Three-Dimensional Microstructure Reconstruction and Phase Boundary by Serial Sectioning and Numerical Approach

2017 ◽  
Vol 899 ◽  
pp. 395-399
Author(s):  
Daniele Aparecida Nogueira ◽  
Aline Aguiar Lopes ◽  
Wesley Luiz Conegundes ◽  
Fabiane Roberta Freitas Silva ◽  
Daniel Rodrigues ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Phase Boundary ◽  
Three Dimensional ◽  
Numerical Approach ◽  
Boundary Structure ◽  
Powder Materials ◽  
Serial Sectioning ◽  
Stainless Steel 316L ◽  
Volume Fractions ◽  
Morphological Aspects

The microstructure and pores of the consolidated powder materials are important to determine the final properties of the pieces produced. Therefore, the control of their volume fractions and morphologies represent actual technological challenges. Besides the quantification of the phase and pores volume fractions there are important features related with the morphological aspects and the phase boundary structure that reveals the mechanisms of properties improvements, which are crucial for development of materials obtained by powder metallurgy techniques. In this paper, stereological measurements of pores present in the material stainless steel (316L) are obtained by combining serial sectioning technique and optical microscopy (OM). Dilatometric experiments were carried out in order to simulate heat treatment for sintering the material. The 3D microstructures are obtained by images reconstruction using numerical pixels treatment and stereological results of the porosities are presented.

scholarly journals Heat treatment effects on three-dimensional morphology of chromium carbide in AISI D2 tool steel studied by serial sectioning method

2018 ◽  
Author(s):  
Seyedeh Mastooreh Seyedi Ghezghapan
Keyword(s):  
Heat Treatment ◽  
Chromium Carbide ◽  
Tool Steel ◽  
Treatment Effects ◽  
Three Dimensional ◽  
Serial Sectioning ◽  
Tempering Temperature ◽  
Sectioning Method ◽  
Aisi D2 ◽  
Aisi D2 Tool Steel

We developed a three-dimensional microstructure analysis system based on the manual serial sectioning method to evaluate the heat treatment effects on chromium carbide size and morphology in AISI D2 tool steel. Two heat treatment factors, austenitizing and tempering temperature were investigated. The results show that increasing in austenitizing temperature leads to further carbide precipitation after the tempering process and increasing in the tempering temperature causes precipitate smaller secondary carbides even more than the primary carbides.

Analyzing the Impact of X-Ray Tomography on the Reliability of Integrated Circuits

2015 ◽  
Author(s):  
Halit Dogan ◽  
Md Mahbub Alam ◽  
Navid Asadizanjani ◽  
Sina Shahbazmohamadi ◽  
Domenic Forte ◽  
...  
Keyword(s):  
Integrated Circuits ◽  
Integrated Circuit ◽  
3D Imaging ◽  
Three Dimensional ◽  
Serial Sectioning ◽  
Promising Technique ◽  
Flash Memories ◽  
X Ray ◽  
3D Information ◽  
The Impact

Abstract X-ray tomography is a promising technique that can provide micron level, internal structure, and three dimensional (3D) information of an integrated circuit (IC) component without the need for serial sectioning or decapsulation. This is especially useful for counterfeit IC detection as demonstrated by recent work. Although the components remain physically intact during tomography, the effect of radiation on the electrical functionality is not yet fully investigated. In this paper we analyze the impact of X-ray tomography on the reliability of ICs with different fabrication technologies. We perform a 3D imaging using an advanced X-ray machine on Intel flash memories, Macronix flash memories, Xilinx Spartan 3 and Spartan 6 FPGAs. Electrical functionalities are then tested in a systematic procedure after each round of tomography to estimate the impact of X-ray on Flash erase time, read margin, and program operation, and the frequencies of ring oscillators in the FPGAs. A major finding is that erase times for flash memories of older technology are significantly degraded when exposed to tomography, eventually resulting in failure. However, the flash and Xilinx FPGAs of newer technologies seem less sensitive to tomography, as only minor degradations are observed. Further, we did not identify permanent failures for any chips in the time needed to perform tomography for counterfeit detection (approximately 2 hours).

