The Influence of Biopolymer Coated Fertilizer on the Agrochemical Parameters of the Soil

2020 ◽  
Vol 869 ◽  
pp. 315-320
Author(s):  
Ibragim M. Bamatov ◽  
Evgeniy V. Rumyantsev ◽  
Magomed M. Arsanov
Keyword(s):  
Electron Microscope ◽  
Nitric Acid ◽  
Scanning Electron Microscope ◽  
Polyvinyl Alcohol ◽  
Biodegradable Polymer ◽  
Core Material ◽  
X Ray ◽  
Coated Fertilizer ◽  
Scanning Electron

This papper is about the use of biopolymer of polyvinyl alcohol (PVA) as a coat of different fertilizer granules (Azafoska 16:16:16 and Yara Kristalon 19:19:19) as a core material in presence of nitric acid. The biodegradable polymer layer provides uniform diffusion of minerals into the soil as the PVA shell decays. Scanning Electron Microscope (SEM) and Energy – Dispersive X-ray spectroscopy (EDX - 3600) were carried out for the characterization of bio-modified materials. The agrochemical changes of the soil in terms of macro-and microelements were also determined.

scholarly journals Characterization of Fe Doped AC/TiO2

2019 ◽  
Vol 8 (12S) ◽  
pp. 1146-1147
Keyword(s):  
Activated Carbon ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Anatase Phase ◽  
Sol Gel ◽  
Sem Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

Abstract: The photocatalytic composite Fe doped AC/TiO2 has been prepared by sol-gel method. The prepared Fe doped AC/TiO2 composite were characterized by scanning electron microscope (SEM) and X-ray diffraction (XRD).The SEM analysis showed that Fe and TiO2 were attached to the Activated Carbon surfaces. The X-Ray Diffraction data showed that Fe doped AC/TiO2 composite mostly contained anatase phase.

scholarly journals Karakterisasi Membran ZSM-5 yang Disintensis dengan Variasi Jenis dan Ukuran Kasa Penyangga

2020 ◽  
Vol 16 (1) ◽  
pp. 1
Author(s):  
Ana Hidayati Mukaromah ◽  
Tulus Ariyadi ◽  
Inas Hasna Azizah ◽  
Mifbakhuddin Mifbakhuddin
Keyword(s):  
Fourier Transform ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Energy Dispersive Spectroscopy ◽  
Energy Dispersive ◽  
X Ray Diffraction ◽  
X Ray ◽  
Aisi 316 ◽  
Scanning Electron

<p>Telah dilakukan sintesis dan karakterisasi membran ZSM-5 dengan penyangga kasa jenis 304 ukuran 200 dan 400 mesh dan jenis kasa AISI 316 ukuran 180 mesh. Tujuan penelitian ini adalah mensintesis membran ZSM-5 dengan penyangga kasa jenis 304 ukuran 200 dan 400 mesh dan jenis kasa AISI 316 ukuran 180 mesh dan mengkarakterisasi membran ZSM-5 hasil sintesis. Sintesis membran dilakukan dengan cara melapiskan prekursor ZSM-5 (<em>coating)</em> pada penyangga kasa yang telah diberi perlakuan dan dipanaskan pada suhu 90 °C selama 4 hari. Selanjutnya, membran yang dihasilkan dikarakterisasi engan metoda <em>X-ray diffraction</em> (XRD), <em>scanning electron microscope-energy dispersive spectroscopy</em> (SEM-EDS) dan <em>Fourier-transform infrared</em> (FTIR). Hasil citra SEM-EDS menunjukkan bahwa ukuran membran ZSM-5 yang semakin besar, menghasilkan jumlah lubang atau pori semakin banyak dengan luasan pori yang semakin kecil. Pola difraksi XRD menunjukkan bahwa membran yang dihasilkan mempunyai intensitas tertinggi pada 2 8º dan 23º yang merupakan karakteristik dari ZSM-5. Hasil spektra FTIR menunjukkan adanya serapan pada bilangan gelombang 450 cm<sup>-</sup><sup>1</sup>yang merupakan ciri khas membran ZSM-5.</p><p class="Text"><strong>Characterization of ZSM-5 Membranes Synthesized by Variation of Support Types and Sizes.</strong> Synthesis and characterization of ZSM-5 membrane were carried out with 304 type 200 and 400 mesh gauze supports and 180 mesh AISI 316 gauze types. The purpose of this study was to synthesize ZSM-5 membrane with 304 type 200 and 400 mesh gauze support and AISI 316 type 180 mesh size 180 mesh and characterize the synthesized ZSM-5 membrane. Membrane synthesis was carried out by coating the pre-treated gauze support with the ZSM-5 precursor and was heated at 90 °C for 4 days. Furthermore, the resulting membrane was characterized by X-ray diffraction (XRD), scanning electron microscope-energy dispersive spectroscopy (SEM-EDS) dan Fourier-transform infrared (FTIR). The SEM-EDX analysis shows that the increasing of ZSM-5 membrane size allowed pores number to increase with smaller pore surface area. The X-ray Diffraction pattern (XRD) shows that the resulting membrane has the highest intensity at 2  of 8º and 23º as the characteristics of ZSM-5. The FTIR spectra results show absorption at wavenumbers 450 cm<sup>-1</sup> which is a characteristic of ZSM-5 membranes.</p>

