scholarly journals The Effect of Adding Halloysite Nanotubes as Filler on the Mechanical Properties of Low-Density Polyethylene

2018 ◽  
Vol 919 ◽  
pp. 144-151 ◽  
Author(s):  
Ľudmila Dulebová ◽  
Karolina Glogowska ◽  
Jaroslav Hájek ◽  
Jakub Fic

Reinforcing thermoplastic polymers with nanotubes or nanoplatelets to form nanocomposites is a way to increase the usage of polymeric materials in engineering applications by improving their mechanical properties. The contribution presents the results of research from basic processing and mechanical properties of nanocomposites. Low-Density Polyethylene (LDPE) was used as a matrix for experiments. The material LDPE was modified by Halloysite nanotubes (HNT) with a mass share of 2, 4, 6 wt% of the matrix. Nanocomposites were filled with 5 wt% Polyethylene grafted with maleic anhydride (PE-graft-MA) as a compatibilizer. The specimens were prepared by injection molding and their selected mechanical properties were tested by static tensile test, Charpy impact test and Shore hardness test.

2016 ◽  
Vol 851 ◽  
pp. 168-172
Author(s):  
Yustiasih Purwaningrum ◽  
Triyono ◽  
Tegar Rileh Argihono ◽  
Ryan Sutrisno

Mechanical and microstructure of double side weld with various angle groove was studied in this research. LR Gr A steel plates (12 mm thickness) were welded using GMAW with corresponding 180 A, 23 V, and 20 l/min respectively with current, voltage, and gas flow. Shielding gas and filler metals used are argon and ER 70S-6. The angle groove that used were 20⁰, 40⁰ and 60⁰. The measured of mechanical properties with regard to hardness, toughness and strength using, Vickers hardness test, Charpy impact test and tensile test respectively The microstructure examined with optical microscope. The results show that the highest hardness values found in welds with groove angle 40ͦ. The transition temperatures of weld metals are at temperatures between -20°C to 0°C. Weld metals with all variations of the groove angle has a value of less than 0.1 mmpy. Microstructure of base metals and HAZ were ferrite and pearlite. While the microstructure of weld metals are accicular ferrite, grain boundary ferrite and Widmanstatten ferrite.


2020 ◽  
Vol 12 (4) ◽  
pp. 531-537 ◽  
Author(s):  
Hyun-Joon Park ◽  
Byung-Wook Ahn ◽  
Jae-Ha Kim ◽  
Jong-Gun Lee ◽  
Seung-Boo Jung

AA6061-T4 composites containing SiC and B4C particles were fabricated by friction stir processing (FSP) with an SKD11 tool. The microstructures and mechanical properties of the composites were investigated with various test methods. With the inclusion of ceramic particles, refined grains in the stir zone (SZ) were observed using a scanning electron microscope (SEM) and tunneling electron microscope (TEM). Because the ceramic particles facilitated grain refinement in the SZ via the pinning effect, the SZ with the particles had a much smaller grain size than the SZ without the particles. Vickers hardness test, tensile test and Charpy impact test were conducted to evaluate the mechanical properties. Mechanical properties of the SZ with the ceramic particles were improved relative to those of the SZ without the particles. Vickers hardness (from 50 to 90 HV), tensile strength (from 117 to 253 MPa) and Charpy impact absorbed energy (from 4.2 to 5.6 J) of the SZ increased with the addition of ceramic particles.


2019 ◽  
Vol 952 ◽  
pp. 180-187
Author(s):  
Martin Reznicek ◽  
Dagmar Měřínská ◽  
Martin Ovsik ◽  
Michal Stanek ◽  
Adam Dockal ◽  
...  

Modification of polymers by fillers is one of the most used material alterations to improve its required properties. This article is about modification of polymer matrix by fillers with layered particles. Linear low density polyethylene (LLDPE) was used as matrix and it was mixed with different kinds of fillers. Fillers used were: CaPhP – Calcium Phenylphosphonate, double layered hydroxides (ZnAl-DDS, ZnAl-lac and ZnAl-CO3) and natural Talc. Individual fillers were mixed into the matrix by kneading machine with the use of several velocities. The article focuses on influence of the individual filler on mechanical properties measured by tensile strength test. This paper also investigates the problem of process parameters’ influence on final mechanical properties and later confirms positive impact of all fillers that were used, although the size of them differs.