Modeling and Assessment of the Produced Water Discharges from Offshore Petroleum Platforms

2007 ◽  
Vol 42 (4) ◽  
pp. 303-310 ◽  
Author(s):  
Zhi Chen ◽  
Lin Zhao ◽  
Kenneth Lee ◽  
Charles Hannath
Keyword(s):  
Random Walk ◽  
Produced Water ◽  
Model Development ◽  
Three Dimensional ◽  
Monitoring Program ◽  
Ecological Monitoring ◽  
Numerical Approach ◽  
Ocean Model ◽  
Scale Model ◽  
Water Stream

Abstract There has been a growing interest in assessing the risks to the marine environment from produced water discharges. This study describes the development of a numerical approach, POM-RW, based on an integration of the Princeton Ocean Model (POM) and a Random Walk (RW) simulation of pollutant transport. Specifically, the POM is employed to simulate local ocean currents. It provides three-dimensional hydrodynamic input to a Random Walk model focused on the dispersion of toxic components within the produced water stream on a regional spatial scale. Model development and field validation of the predicted current field and pollutant concentrations were conducted in conjunction with a water quality and ecological monitoring program for an offshore facility located on the Grand Banks of Canada. Results indicate that the POM-RW approach is useful to address environmental risks associated with the produced water discharges.

scholarly journals Charge algebra in Al(A)dSn spacetimes

2021 ◽  
Vol 2021 (5) ◽  
Author(s):  
Adrien Fiorucci ◽  
Romain Ruzziconi
Keyword(s):  
Boundary Conditions ◽  
Dirichlet Boundary ◽  
Three Dimensional ◽  
Dirichlet Boundary Conditions ◽  
Boundary Structure ◽  
Asymptotic Symmetry ◽  
Renormalization Procedure ◽  
Field Dependent ◽  
Odd Dimensions

Abstract The gravitational charge algebra of generic asymptotically locally (A)dS spacetimes is derived in n dimensions. The analysis is performed in the Starobinsky/Fefferman-Graham gauge, without assuming any further boundary condition than the minimal falloffs for conformal compactification. In particular, the boundary structure is allowed to fluctuate and plays the role of source yielding some symplectic flux at the boundary. Using the holographic renormalization procedure, the divergences are removed from the symplectic structure, which leads to finite expressions. The charges associated with boundary diffeomorphisms are generically non-vanishing, non-integrable and not conserved, while those associated with boundary Weyl rescalings are non-vanishing only in odd dimensions due to the presence of Weyl anomalies in the dual theory. The charge algebra exhibits a field-dependent 2-cocycle in odd dimensions. When the general framework is restricted to three-dimensional asymptotically AdS spacetimes with Dirichlet boundary conditions, the 2-cocycle reduces to the Brown-Henneaux central extension. The analysis is also specified to leaky boundary conditions in asymptotically locally (A)dS spacetimes that lead to the Λ-BMS asymptotic symmetry group. In the flat limit, the latter contracts into the BMS group in n dimensions.

Simulation of small-angle scattering curves by numerical Fourier transformation

2007 ◽  
Vol 40 (1) ◽  
pp. 16-25 ◽  
Author(s):  
Klaus Schmidt-Rohr
Keyword(s):  
Form Factor ◽  
Small Angle ◽  
Fourier Transformation ◽  
Three Dimensional ◽  
Power Laws ◽  
Numerical Approach ◽  
Peak Position ◽  
Two Dimensions ◽  
Correlation Peak ◽  
Scattering Intensity

A simple numerical approach for calculating theq-dependence of the scattering intensity in small-angle X-ray or neutron scattering (SAXS/SANS) is discussed. For a user-defined scattering density on a lattice, the scattering intensityI(q) (qis the modulus of the scattering vector) is calculated by three-dimensional (or two-dimensional) numerical Fourier transformation and spherical summation inqspace, with a simple smoothing algorithm. An exact and simple correction for continuous rather than discrete (lattice-point) scattering density is described. Applications to relatively densely packed particles in solids (e.g.nanocomposites) are shown, where correlation effects make single-particle (pure form-factor) calculations invalid. The algorithm can be applied to particles of any shape that can be defined on the chosen cubic lattice and with any size distribution, while those features pose difficulties to a traditional treatment in terms of form and structure factors. For particles of identical but potentially complex shapes, numerical calculation of the form factor is described. Long parallel rods and platelets of various cross-section shapes are particularly convenient to treat, since the calculation is reduced to two dimensions. The method is used to demonstrate that the scattering intensity from `randomly' parallel-packed long cylinders is not described by simple 1/qand 1/q4power laws, but at cylinder volume fractions of more than ∼25% includes a correlation peak. The simulations highlight that the traditional evaluation of the peak position overestimates the cylinder thickness by a factor of ∼1.5. It is also shown that a mix of various relatively densely packed long boards can produceI(q) ≃ 1/q, usually observed for rod-shaped particles, without a correlation peak.

scholarly journals Modelling of Applied Magnetic Field and Thermal Radiations Due to the Stretching of Cylinder

