Two-Step Aging Behaviour of Solution Treated A356 System Alloy

2018 ◽  
Vol 941 ◽  
pp. 1083-1087
Author(s):  
Masahiko Iijima ◽  
Tomoya Ozasa ◽  
Susumu Ikeno ◽  
Kenji Matsuda ◽  
Seiji Saikawa
Keyword(s):  
Solution Treatment ◽  
Aging Treatment ◽  
Hardness Measurement ◽  
Mg Alloy ◽  
Peak Hardness ◽  
System Alloy ◽  
Solution Treated ◽  
Heat Treated ◽  
Final Aging ◽  
Positive Effect

Al-7mass%Si-0.3mass%Mg alloy is widely applied to the automotive components, such as road wheel or suspension frame because of having higher ductility and corrosion resistance. Two-step aging behavior of solution treated Al-7mass%Si-0.3mass%Mg system alloy A356 cast into permanent mold and solution treated was investigated by micro-vickers hardness measurement, optical microscopy (OM) and transmission electron microscopy (TEM). The microstructure of as-cast state was consist of primary crystallized α-Al and secondary crystallized eutectic phases. Al-7mass%Si-0.3mass%Mg alloy after casting, the test specimens were heat treated for different pre-aging temperatures at 273K, 348K and 423K for various times after solution treatment at 813K for 36ks. After pre-aging treatment, the test specimens were heat treated for artificial aging at 523K for various times. The peak hardness increased almost the same value when the pre-aging temperature was 273K. On the other hands, positive effect of the final-aging was occurred after pre-aging at 348K and 423K with significantly increasing hardness in the under-aging region. The fine precipitates were observed in the specimen which was final aging at 523K after pre-aging at 348K and 423K.Such a positive effect is considered due to the influence of precipitated phase mainly such as clusters and /or G.P.zone.The present study aims to investigate the effect of pre-aged temperature on final-aged behavior in A356 system alloy.

Effect of Thermo-Mechanical Treatment (TMT) on Hardness of Heat-Treated Al-Mg-Si (6082) Alloys: Experimental Correlation Using (DOE) Method

2013 ◽  
Vol 376 ◽  
pp. 163-172 ◽  
Author(s):  
Mahmoud M. Tash ◽  
S. Alkahtani
Keyword(s):  
Heat Treatment ◽  
Aging Time ◽  
Solution Heat Treatment ◽  
Mechanical Treatment ◽  
Cold Work ◽  
Solution Treatment ◽  
Aging Treatment ◽  
Solution Treated ◽  
Heat Treated ◽  
Thermo Mechanical Treatment

The present study was undertaken to investigate the effect of Thermo-mechanical Treatment (TMT) on aging and hardness of Al-Mg-Si (6082) alloys. The effect of cold work after solution treatment, aging time and temperature on the microstructure and hardness were studied. Hardness measurements were carried out on specimens prepared from 6082 alloys in the as solution treated specimens and heat-treated conditions, using different cold work percentage before aging treatment. Aging treatments were carried out for the as solution treated specimens (after quenching in water) as well as for the as cold worked specimens (after solution treatment and quenching in water). The specimens were aged at different conditions; Natural aging was carried out at room temperature for different periods of time. Artificial aging was performed at 100 °C, 150 °C, and 200 °C for various times. It is noticed that cold work, following solution treatment, accelerates the precipitation rate leading to a rise in strength.A statistical design of experiments (DOE) approach using fractional factorial design was applied to determine the influence of controlling variables of cold work and heat treatment parameters and any interactions between them on the hardness of 6082 alloys. A mathematical model is developed to relate the alloy hardness with the different metallurgical parameters i.e. Cold work prior solution heat treatment (CWBSHT), Cold work after solution heat treatment (CWASHT), Pre-aging Temperature (PA T0C), Pre-aging time (PA t h), Aging temperature (AT0C), Aging time (At h), Cold work after aging treatment (CWAAT), Annealing temperature (An.T0C) and Annealing time (An.t min) to acquire an understanding of the effects of these variables and their interactions on the hardness of Al-Mg-Si 6082 alloys.

