Flexural Properties of T700 2D Cf/SiC Composites via Precursor Infiltration and Pyrolysis

2015 ◽  
Vol 816 ◽  
pp. 152-156
Author(s):  
Xin Ma ◽  
Xin Bo He ◽  
Hai Feng Hu ◽  
Yu Di Zhang ◽  
Yong Li

2D Cf/SiC composites were prepared by precursor infiltration and pyrolysis (PIP) process with spreaded T700-12K plain weave carbon clothes as the reinforcement. The mechanical properties and microstructures were investigated. The composites are compact with few internal defects since the precursor could infiltrate the preform effectively. CVD-PyC interface modified the surface of T700 carbon fiber, a rough surface is helpful for the interfacial combination and the load transfer. For the Cf/PyC/SiC composites, the flexural strength and flexural modulus were 425±23.2 MPa and 36.3±3.1 GPa, respectively.

2017 ◽  
Vol 726 ◽  
pp. 137-142 ◽  
Author(s):  
Zhi Hua Chen ◽  
Si'an Chen ◽  
Jin Tai Wu ◽  
Hai Feng Hu ◽  
Yu Di Zhang

The reainforcement of T700 carbon fiber was oxidized at 400°C, as-received and treated carbon fiber reinforced mini Cf/SiC matrix composites were fabricated by precursor infiltration and pyrolysis (PIP) method. The mechanical properties of the composites were determined and compared. The results showed that with the time of oxidation increased, the flexural strength of composites decreased. The flexural modulus and tensile modulus were increased by the 87.8 GPa to 92.9 GPa and 131 GPa to 150 GPa. Without oxidation pretreatment, the composites represented maximum flexural strength of 649 MPa. For 1h oxidation, the composites reached the maximum tensile strength of 821 MPa. However, carbon fiber pre-oxidation for 2h, C/SiC composites mechanical properties appeared to reduce seriously.


2011 ◽  
Vol 675-677 ◽  
pp. 779-782 ◽  
Author(s):  
Si’an Chen ◽  
Hai Feng Hu ◽  
Chang Rui Zhang ◽  
Yu Di Zhang ◽  
Xin Bo He ◽  
...  

Chemical liquid-vapor deposition (CLVD) process is a new style of fast densification, which combines the advantages of PIP process and CVI process. 2D C/SiC composites were prepared at 800~1200°C for 3~4 hours with liquid polycarbosilane and carbon fiber cloth by CLVD process with induction heating, and had the density of 1.7 g/cm3, the flexural strength of 84.6MPa, and the flexural modulus of 20GPa. XRD pattern of the sample proved that the matrix was β-SiC. It was found that SiC deposited mainly around single fiber instead of among fiber bundles and layers.


2021 ◽  
pp. 002199832110316
Author(s):  
IA Abdulganiyu ◽  
INA Oguocha ◽  
AG Odeshi

The effects of microfiller addition on the flexural properties of carbon fiber reinforced phenolic (CFRP) matrix composites were investigated. The CFRP was produced using colloidal silica and silicon carbide (SiC) microfillers, 2 D woven carbon fibers, and two variants of phenolic resole (HRJ-15881 and SP-6877). The resins have the same phenol and solid content but differ in their viscosities and HCHO (formaldehyde) content. The weight fractions of microfillers incorporated into the phenolic matrix are 0.5 wt.%, 1 wt.%, 1.5 wt.%, and 2 wt.%. Flexural properties were determined using a three-point bending test and the damage evolution under flexural loading was investigated using optical and scanning electron microscopy. The results indicated that the reinforcement of phenolic resins with carbon fibers increased the flexural strength of the HRJ-15881 and SP-6877 by 508% and 909%, respectively. The flexural strength of the CFRP composites further increased with the addition of SiC particles up to 1 wt.% SiC but decreased with further increase in the amount of SiC particles. On the other hand, the flexural modulus of the CFRP composites generally decreased with the addition of SiC microfiller. Both the flexural strength and flexural modulus of the CFRP did not improve with the addition of colloidal silica particles. The decrease in flexural properties is caused by the agglomeration of the microfillers, with colloidal silica exhibiting more tendency for agglomeration than SiC. The fractured surfaces revealed fiber breakage, matrix cracking, and delamination under flexural loading. The tendency for failure worsened at microfiller addition of ≥1.5 wt.%.


2021 ◽  
Vol 2021 ◽  
pp. 1-11
Author(s):  
K. B. Prakash ◽  
Yahya Ali Fageehi ◽  
Rajasekaran Saminathan ◽  
P. Manoj Kumar ◽  
S. Saravanakumar ◽  
...  

