Hardness Evaluation of Carbonate Apatite Cement Based on Various Ratio of Precursor

2017 ◽  
Vol 758 ◽  
pp. 52-55 ◽  
Author(s):  
Nina Djustiana ◽  
Mitha Amaranila ◽  
Nadia Greviana ◽  
Myrna Nurlatifah Zakaria ◽  
Sunarso ◽  
...  
Keyword(s):  
Vickers Hardness ◽  
Bone Substitute ◽  
Testing Machine ◽  
Control Group ◽  
Carbonate Apatite ◽  
Hardness Testing ◽  
Hardness Level ◽  
Natural Bone ◽  
Apatite Cement ◽  
Precursor Ratio

Carbonate Apatite (CO3Ap) cement is considered as an ideal bone substitute due to its biocompatibility and osteoconductivity. Also, CO3Ap cement has the chemical composition that closes to natural bone. During cement preparation, precursors play an important role that affects the properties of CO3Ap cement. Cement hardness is one of the important properties that need to be evaluated before the obtained cement can be applied as a bone substitute. Therefore, the purpose of this study is to determine the effect of precursor ratio of CaCO3 and CaHPO4 on the hardness level of CO3Ap cement. In the present study, the CO3Ap cement was prepared from CaCO3 and CaHPO4. Both Commercial and synthesized CaCO3 were used. The CO3Ap cement obtained from commercial CaCO3 was used as a control group. Synthesized CaCO3 was obtained from Indonesian natural limestone. Three different CaCO3:CaHPO4 ratios, 40:60, 30:70 and 20:80 were mixed with 1 mol/L Na2HPO4. Samples were kept at 37°C with 100% relative humidity for 24 hours then tested using micro Vickers hardness testing machine. The micro Vickers hardness of the control group with CaCO3:CaHPO4 ratio of 40:60, 30:70 and 20:80 were 5.09 VHN, 6.34 VHN, and 6.73 VHN, respectively. Meanwhile, the micro Vickers hardness of the CO3Ap cement obtained from synthesized CaCO3 were 6.22 VHN, 7.50 VHN, and 10.37 VHN for the CaCO3:CaHPO4 ratio of 40:60, 30:70 and 20:80, respectively. The micro Vickers hardness level of CO3Ap cement precursor ratio from the lowest to the highest was 40:60 < 30:70 < 20:80. In conclusion, the precursor ratio significantly affects the hardness level of the CO3Ap cement. The hardness level of CO3Ap cement obtained from synthesized CaCO3 was higher compared with that obtained from commercial CaCO3.

scholarly journals Radiodensitometric Analysis of Maxillary Sinus-Lift Areas Enforced with Bone Substitute Materials Containing Calcium Phophate

2012 ◽  
Vol 12 (1) ◽  
pp. 41-44
Author(s):  
Laura Neimane ◽  
Andrejs Skagers ◽  
Girts Salms ◽  
Liga Berzina-Cimdina
Keyword(s):  
Maxillary Sinus ◽  
Bone Substitute ◽  
Alveolar Bone ◽  
Control Group ◽  
Study Group ◽  
Sinus Lift ◽  
Natural Bone ◽  
One Stage ◽  
Bone Substitute Materials ◽  
Substitute Materials

SummaryIntroduction. An enforcement of atrophic maxilla with biomaterials during sinus-lift surgery improves size and quality of alveolar bone. Radiological densitometric analysis can prove it. Within the study a density of bone was investigated and findings were compared with natural bone around the implants.Aim of the Study.Was to determine if density around the implant inserted with one stage sinus-lift operation using bone substitute materials increase and if that can be detected radiologically.Materials and Methods.Totally there were examined 22 patients where 64 implants were inserted in maxilla: 48 implants were inserted with one stage sinus-lift operation using bone substitute materials; represented study group. Sixteen implants were inserted in natural maxillary alveolar bone of the same patients, representing control group. The density of implant supporting tissue was measured with cone beam computed tomography and expressed in Hounsfield units (HU). The measurements were performed according to standardized pattern.Results.Densitometric measurements were higher in the study group than in the control group in all points, but statistically significant difference was observed in two measurement sites: buccally in sinus elevation area (BSM) (p=0.005) and palatinally in sinus elevation area (PSM) (p=0.0012), and corresponding areas in control group.Conclusions.Surgical elevation of maxillary sinus floor using calcium phosphate bone substitute materials resulted in higher optical density compared to natural bone. Mineralization of the bone, induced by the bone substitute materials, can be detected radiologically

scholarly journals Calibration Of Vickers Hardness Test PT.Tenaris Seamless Pipe Indonesia Jaya Cilegon Using Standar Blok