2016 ◽  
Vol 835 ◽  
pp. 167-172
Author(s):  
Yustiasih Purwaningrum ◽  
Triyono ◽  
Tegar Rileh Argihono ◽  
Ryan Sutrisno

The effects of root opening process parameters on the phisical and mechanical properties of mild steel specimens of grade LR Gr A having dimensions 200 mm× 100 mm× 12 mm, welded by gas metal arc welding were investigated. The variation of root opening that used were 3 mm, 5 mm and 7 mm. The physical properties examined with regard with microstructure, macrosructure, and corrosion using optical microscope and stereozoom. The measured of mechanical properties with regard to strength, hardness and toughness using, tensile test, Vickers hardness Test, and Charpy impact test. The test results show the base metal had a hardness of approximately 110 VHN and a maximum hardness of approximately 190 VHN that corellates with microstructure of weld metals. Microstructure of base metal and HAZ are ferite and perlite, while microstructure of weld zone are acicular ferrite and grain boundary ferrite. The corrosion rate of weld metals with various root opening categorized as materials having excellent corrosion resistance value. Welding joints with opening roots 3 mm and 5 mm can be used for construction. All welded specimens exhibited fracture at base metals


2017 ◽  
Vol 7 ◽  
pp. 184798041771592 ◽  
Author(s):  
Bei Su ◽  
Ying-Guo Zhou ◽  
Hai-Hong Wu

The mechanical blending of polypropylene and low-density polyethylene is an economical and simple method for producing new polymeric materials for specific applications. However, the reduction in mechanical properties of the blend is one of its main shortcomings. In this study, a filler masterbatch including nano-silicon dioxide, compatibilizer, lubricant agent, and antioxidant agent was prepared, and polypropylene–low-density polyethylene composite parts with different content of filler masterbatch were fabricated and tested for mechanical properties at two tensile test speeds. Also, to investigate the underlying mechanism of the mechanical properties improvement, the tested samples were carefully analyzed and compared and further characterized by scanning electron microscopy and differential scanning calorimetry. The results indicate that the mechanical properties, including tensile strength, moduli, and elongation, can be all drastically improved simultaneously with the addition of the filler masterbatch. The results also suggest that the compatibility of the two phases increases with the increase in the filler masterbatch, and the crystal size decreases and distribution uniforms owing to the addition of the filler masterbatch. Furthermore, it was also found that there is a close relationship between the mechanical properties and morphological structures, which are improved by the existence of the filler masterbatch.


2012 ◽  
Vol 576 ◽  
pp. 366-369 ◽  
Author(s):  
Siti Khadijah Alias ◽  
Bulan Abdullah ◽  
Ahmed Jaffar ◽  
Abdul Hakim Abdullah ◽  
Norhisyam Jenal

The studies emphasis on the development of niobium alloyed ductile iron with higher strength comparing to unalloyed ductile iron. 0.5wt% to 2wt% niobium were added into mixture of ductile iron casting containing pig iron, carburizer and steel scrap, and nodulized through 1.6wt% Fe-Si-Mg addition in CO2 sand casting process. Samples were then machined according to TS EN 10001 standards for tensile test and ASTM E23 for Charpy impact test. In addition, Rockwell hardness test was also performed. Microstructure observations were made after 2% Nital chemical etched and the phase structures were validated through XRD analysis. It was found that addition of niobium in ductile iron provide significant enhancement in mechanical properties when compared to unalloyed ductile iron. Addition of higher amount of niobium had further increased the strength and impact toughness properties. The enhancement of the mechanical properties is expected to further expand the applications of ductile iron.