There is more demand for natural fiber-reinforced composites in the energy sector, and their impact on the environment is almost zero. Natural fiber has plenty of advantages, such as easy recycling and degrading property, low density, and low price. Natural fiber’s thermal properties and flexural properties are less than conventional fiber. This work deals with the changes in the thermal properties and mechanical properties of S-glass reinforced with a sodium hydroxide-treated pineapple leaf (PALF) and banana stem fibers. Banana stem and pineapple leaf fibers (PALF) were used at various volume fractions, i.e., 30%, 40%, and 50%, and various fiber lengths of 20 cm, 30 cm, and 40 cm with S-glass, and their effects on the thermal and mechanical properties were studied, and their optimum values were found. It was evidenced that increasing the fiber volume and fiber length enhanced the flexural and thermal properties up to 40% of the fiber volume, and started to decrease at 50% of the fiber volume. The fiber length provides an affirmative effect on the flexural properties and a pessimistic effect on the thermal properties. The PALF S-glass combination of 40% fiber load and 40 cm fiber length provides maximum flexural strength, flexural modulus, storage modulus, and lowest loss modulus based on hybrid Taguchi grey relational optimization techniques. PALF S-glass hybrid composite has been found to have 7.80%, 3.44%, 1.17% higher flexural strength, flexural modulus, and loss modulus, respectively, and 15.74% lower storage modulus compared to banana S-glass hybrid composite.


2019 ◽  
Vol 809 ◽  
pp. 41-46
Author(s):  
Franz Habla ◽  
M. Kropka ◽  
M. Muehlbacher ◽  
T. Neumeyer ◽  
Volker Altstädt

In this study, the quality of pre-consolidation of a PA6 based glass/carbon hybrid and a glass mono-material UD-tape laminate has been analyzed and the influence of the pre-consolidation step on flexural properties of end-consolidated laminates was determined. For this reason, three different pre-consolidation qualities were mechanically and optically analyzed. The investigations show that the quality of pre-consolidation is not critical for mono-material lay-ups considered in this work. However, the pre-consolidation step has a significant effect on the flexural properties of the hybrid-material laminate presented in this work. The flexural modulus is increased by more than 25 % and the flexural strength up to 9 % due to better welding of the distinct layers. Additionally, the influence of carbon fiber share on the flexural modulus of the UD hybrid-material was examined. It could be recognized that the flexural modulus can be increased up to 171 % by the exchange of glass with carbon fiber layers with a sandwich stacking compared to glass mono-material with constant thickness.


2007 ◽  
Vol 546-549 ◽  
pp. 1509-1514 ◽  
Author(s):  
G.H. Zhou ◽  
Shi Wei Wang ◽  
Xiao Xian Huang ◽  
Jing Kun Guo

Unidirectional carbon fiber reinforced fused silica (uni-Cf/SiO2) composite was prepared by slurry infiltration and hot-pressing. The room and elevated temperatures flexural properties were investigated and the fracture features of the composite were observed. This composite exhibited non-catastrophic failure at room and elevated temperatures. The oxidation of carbon fiber at elevated temperatures was the main reason for the degradation of flexural strength and elastic modulus. The flexural strength tested at 1200 was 376MPa and exhibited anomalously higher than that at 1000 (277MPa), which was attributed to the viscous flow of fused silica matrix and therefore the occurrence of microcracking in the matrix was deferred. And it was inferred that the brittle to plastic transition temperature (Tb-p) of uni-Cf/SiO2 composite corresponded to a certain temperature around 1200°C.


2018 ◽  
Vol 281 ◽  
pp. 408-413 ◽  
Author(s):  
Wei Jie Xie ◽  
Hai Peng Qiu ◽  
Ming Wei Chen ◽  
Shan Hua Liu

The purpose of this study was to investigate the influence of carbon fiber treatment on flexural properties of carbon fiber reinforced SiC matrix (C/SiC) composites. C/SiC composites were prepared by polymer impregnation pyrolysis (PIP) progress with polycarbosilane (PCS) as impregnant and carbon fiber as reinforcement. The flexural strength at room temperature of the 2D laminated composites were measured and analyzed with different carbon fiber treatment process. It was found that the flexural strength of the composites with carbon fibers coated by pyrolytic carbon was 53.5% higher than that with non-coated carbon fibers. The results also show that the flexural strength of the composites with 1600°C heat treated carbon fibers increased by 25.4% compared with the composites with non-heat treated fibers.