EFFECT OF HEAT TREATMENTS ON THE MICROSTRUCTURE AND PROPERTIES OF Al/SiCp COMPOSITES PREPARED BY NON-ASSISTED INFILTRATION

2012 ◽  
Vol 1373 ◽  
Author(s):  
R. Martínez-López ◽  
M. I. Pech-Canul ◽  
Z. Chaudhury ◽  
L. A. González
Keyword(s):  
Heat Treatment ◽  
Thermal Stresses ◽  
Solution Treatment ◽  
Heat Treatments ◽  
Peak Hardness ◽  
Maximum Hardness ◽  
X Ray ◽  
Solution Treated ◽  
Hardness Tests ◽  
Heat Treated

ABSTRACTAl/SiCp composites fabricated by the non-assisted infiltration route are attractive materials for various engineering applications. However, the presence of thermal stresses can impair their mechanical properties if they are utilized directly after processing. Therefore, heat treatments are potential solutions to this problem. In this work, the effect of T6-heat-treatment on the microstructure and hardness of Al/50% SiCp composites prepared by the non-assisted infiltration route is investigated. Previous to preform preparation, the SiC powders are coated with colloidal SiO2. Infiltration tests are conducted using two experimental Al-Si-Mg alloys. The composites are sectioned in specimen sizes of 1 cm2 and prepared using standard metallographic procedures. Then they are heat treated performing a solution treatment at 350°C for 3 h and artificial aging at 170°C for 1, 3 and 5 hours. In addition, the specimens are characterized by X-ray diffraction (XRD), optical microscopy, scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS). They are also characterized in hardness tests, comparing the behavior for the alloy with and without the various treatments. The results show that heat treatments do not affect the matrix/reinforcement interfacial condition and that the undesirable Al4C3 phase is not developed as consequence of thermal treatments. Hardness tests show that for alloy 1 the maximum hardness value is for the solution-heat-treated samples at 350°C and 5 h aging (28.26±4.02 HC); for alloy 2 the maximum hardness is achieved with solution heat treatment at 350°C and 3 h aging (25.86±4.05 HC). For composites processed with alloy1, the maximum hardness is obtained for the solution treated sample at 350 ° C for 3 h (91.8±2.17 HC), whereas for composites processed with alloy 2 the peak hardness is obtained in solution treated samples and aged at 170°C for 1 h (95.2±0.94 HC).

Effect of Solution Treatment on Microstructures and Hardness of Mg-Gd-Y-Zr Alloy

2014 ◽  
Vol 937 ◽  
pp. 182-186
Author(s):  
Quan An Li ◽  
Lei Lei Chen ◽  
Wen Chuang Liu ◽  
Xing Yuan Zhang ◽  
Hui Zhen Jiang
Keyword(s):  
Vickers Hardness ◽  
Cast Alloy ◽  
Solution Treatment ◽  
Hardness Measurement ◽  
Solution Temperature ◽  
X Ray Diffraction ◽  
X Ray ◽  
Solution Treated ◽  
Primary Particles ◽  
Zr Alloy

The influence of the solution treatment (at the temperature of 500-520°C for 4-12 h) on microstructures and mechanical properties of Mg-Gd-Y-Zr alloy was investigated by means of optical microscopy, scanning electron microscopy (SEM), X-ray diffraction (XRD) and Vickers hardness measurement. The as-cast alloy contains a microstructure consisting of α-Mg matrix, Mg5Gd phase and Mg24Y5phase. With increasing solution temperature and time, the quantity of the primary particles (Mg5Gd and Mg24Y5) in the alloy continually decreased, and the degree of recrystallization gradually increased, which result in the gradual decrease of the Vickers hardness of the solution-treated alloys.

scholarly journals Effect of Ti Addition to Age Hardening Response of Al-10Zn-6MgxTi Alloy Produced by Squeeze Casting

2018 ◽  
Vol 186 ◽  
pp. 02009
Author(s):  
Dwi Ayu Nurcahyaningsih ◽  
Risly Wijanarko ◽  
Irene Angela ◽  
Bondan Tiara Sofyan
Keyword(s):  
Squeeze Casting ◽  
Solution Treatment ◽  
Organic Rankine Cycle ◽  
Rankine Cycle ◽  
Hardness Measurement ◽  
Impact Testing ◽  
Age Hardening ◽  
Peak Hardness ◽  
7Xxx Alloy ◽  
Ti Addition

This research focused on investigating the effects of Ti addition on the age hardening response of Al 7xxx alloy for Organic Rankine Cycle (ORC) turbine impeller application in power plant generators. Al-10Zn-6Mg wt. % alloys were produced by squeeze casting with 0.02, 0.05, and 0.25 wt. % Ti addition. As-cast samples were homogenized at 400 °C for 4 h. Solution treatment was conducted at 440 °C for 1 h, followed by quenching and ageing at 130 °C for 200 h. Age hardening result was observed using Rockwell B hardness measurement. Other characterizations included impact testing, STA, optical microscopy, and SEM-EDS. Results showed that the addition of Ti in all content variations increased the as-cast hardness due to the diminution of secondary dendrite arm spacing (SDAS) values of the alloy. Ageing at 130 °C strengthened the alloys, however the addition of Ti was not found to affect neither peak hardness nor impact values of the alloy. Identities of second phases formed during solidification were found to be T (Mg32(Al,Zn)49), β (Al8Mg5), and TiAl3, while precipitates produced during ageing were GP Zone, η′, and η (MgZn2).