Microstructure Characterization of Laser Clad TiVCrAlSi High Entropy Alloy Coating on Ti-6Al-4V Substrate

2010 ◽  
Vol 154-155 ◽  
pp. 621-625 ◽  
Author(s):  
Can Huang ◽  
Yong Zhong Zhang ◽  
Rui Vilar
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Alloy Coating ◽  
High Entropy Alloy ◽  
X Ray Diffraction ◽  
X Ray ◽  
High Entropy ◽  
Bcc Phase ◽  
Scanning Electron

Due to the promising properties of high entropy alloy, TiVCrAlSi high entropy alloy coating was prepared on Ti-6Al-4V alloy surface by laser cladding. The microstructure and phase analysis of as-cast TiVCrAlSi alloy and laser clad coating were characterized by scanning electron microscope and X-ray diffraction. The results indicate that as-cast TiVCrAlSi alloy is mainly composed of (Ti,V)5Si3 and bcc phase. The laser clad coating is metallurgically bonded to the substrate with few pores and cracks. Laser clad TiVCrAlSi coating is also composed of (Ti,V)5Si3 and bcc phases.

STRUCTURAL AND OPTICAL CHARACTERIZATION OF NANOCRYSTALLINE CuAlS2 CHALCOPYRITE SYNTHESIZED BY POLYOL METHOD IN AUTOCLAVE

2012 ◽  
Vol 26 (31) ◽  
pp. 1250179 ◽  
Author(s):  
Y. VAHIDSHAD ◽  
A. IRAJIZAD ◽  
R. GHASEMZADEH ◽  
S. M. MIRKAZEMI ◽  
A. MASOUD
Keyword(s):  
Electron Microscope ◽  
Polyethylene Glycol ◽  
Scanning Electron Microscope ◽  
Optical Characterization ◽  
Polyol Method ◽  
Capping Agent ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

Chalcopyrite CuAlS 2 nanoparticles were synthesized with polyol method. The solvothermal with autoclave nanoparticles synthesized are investigated. The amount and temperature of reducer, the solvent of salts could be important parameters that were studied. The nanoparticles were synthesized with CuCl , AlCl 3 and thiourea ( SC ( NH 2)2) as precursors, diethylene glycol (( CH 2 CH 2 OH )2 O ) and polyethylene glycol 600 ( HO ( C 2 H 4 O )n H ) as solvent and capping agent respectively, and ammonia ( NH 4 OH ) as reducing agent. The parameters of synthesis were studied by X-Ray diffraction (XRD) for analysis of structure, scanning electron microscope (SEM) for morphology and by ultraviolet–visible (UV–VIS) spectrophotometer for analysis of light structure. The possible formation mechanism is also discussed.

scholarly journals Geochemical and Petrographic Characterization of Bricks and Mortars of the Parish Church SANTA Maria in Padovetere (Comacchio, Ferrara, Italy)

Minerals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 530
Author(s):  
Elena Marrocchino ◽  
Chiara Telloli ◽  
Mario Cesarano ◽  
Manlio Montuori
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Archaeological Investigation ◽  
X Ray ◽  
Parish Church ◽  
Materials Used ◽  
Santa Maria ◽  
The Church ◽  
Scanning Electron

From the 1950s and 1960s of the last century, a parish church dating back to the 6th century AD was identified during reclamation works of Valle Pega. The archaeological investigation allowed the recovery of the parish and the attached baptistery, as well as some tombs closely connected to the church. Following the excavation, it was possible to collect some samples of bricks and mortars in order to identify the different compositions of the materials used for the construction of the parish. All the samples were analyzed through optical microscopy, X-ray powder diffractometric analysis and observation through scanning electron microscope. Thanks to the investigations carried out on the samples, it was possible to hypothesize the different construction phases and the different materials used and to identify the firing temperatures at which the bricks were built.