Processes ◽  
2021 ◽  
Vol 9 (6) ◽  
pp. 1077
Author(s):  
Muhammad Tamoor ◽  
Muhammad Kamran ◽  
Sadique Rehman ◽  
Aamir Farooq ◽  
Rewayat Khan ◽  
...  
Keyword(s):  
Heat Transfer ◽  
Fluid Velocity ◽  
Three Dimensional ◽  
Numerical Approach ◽  
Skin Friction Coefficient ◽  
Physical Parameters ◽  
Boundary Layer Equations ◽  
Convective Parameter ◽  
Momentum And Heat Transfer ◽  
Dimensional Boundary

In this study, a numerical approach was adopted in order to explore the analysis of magneto fluid in the presence of thermal radiation combined with mixed convective and slip conditions. Using the similarity transformation, the axisymmetric three-dimensional boundary layer equations were reduced to a self-similar form. The shooting technique, combined with the Range–Kutta–Fehlberg method, was used to solve the resulting coupled nonlinear momentum and heat transfer equations numerically. When physically interpreting the data, some important observations were made. The novelty of the present study lies in finding help to control the rate of heat transfer and fluid velocity in any industrial manufacturing processes (such as the cooling of metallic plates). The numerical results revealed that the Nusselt number decrease for larger Prandtl number, curvature, and convective parameters. At the same time, the skin friction coefficient was enhanced with an increase in both slip velocity and convective parameter. The effect of emerging physical parameters on velocity and temperature profiles for a nonlinear stretching cylinder has been thoroughly studied and analyzed using plotted graphs and tables.

scholarly journals A Numerically Supported Investigation of the 3D Flow in Centrifugal Impellers: Part I — The Validation Base

1996 ◽  
Author(s):  
Ch. Hirsch ◽  
S. Kang ◽  
G. Pointel
Keyword(s):  
Boundary Layer ◽  
Three Dimensional ◽  
Boundary Layer Separation ◽  
Numerical Approach ◽  
Secondary Flows ◽  
Pump Impeller ◽  
High Loss ◽  
Leakage Flows ◽  
Fine Mesh ◽  
Radial Pump

The three-dimensional flow in centrifugal impellers is investigated on the basis of a detailed analysis of the results of numerical simulations. In order to gain confidence in this process, an in-depth validation is performed, based on computations of Krain’s centrifugal compressor and of a radial pump impeller, both with vaneless diffusers. Detailed comparisons with available experimental data provide high confidence in the numerical tools and results. The appearance of a high loss ‘wake’ region results from the transport of boundary layer material from the blade surfaces to the shroud region and its location depends on the balance between secondary and tip leakage flows and is not necessarily connected to 3D boundary layer separation. Although the low momentum spots near the shroud can interfere with 3D separated regions, the main outcome of the present analysis is that these are two distinct phenomena. Part I of this paper focuses on the validation base of the numerical approach, based on fine mesh simulations, while Part II presents an analysis of the different contributions to the secondary flows and attempts to estimate their effect on the overall flow pattern.

Thermal jet drilling of granite rock: a numerical 3D finite-element study

2021 ◽  
Vol 379 (2196) ◽  
pp. 20200128
Author(s):  
Timo Saksala ◽  
Reijo Kouhia ◽  
Ahmad Mardoukhi ◽  
Mikko Hokka
Keyword(s):  
Finite Elements ◽  
Numerical Study ◽  
Thermal Flux ◽  
Three Dimensional ◽  
Numerical Approach ◽  
Mass Scaling ◽  
Granite Rock ◽  
Fracture Dynamics ◽  
Rock Heterogeneity ◽  
Thermal Drilling

This paper presents a numerical study on thermal jet drilling of granite rock that is based on a thermal spallation phenomenon. For this end, a numerical method based on finite elements and a damage–viscoplasticity model are developed for solving the underlying coupled thermo-mechanical problem. An explicit time-stepping scheme is applied in solving the global problem, which in the present case is amenable to extreme mass scaling. Rock heterogeneity is accounted for as random clusters of finite elements representing rock constituent minerals. The numerical approach is validated based on experiments on thermal shock weakening effect of granite in a dynamic Brazilian disc test. The validated model is applied in three-dimensional simulations of thermal jet drilling with a short duration (0.2 s) and high intensity (approx. 3 MW m −2 ) thermal flux. The present numerical approach predicts the spalling as highly (tensile) damaged rock. Finally, it was shown that thermal drilling exploiting heating-forced cooling cycles is a viable method when drilling in hot rock mass. This article is part of the theme issue ‘Fracture dynamics of solid materials: from particles to the globe’.

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