2011 ◽  
Vol 383-390 ◽  
pp. 3313-3319 ◽  
Author(s):  
Bulan Abdullah ◽  
Siti Khadijah Alias ◽  
Ahmed Jaffar ◽  
Farisol Abd Rahim ◽  
Abdullah Ramli

The purpose of this research is to investigate the mechanical and corrosion characteristics of Ni-Cu alloyed Austempered Ductile Iron before and after austempering process. Specimens of ductile iron and 0.5% Cu-Ni ductile iron were produced through conventional CO2 sand casting method. The specimens were then austenitized at 9000C before austempered at 3500C at three different holding times which were 1 hour, 2 hours and 3 hours subsequently. The corrosion characteristics of newly developed material were obtained by means of polarization test and the mechanical testing involved tensile test (TS 138 EN1002-1), Rockwell hardness test and Charpy Impact test (ASTM E23). Density test as well as microstructure and SEM observations were also done to ductile iron and Cu-Ni alloyed ductile iron samples. All the testing was done to both as cast and austempered specimens. Addition of copper and Nickel was found to slightly increased the mechanical properties due to solid strengthening effect of Copper and Nickel. The results also indicated that austempering process at 1 hour gives the optimum mechanical properties in term of tensile strength and impact properties compared to other specimens. Increasing the austempering holding times to 2 hours and 3 hours, in contrast had resulted in decrement of the mechanical properties. There are however only slight improvement in hardness properties and no significant effect on density properties of the specimens.


2021 ◽  
Vol 8 ◽  
Author(s):  
Muhammad Sulaiman ◽  
Tanveer Iqbal ◽  
Saima Yasin ◽  
Hamayoun Mahmood ◽  
Ahmad Shakeel

Diverse applications of polymeric materials have prompted development of eco-friendly, efficient, and economical materials. These characteristics can be obtained by incorporating appropriate fillers in the polymeric matrix. The objective of this work is to investigate impact of aqueous glycerol (Gly) treated rice husk (RH) on surface mechanical properties of produced biocomposites. RH was treated with aqueous Gly (75 wt%) and compounded with low density polyethylene (LDPE) at different loadings (10, 20, and 30 wt%). The resulting mixture was thermally pressed in molds to fabricate biocomposites. Surface mechanical properties such as elastic modulus, hardness, creep rate, and plasticity of biocomposites reinforced with untreated and treated RH were investigated using nanoindenter. Experimental values depicted that hardness (H) and elastic modulus (Es) of treated biocomposites were higher than untreated ones. Treated biocomposites showed the noticeable improvement in elastic modulus by 24 and 37% compared to untreated biocomposites at 20 wt% loading and neat LDPE, respectively. Reductions in the creep rate by 20 and 14% were observed for untreated and treated biocomposites, respectively, in comparison to the neat LDPE. H/E ratio was increased by 23 and 18% for treated and untreated biocomposites, respectively, as compared to virgin LDPE. Furthermore, mechanical and structural properties of untreated and treated RH are reported based on nanoindentation response and Fourier transform infrared spectroscopy (FTIR) techniques The study indicated that aqueous glycerol pretreatment can partially strip off non-cellulosic constituents from lignocellulose matrix to generate cellulose-rich pulp for engineered composite applications.


2018 ◽  
Vol 62 (4) ◽  
pp. 115-120
Author(s):  
M. Hagarová ◽  
D. Jakubéczyová ◽  
G. Baranová ◽  
M. Fujda

Abstract The paper deals with the mechanical properties of steel gas pipeline DN 500 after more than 40 years of operation. Mechanical properties of the pipeline were established by a tensile test at an ambient temperature according to the standard EN ISO 6892-1. The resistance of the pipeline against brittle failure was evaluated by using Charpy impact test according to EN 10045-1. The character of fracture surface after the Charpy test was analysed by using scanning electron microscopy. A high proportion of transcrystalline cleavage was a characteristic feature of fracture surfaces. Mechanical characteristics obtained by static tensile testing were compared with the values obtained from steel manufacturer. Higher elongation was observed in a parallel direction compared to the perpendicular direction to the axis of the pipe. The observed anisotropy of properties was related to the distribution of inclusions in the direction of the deformation of the steel sheets used for the pipeline construction.


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