Characterization of Thai Amulets: A PIXE Study

2011 ◽  
Vol 324 ◽  
pp. 505-508 ◽  
Author(s):  
Krit Won-In ◽  
Songtam Suksawang ◽  
Sawet Intarasiri ◽  
Chom Thongleurm ◽  
Teerasak Kamwanna ◽  
...  
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Emission Spectroscopy ◽  
Energy Dispersive ◽  
X Ray ◽  
Two Samples ◽  
Fluorescence Spectrometer ◽  
First Time ◽  
Scanning Electron

The Thai amulets that created in an image of Lord Buddha meditation were made to explain the Dharma of Buddha and believed to bless every life in this world for good karma. Phra Somdej Wat Rakhang amulet is the top of the five most famous Thai amulets. There are many molds with various compositions. In this work, it was the first time that X-ray fluorescence spectrometry methods; scanning electron microscope cooperated with energy dispersive X-ray fluorescence spectrometer (SEM/EDS) and particle induced X-ray emission spectroscopy (PIXE) were carried out to analyze their compositions. Two samples were collected from different molds. Results revealed C, Ca and Si were main composition. The differences in their compositions have been used to identify and characterize for each molds.

Synthesis and Characterization of Metal and Semiconductor Nanowires

2013 ◽  
Vol 201 ◽  
pp. 21-64 ◽  
Author(s):  
Hardev Singh Virk
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Anodic Alumina ◽  
X Ray ◽  
Tunneling Diode ◽  
Laboratory Characterization ◽  
Potential Applications ◽  
Dual Source ◽  
Scanning Electron

One-dimensional nanowires (NWs) have attracted considerable attention in recent years because of their novel physical properties and potential applications as interconnects in nanometre-scale electronics. NWs have potential applications in nanoscale electronics, optoelectronics, photonics, sensors, and solar cells due to their unique electrical, chemical, and optical properties. Several chemical and physical methods are commonly used to produce NWs. Among them, electrochemical synthesis and vapour-liquid-solid (VLS) methods to produce NWs have become popular among scientific workers due to a number of advantages. Synthesis of NWs using anodic alumina and polymer templates in an electrochemical cell has been described in detail as investigated in our laboratory. Characterization of metal and semiconductor NWs has been accomplished using scanning electron microscope (SEM), field emission scanning electron microscope (FESEM), high resolution transmission microscope (HRTEM), X-ray diffraction (XRD), and energy dispersive X-ray analysis (EDAX). Morphology of NWs has been revealed by SEM, structure by TEM, crystallinity by XRD and chemical composition by EDAX. I-V characteristics of copper and semiconductor NWs were recorded in-situ, as grown in pores of anodic alumina template, using Dual Source Meter (Keithley Model 4200 SCS) with platinum probes for contacts. Resonating tunneling diode (RTD) characteristics of fabricated NWs have been investigated. Bulk production of Copper NWs has been described by seed growth technique. Applications of NWs are not covered in any detail under this review. Table of Contents

Mimicking the Formation of Biomineral Composites through Deposition of Calcium Carbonate Thin-Films on Modified Fiber Net Templates

2003 ◽  
Vol 774 ◽  
Author(s):  
Parayil Kumaran Ajikumar ◽  
Rajamani Lakshminarayanan ◽  
Valiyaveettil Suresh
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Electron Microscope ◽  
Calcium Carbonate ◽  
Scanning Electron Microscope ◽  
X Ray Diffraction ◽  
X Ray ◽  
Controlled Deposition ◽  
Scanning Electron

AbstractThin films of calcium carbonate were deposited on the surfaces of synthetic substrates using a simple biomimetic pathway. The Nylon 66 fiber knit pre-adsorbed with acidic polymers was used as a template for the controlled deposition of CaCO3 thin film. The presence of the soluble macromolecules on the fiber knit surface was characterized using ATR-FTIR spectroscopy. The characterization of the mineral films was carried out using scanning electron microscope (SEM), X-ray diffraction (XRD) and energy dispersive Xray scattering (EDX) studies.

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