2020 ◽  
Vol 64 (3) ◽  
pp. 81-87
Author(s):  
Dodi Dodi Sofyan Arief ◽  
◽  
Muftil Badri ◽  
M Dalil ◽  
Agus Reforiandi ◽  
...  
Keyword(s):  
Vickers Hardness ◽  
Testing Machine ◽  
Hardness Test ◽  
International Standards ◽  
Measuring Instruments ◽  
Test Machine ◽  
Hardness Testing ◽  
Diamond Pyramid ◽  
Vickers Hardness Test

A calibration is an activity to determine the conventional validity of the appointment value of measuring instruments and measuring materials by comparing them to standard measurements that are traceable to national and international standards for measurement units and or international and certified reference materials. The calibration is generally a process of adjusting the output or indication of a measurement device to match the magnitude of the standard used in certain accuracy. The purpose of this paper is to find out the vickers hardness test calibration whether the machine running normally or there is a problem with the device. A case study was conducted in PT. Tenaris SPIJ, Cilegon, Indonesia. A vickers hardness testing in the case study has its own reference standard, namely ISO 6507-2: 2018 Metal material - Hardness Test Verification and Calibration of the test machine. The vickers hardness test equipment is a machine to conduct tests using a diamond pyramid with a plane angle of 136°, by means of an emphasis by an indentor that results in a trace or indentation on the surface of the test object. The vickers hardness testing is abbreviated as HV or HVN and also known as Diamond Pyramid Hardness Test (DPH). Result of calibration in the case study was found the repeatability value on vickers hardness testing machine of 32 HV 10 and the error value of ±3%.

Diametral Tensile Strength Evaluation of Carbonate Apatite Cement Reinforced by Genipin Cross-Linked Gelatin

2019 ◽  
Vol 829 ◽  
pp. 28-33
Author(s):  
Zatira Avriyanti ◽  
Zulia Hasratiningsih ◽  
Arief Cahyanto
Keyword(s):  
Tensile Strength ◽  
Mechanical Strength ◽  
Weight Ratio ◽  
Control Group ◽  
Carbonate Apatite ◽  
High Porosity ◽  
Bone Substitute Material ◽  
Average Value ◽  
Apatite Cement ◽  
Diametral Tensile Strength

Carbonate apatite is one of the most widely studied bioceramic material for its use as bone cement. On the previous study, it has already stated that CO3Ap cement has good osteoconductivity which makes this cement could be replaced by bone. However, the mechanical strength of CO3Ap cement is still low. This low mechanical strength is estimated due to the high porosity and absence of organic components. The aim of this study is to improve the mechanical strength of the CO3Ap cement reinforced by gelatin as an organic component with genipin as a cross-linking agent (Gelapin). The powder phase of vaterite and DCPA at weight ratio 40:60 were mixed with 0.2 mol/L Na2HPO4, 5% (w/v) gelatin, and 20% (v/v) genipin using 0.5 liquid to powder (L/P) ratio. The liquid phase ratios of Na2HPO4 and Gelapin were 50:50, 70:30, and 90:10. For control group, Gelapin were didn’t mixed in the liquid. Diametral tensile strength was improving and statistically significant (p<0.05) on set cement with 50:50 liquid ratio, the average value was 6.02 ± 0.14 MPa whereas the average value of the control group was only 3.10 ± 0.15 MPa. For this instance, gelatin serves a polymer matrix so the carbonate apatite crystallites could be well distributed within it which then gives more flexibility and resistance for the cement. On the other hand, genipin was also successfully cross-linked the gelatin. This study showed that by reinforcing CO3Ap cement using genipin cross-linked gelatin might be a good candidate for a bone substitute material.

Standardized Study of Carbonate Apatite as Bone Substitute in Rabbit’s Tibia

2011 ◽  
Vol 493-494 ◽  
pp. 242-246
Author(s):  
I. Cezar ◽  
G. Kammer ◽  
A. Alves ◽  
J. Calasans-Maia ◽  
M.A. Gress ◽  
...  
Keyword(s):  
Bone Substitute ◽  
Bone Repair ◽  
Histological Analysis ◽  
Control Group ◽  
Carbonate Apatite ◽  
Serial Sections ◽  
Bright Field ◽  
Polarized Microscopy ◽  
Ethics Commission ◽  
Made In