The Effects of Solid-Solution on Properties and Microstructure of 6063 Aluminum Alloy

2014 ◽  
Vol 881-883 ◽  
pp. 1346-1350 ◽  
Author(s):  
Ben Chen ◽  
Yu Jiao Wu ◽  
Tao Zhu ◽  
Xin Yun Li
Keyword(s):  
Solid Solution ◽  
Electrical Resistivity ◽  
Aluminum Alloy ◽  
Solution Process ◽  
Solution Treatment ◽  
Aging Treatment ◽  
Solution Treated ◽  
Suitable Solution ◽  
6063 Aluminum Alloy

The solution treatment of 6063 aluminum alloy was carried out and the influences of solution process on microstructure, strength, hardness, and electrical resistivity of 6063 aluminum alloy was analyzed. The result shows that the suitable solution treatment can improve alloy solution-degree fully, meanwhile the changes of electrical resistivity of alloy tend to be balanced. The suitable solution process for 6063 aluminum alloy is solution-treated at 520°C for 3.5h, and the strength and hardness of alloy can be enhanced extremely after aging-treatment at 200°C for 5h.

scholarly journals Microstructure Evolution and Mechanical Properties of AZ80 Mg Alloy during Annular Channel Angular Extrusion Process and Heat Treatment

Materials ◽  
2019 ◽  
Vol 12 (24) ◽  
pp. 4223 ◽  
Author(s):  
Xi Zhao ◽  
Shuchang Li ◽  
Fafa Yan ◽  
Zhimin Zhang ◽  
Yaojin Wu
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Microstructure Evolution ◽  
Solution Treatment ◽  
Aging Treatment ◽  
Annular Channel ◽  
Mg Alloy ◽  
Strengthening Effect ◽  
Β Phase ◽  
Angular Extrusion

Microstructure evolution and mechanical properties of AZ80 Mg alloy during annular channel angular extrusion (350 °C) and heat treatment with varying parameters were investigated, respectively. The results showed that dynamic recrystallization of Mg grains was developed and the dendritic eutectic β-Mg17Al12 phases formed during the solidification were broken into small β-phase particles after hot extrusion. Moreover, a weak texture with two dominant peaks formed owing to the significant grain refinement and the enhanced activation of pyramidal <c + a> slip at relative high temperature. The tension tests showed that both the yield strength and ultimate tensile strength of the extruded alloy were dramatically improved owing to the joint strengthening effect of fine grain and β-phase particles as compared with the homogenized sample. The solution treatment achieved the good plasticity of the alloy resulting from the dissolution of β-phases and the development of more equiaxed grains, while the direct-aging process led to poor alloy elongation as a result of residual eutectic β-phases. After solution and aging treatment, simultaneous bonding strength and plasticity of the alloy were achieved, as a consequence of dissolution of coarse eutectic β-phases and heterogeneous precipitation of a large quantity of newly formed β-phases with both the morphologies of continuous and discontinuous precipitates.

Aging Behaviors of Al 6061 and Al 6061/SiCp Composite

2011 ◽  
Vol 410 ◽  
pp. 240-244 ◽  
Author(s):  
S.M.R. Ourang ◽  
A. Ekrami ◽  
S.M. Seyed Reihani ◽  
S.M.R.Mousavi Abarghouie
Keyword(s):  
Solution Treatment ◽  
Peak Hardness ◽  
Powder Metallurgy Method ◽  
Aging Behavior ◽  
Al 6061 ◽  
Solution Treated ◽  
Treatment Conditions ◽  
Aging Kinetics ◽  
Optimum Solution ◽  
Hardness Values

In the present research the aging behavior of Al6061 alloy and Al6061/SiCp composite fabricated by powder metallurgy method was investigated. The solution treatment of the samples were carried out at 527°C for 2, 3and 4 h followed by aging at 180°C for different aging times between 1 and 10 h. The existence of SiC particles led to increasing the peak hardness of the composite. The peak hardness of the composite took place at shorter times than that of the 6061 alloy for the samples solution treated for 3and 4 h, but took place at longer times for the samples solution treated for 2 h. The optimum solution treating time was about 3 h for both the composite and the 6061 alloy that led to the fastest aging kinetics and the maximum hardness. At the solution treating time shorter than 3h due to incomplete dissolution of precipitates, the aging kinetics decelerated and the hardness values decreased. For the composites solution treated more than 3 h, hardness values decreased due to the grain growth of matrix while changing in the aging kinetics was not significant. EDS and SEM studies indicated the presence of bight enrichment zones including Mg and Si elements in the composite in solution treatment conditions.