2019 ◽  
Vol 8 (1) ◽  
pp. 484-492 ◽  
Author(s):  
Yinqiu Wu ◽  
Bolin Tang ◽  
Kun Liu ◽  
Xiaoling Zeng ◽  
Jingjing Lu ◽  
...  

Abstract The reinforcing effect of graphene oxide (GO) in enhancing the flexural strength and flexural modulus of aramid fiber (AF)/epoxy composites were investigated with GO-AFs at a weight fraction of 0.1-0.7%. The flexural strength and flexural modulus of the composite reached 87.16 MPa and 1054.7 MPa, respectively, which were about 21.19% and 40.86% higher than those of the pure epoxy resin, respectively. In addition, the flexural properties and interfacial shear strength (IFSS) of composite reinforced by GO-AFs were much higher than the composites reinforced by AFs due to GO improved the interfacial bonding between the reinforcement material and matrix.


2021 ◽  
pp. 002199832110047
Author(s):  
Mahmoud Mohamed ◽  
Siddhartha Brahma ◽  
Haibin Ning ◽  
Selvum Pillay

Fiber prestressing during matrix curing can significantly improve the mechanical properties of fiber-reinforced polymer composites. One primary reason behind this improvement is the generated compressive residual stress within the cured matrix, which impedes cracks initiation and propagation. However, the prestressing force might diminish progressively with time due to the creep of the compressed matrix and the relaxation of the tensioned fiber. As a result, the initial compressive residual stress and the acquired improvement in mechanical properties are prone to decline over time. Therefore, it is necessary to evaluate the mechanical properties of the prestressed composites as time proceeds. This study monitors the change in the tensile and flexural properties of unidirectional prestressed glass fiber reinforced epoxy composites over a period of 12 months after manufacturing. The composites were prepared using three different fiber volume fractions 25%, 30%, and 40%. The results of mechanical testing showed that the prestressed composites acquired an initial increase up to 29% in the tensile properties and up to 32% in the flexural properties compared to the non-prestressed counterparts. Throughout the 12 months of study, the initial increase in both tensile and flexural strength showed a progressive reduction. The loss ratio of the initial increase was observed to be inversely proportional to the fiber volume fraction. For the prestressed composites fabricated with 25%, 30%, and 40% fiber volume fraction, the initial increase in tensile and flexural strength dropped by 29%, 25%, and 17%, respectively and by 34%, 26%, and 21%, respectively at the end of the study. Approximately 50% of the total loss took place over the first month after the manufacture, while after the sixth month, the reduction in mechanical properties became insignificant. Tensile modulus started to show a very slight reduction after the fourth/sixth month, while the flexural modulus reduction was observed from the beginning. Although the prestressed composites displayed time-dependent losses, their long-term mechanical properties still outperformed the non-prestressed counterparts.


Polymers ◽  
2021 ◽  
Vol 13 (14) ◽  
pp. 2268
Author(s):  
Pavel V Kosmachev ◽  
Vladislav O Alexenko ◽  
Svetlana A Bochkareva ◽  
Sergey V Panin

Laminated composites based on polyetheretherketone (PEEK) and polyimide (PI) matrices were fabricated by hot compression. Reinforcing materials (unidirectional carbon-fiber (CF) tapes or carbon fabric) and their layout patterns were varied. Stress–strain diagrams after three-point flexural tests were analyzed, and both lateral faces of the fractured specimens and fractured surfaces (obtained by optical and scanning electron microscopy, respectively) were studied. It was shown that the laminated composites possessed the maximum mechanical properties (flexural elastic modulus and strength) in the case of the unidirectional CF (0°/0°) layout. These composites were also not subjected to catastrophic failure during the tests. The PEEK-based composites showed twice the flexural strength of the PI-based ones (0.4 and 0.2 GPa, respectively), while the flexural modulus was four times higher (60 and 15 GPa, correspondently). The reason was associated with different melt flowability of the used polymer matrices and varied inter- (intra)layer adhesion levels. The effect of adhesion was additionally studied by computer simulation using a developed two-dimensional FE-model. It considered initial defects between the binder and CF, as well as subsequent delamination and failure under loads. Based on the developed FE-model, the influence of defects and delamination on the strength properties of the composites was shown at different stress states, and the corresponding quantitative estimates were reported. Moreover, another model was developed to determine the three-point flexural properties of the composites reinforced with CF and carbon fabric, taking into account different fiber layouts. It was shown within this model framework that the flexural strength of the studied composites could be increased by an order of magnitude by enhancing the adhesion level (considered through the contact area between CF and the binder).


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