The objective of this study was to investigate the bone repair of carbonate apatite (cHA) in comparison to hydroxyapatite (HA, control group) on osseous repair of rabbit’s tibia. Spheres (400-500 µm) of both materials were synthesized under 37°C (cHA) and 90°C (HA) and were not sinterized. Ethics Commission on Teaching and Research in Animals approved this project (CEPA/NAL 208/10). Six White New Zealand rabbits were submitted to general anesthesia and one perforation (2mm) was made in each tibia for implantation of cHA (left tibia) and HA spheres (right tibia). After 4 weeks all animals were killed and one fragment of each tibia with the biomaterial was collected with a total of 6 bone blocks for each group. Five bone blocks of each group were demineralized and 5-µm thick semi-serial sections were stain with Hematoxillin and Eosin and Trichromic of Masson for histological analysis and two fragments were collected and embedded in a methacrylate-based resin and cut into slices with ~30 µm and were analyzed by light microscopy (bright field and polarized microscopy). Both groups didn’t show the spheres after 4 weeks, new-formed bone was observed from the periphery toward to the center of the surgical defect, which was even filled with connective tissue. Both materials are biocompatible, promote osteoconduction and showed to be resorbable.

scholarly journals Resistance to Fracture of Dental Roots Obturated with Different Materials

2015 ◽  
Vol 2015 ◽  
pp. 1-5 ◽  
Author(s):  
Berkan Celikten ◽  
Ceren Feriha Uzuntas ◽  
Kamran Gulsahi
Keyword(s):  
Fracture Resistance ◽  
Testing Machine ◽  
Negative Control Group ◽  
Positive Control ◽  
Negative Control ◽  
Positive Control Group ◽  
Control Group ◽  
Root Canal Filling ◽  
Filling Materials ◽  
Group 2

The aim of this study was to compare the vertical fracture resistance of roots obturated with different root canal filling materials and sealers. Crowns of 55 extracted mandibular premolar teeth were removed to provide root lengths of 13 mm. Five roots were saved as negative control group (canals unprepared and unfilled). Fifty root canals were instrumented and then five roots were saved as positive control group (canals prepared but unfilled). The remaining 45 roots were randomly divided into three experimental groups (n=15root/group) and obturated with the following procedures: in group 1, glass ionomer-based sealer and cone (ActiV GP obturation system); in group 2, bioceramic sealer and cone (EndoSequence BC obturation system); and in group 3, roots were filled with bioceramic sealer and cone (Smartpaste bio obturation system). All specimens were tested in a universal testing machine for measuring fracture resistance. For each root, the force at the time of fracture was recorded in Newtons. The statistical analysis was performed by using Kruskal-Wallis and post hoc test. There were no significant differences between the three experimental groups. The fracture values of three experimental and negative control groups were significantly higher than the positive control group. Within the limitations of this study, all materials increased the fracture resistance of instrumented roots.

scholarly journals Comparative Evaluation of Fracture Resistance of Endodontically Treated Teeth Restored with Resin Fiber Post and Stainless Steel Post: An In Vitro Study

2015 ◽  
Vol 03 (02) ◽  
pp. 080-084
Author(s):  
Vijay Singh ◽  
Poonam Bogra ◽  
Saurabh Gupta ◽  
Navneet Kukreja ◽  
Neha Gupta
Keyword(s):  
Stainless Steel ◽  
Fracture Resistance ◽  
Testing Machine ◽  
Compressive Force ◽  
Control Group ◽  
Fiber Post ◽  
Endodontically Treated Teeth ◽  
Group I ◽  
Significant Difference

AbstractFracture resistance of endodontically treated teeth restored with post. Aims: This study aims to compare the fracture resistance of endodontically treated teeth restored with resin fiber and stainless steel post. Commercially available prefabricated resin fiber post(Dentsply Maillefer Easy Post), prefabricated stainless steel post(Coltene/Whaledent Parapost) were used. Methods and Material: Forty five maxillary central incisors were obturated and divided into 3 groups: Control Group (Group I) without any post (n = 15), Resin Fiber Post Group (Group II) (n = 15) and Stainless Steel Post Group (Group III) (n = 15). In all Groups except control group, post space was prepared; a post was cemented, and a core build-up was provided. All the specimens were subjected to compressive force under a universal testing machine until fracture. Statistical analysis used: The results were analyzed using the variable analysis test (ANOVA). Results: One-way analysis of variance revealed significant difference among test groups. The control group demonstrated highest fracture resistance (925.2183 N), followed by the resin fiber post group (486.7265 N) and stainless steel post group (423.539N). Conclusions: Teeth restored with resin fiber post showed higher fracture resistance values than prefabricated stainless steel post.

scholarly journals The Effect of Different Disinfecting Agents on Bond Strength of Resin Composites

