic coatings were investigated by XRD, SEM and XRF. The samples were treated in argon and the as-coated ones were calcined in air at 1000 oC to study the anti-oxidation properties of the samples. The results show that Al2TiO5 was decomposed very soon and transformed into α-Al2O3 and rutile TiO2 in air. However, Al2TiO5 was decomposed very slowly in argon and the final coating surface was completely α-Al2O3. Also, the morphology of the ceramic coatings after the calcination was different. The coatings calcined in argon were fined; grains and pores were smaller than those in air. High temperature oxidation occurred very strongly in the TC4 substrate, the weight gains of the as-coated ceramic coatings and the treated ones in argon were nearly changing in the form of parabola, and the weight gains of the coated samples treated in argon were comparatively lower than those of the as-coated samples.


Author(s):  
Róbert Bidulský ◽  
Jana Bidulská ◽  
Freddy Arenas ◽  
Marco Actis Grande

AbstractThe present paper deals with the tribological behaviour of the boride and carbide hardmetals evaluated by performing comparative dry sliding pin-on-disc experiments using normal contact loads. Analyses of the wear performance results, microstructural evaluation and processing conditions effect indicate that microstructure inhomogenities play an important role in abrasive wear behaviour of cermets. In term of grain size and chemical composition, the addition of VC also play an important role in increasing the wear resistance.


2017 ◽  
Vol 2017 ◽  
pp. 1-9
Author(s):  
J. Sukumaran ◽  
R. Keresztes ◽  
G. Kalácska ◽  
H. Almaliki ◽  
P. D. Neis ◽  
...  

Polyamide (PA6/6) is often used as a tribological pair in abrasion prevalent applications such as hinges and sliders. PA6/6 is frequently processed by injection moulding and extrusion process. It is known that these processes influence the polymers mechanical behaviour, but their influence on the polymers wear response has not been studied. Hence the present research attempts to study the influence of different manufacturing processes on tribological behaviour for PA6/6. Wear tests were performed on a pin abrading tester (DIN 50322). Abrasion resistance of both extruded and injection moulded PA6/6 were tested at different loads (20 and 35 N). Single-pass (nonoverlapping mode) and multipass testing (overlapping mode) were used to understand the influence of clogging of wear debris. It is evidenced that with increasing load the specific wear rate decreases; moreover, fine abrasives tend to reduce the wear rate. In multipass testing a transfer layer clogged on the counterface that acted as a protective agent and lowers wear rate. Poor mechanical strength of injection moulded polymers is apparently compensated by microstructural response for having a similar wear behaviour between extruded and injection moulded PA 6/6. Hence a proper balance between microstructural and mechanical characteristics is an absolute must in PA 6/6 for better wear performance.


Author(s):  
JL Viesca ◽  
S González-Cachón ◽  
A García ◽  
R González ◽  
A Hernández Battez

This paper compares the tribological behaviour of microalloyed rail steel with conventional C–Mn rail steel under different test conditions (load, temperature and humidity). Pin-on-disc tribological tests were performed inside a climate chamber under different loads (20, 30 and 40 N), relative humidity (15, 55 and 70%) and temperatures (20 and 40 ℃). After the friction and wear tests, the worn surfaces were analysed using both confocal and scanning electron microscopies. The results obtained show that the use of microalloyed steel in railway applications under severe conditions (high loads and humidity) could lead to increased service life of the rails and could extend the time between maintenance operations.


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