The Effect of Heat Treatment on Fatigue and Mechanical Properties of 6061 Aluminium Alloy

2014 ◽  
Vol 699 ◽  
pp. 227-232
Author(s):  
Nurulhilmi Zaiedah Nasir ◽  
Mohd Ahadlin Mohd Daud ◽  
Mohd Zulkefli Selamat ◽  
Ahmad Rivai ◽  
Sivakumar Dhar Malingam
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Impact Strength ◽  
Aluminium Alloy ◽  
Aging Treatment ◽  
Hardness Measurement ◽  
Hardness Tester ◽  
Quenching Media ◽  
Heat Treated ◽  
6061 Aluminium Alloy

This paper investigated the effect of heat treatment on mechanical properties and microstructure of 6061 aluminium alloy. The aluminium alloys were examined in the heat treated conditions, using different quenching media, water and oil. The alloy was solution heat treated at temperature of 529oC for one, three and five hour respectively. Aging treatment was carried out at temperature of 160oC which is assumed to be the best temperature for ageing process. Hardness measurement was carried out using a Brinell Hardness Tester Machine. The results shows hardness and impact strength are inversely proportional to each other, as the hardness of 6061 aluminium alloy decreases and impact strength increases.

Effect of Aluminum Addition on the Static Recrystallization Behavior of Magnesium

2012 ◽  
Vol 724 ◽  
pp. 163-168 ◽  
Author(s):  
Keun Joon Kim ◽  
Tae Kwon Ha
Keyword(s):  
Static Recrystallization ◽  
Solution Treatment ◽  
Annealing Treatment ◽  
Hardness Measurement ◽  
Recrystallization Behavior ◽  
Microstructure Observation ◽  
Heat Treated ◽  
Increasing Temperature ◽  
Kinetics Of ◽  
Rolled Plates

Recrystallization kinetics of Mg alloy has been investigated in this study. Mg alloys such as Mg-3Al and Mg-6Al in weight percents were cast into rectangular shaped ingots of 20mm thickness. Solution treatment at 400°C for 24 hrs has been carried out on these ingots and pure Mg for comparison. Heat treated ingots including pure Mg were rolled at room temperature by thickness reductions of 10, 20, and 30 percents. Annealing treatment for recrystallization has been conducted on these cold-rolled plates at temperatures of 200, 300, and 400°C for various times from 1 min to 24 hrs. The microstructure observation and hardness measurement conducted on the recrystallized specimens revealed that static recrystallization at 200°C was very slow and expedited with increasing temperature, regardless of Al contents. While recrystallization behavior of Mg at 300°C appeared to be retarded by increase in Al contents, that of Mg was not affected at 400°C.

Microstructural Changes of FSX-414 Superalloy during TLP Bonding

2011 ◽  
Vol 312-315 ◽  
pp. 399-404 ◽  
Author(s):  
R. Bakhtiari ◽  
A. Ekrami
Keyword(s):  
Aging Treatment ◽  
Eutectic Structure ◽  
Isothermal Solidification ◽  
Heat Treatment Condition ◽  
Hardness Profile ◽  
Solution Treated ◽  
Tlp Bonding ◽  
Heat Treated ◽  
M23c6 Type ◽  
Bond Region

The as-cast FSX-414 Co-based superalloy samples were solution treated at 1150oC for 4h and then aged at 980oC for 4h. Specimens for joining were cut from the as-cast ingot and TLP bonding carried out at the same conditions as for the solution and solution+aging treatment, using MBF-30 interlayer. Microstructures were studied for as-cast, heat treated and TLP bonded specimens. These studies showed that the ununiform distributed carbides of MC type in the as-cast specimens replaced by M23C6 type carbides with uniform distribution in the heat treated microstructure. Due to complete isothermal solidification, no eutectic structure in the bond region were wasobserved, but some intermetallics in the diffusion affected zone (DAZ) were observed. Microhardness tests were used to compare the hardness of age hardened specimens with bonded specimens at the same heat treatment condition. Hardness profile also showed a peak in DAZ region in spite of complete isothermal solidification.

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