2014 ◽  
Vol 2014 ◽  
pp. 1-7 ◽  
Author(s):  
Ahmed Mohammed Hassan ◽  
Ahmed Ali Goda ◽  
Kusai Baroudi
Keyword(s):  
Bond Strength ◽  
Sodium Hypochlorite ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Testing Machine ◽  
Control Group ◽  
Posterior Teeth ◽  
Surface Pretreatment ◽  
Dentin Surface ◽  
Post Hoc

Objective. The aim of this study was to evaluate the effect of different disinfectant agents on bond strength of two types of resin composite materials.Methods. A total of 80 sound posterior teeth were used. They were divided into four groups(n=20)according to the dentin surface pretreatment (no treatment, chlorhexidine gluconate 2%, sodium hypochlorite 4%, and EDTA 19%). Each group was divided into two subgroups according to the type of adhesive (prime and bond 2.1 and Adper easy one). Each subgroup was further divided into two subgroups according to the type of resin composite (TPH spectrum and Tetric EvoCeram). Shear bond strength between dentin and resin composite was measured using Universal Testing Machine. Data collected were statistically analyzed byt-test and one-way ANOVA followed by Tukey’spost hoctest.Results. It was found that dentin treated with EDTA recorded the highest shear bond strength values followed by sodium hypochlorite and then chlorhexidine groups while the control group showed the lowest shear bond strength.Conclusions. The surface treatment of dentin before bonding application has a great effect on shear bond strength between resin composite and dentin surface.

Influence of High Temperature Annealing on Microstructure Evolution of Ni-24Fe-14Cr-8Mo Superalloy

2021 ◽  
Vol 904 ◽  
pp. 117-123
Author(s):  
Yi Cui ◽  
Yun Fei Zhang ◽  
Yan Guang Han ◽  
Da Lv
Keyword(s):  
High Temperature ◽  
Microstructure Evolution ◽  
Testing Machine ◽  
Aging Treatment ◽  
Growth Patterns ◽  
High Temperature Annealing ◽  
Rockwell Hardness ◽  
Hardness Testing ◽  
X Ray Diffraction ◽  
X Ray

The effect of high temperature annealing on microstructure evolution of Ni-24Fe-14Cr-8Mo alloy was investigated through Optical Microscopy (OM), Scanning Electron Microscopy (SEM), X-Ray Diffraction (XRD) and Rockwell Hardness Testing Machine. Three kinds of grain growth patterns were found at different annealing temperatures due to carbides precipitation and dissolution. After a combination of high temperature annealing and aging treatment, the hardness versus time curves performed a parabolic pattern. The highest hardness was achieved under 1070°C/60 minutes treatment, and the desirable annealing time should be 60 minutes to 90 minutes.

scholarly journals Effect of Using Nano and Micro Airborne Abrasive Particles on Bond Strength of Implant Abutment to Prosthesis

2015 ◽  
Vol 26 (1) ◽  
pp. 50-55 ◽  
Author(s):  
Mansour Rismanchian ◽  
Amin Davoudi ◽  
Elham Shadmehr
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Control Group ◽  
Abrasive Particles ◽  
Significant Difference ◽  
Implant Abutments ◽  
Implant Abutment ◽  
Roughened Surface ◽  
Bond Strengths ◽  
Spss Software

Connecting prostheses to the implant abutments has become a concern and achieving a satisfactory retention has been focused in cement-retention prostheses recently. Sandblasting is a method to make a roughened surface for providing more retention. The aim of this study was to compare effects of nano and micro airborne abrasive particles (ABAP) in roughening surface of implant abutments and further retention of cemented copings. Thirty Xive abutments and analogues (4.5 D GH1) were mounted vertically in self-cured acrylic blocks. Full metal Ni-Cr copings with a loop on the top were fabricated with appropriate marginal adaptation for each abutment. All samples were divided into 3 groups: first group (MPS) was sandblasted with 50 µm Al2O3 micro ABAP, second group (NSP) was sandblasted with 80 nm Al2O3 nano ABAP, and the third group (C) was assumed as control. The samples were cemented with provisional cement (Temp Bond) and tensile bond strength of cemented copings was evaluated by a universal testing machine after thermic cycling. The t test for independent samples was used for statistical analysis by SPSS software (version 15) at the significant level of 0.05. Final result showed significant difference among all groups (p<0.001) and MPS manifested the highest mean retention (207.88±45.61 N) with significant difference among other groups (p<0.001). The control group showed the lowest bond strength as predicted (48.95±10.44 N). Using nano or micro ABAP is an efficient way for increasing bond strengths significantly, but it seems that micro ABAP was more effective.

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