The Effect of Heating Rate and Temperature on Microstructure and R-Value of Type 430 Ferritic Stainless Steel

2018 ◽  
Vol 941 ◽  
pp. 364-369
Author(s):  
Matias Jaskari ◽  
Antti Järvenpää ◽  
L. Pentti Karjalainen

Typical applications of ferritic stainless steels require good formability of a steel that is highly dependent on the processing route. In this study, the effects of heating rate and peak temperature on the texture and formability of a 78% cold-rolled unstabilized 17%Cr (AISI 430) ferritic stainless steel were studied. The cold-rolled sheet pieces were heated in a Gleeble 3800 simulator at the heating rates of 25 °C/s and 500 °C/s up to various peak temperatures below 950 °C for 10 s holding before the final cooling at 35 °C/s to room temperature. Microstructures were characterized and the texture of the annealed samples determined by the electron backscatter diffraction method. The R-value in various directions was determined by tensile straining to 15%. It was established that the high heating rate of 500 °C/s tends to promote the nucleation of grains with the {111}<uvw> orientations during the early state of the recrystallization. The higher heating rate led to a slightly finer grain size and to a marginal improvement in the intensity of the gamma-fibre texture. A coarser grain size would be beneficial for the formability, but the grain growth was suppressed due to low peak temperatures and a short soaking time. Anyhow, the fast annealing resulted in an enhanced R-value in the transverse to rolling direction. The results indicate that even a short annealing cycle is plausible for producing ferritic stainless steels with the formability properties comparable to those of commercial counterparts.

2018 ◽  
Vol 786 ◽  
pp. 3-9
Author(s):  
Matias Jaskari ◽  
Antti Järvenpää ◽  
Pentti L. Karjalainen

Typical applications of ferritic stainless steels require good formability of the material that is highly dependent on the processing route. In this study, the effects of the heating rate and peak heating temperature on the texture and deep drawability (R-value) of a 78% cold rolled, stabilized 18Cr (AISI 441) ferritic stainless steel were studied. Pieces of cold rolled sheet were heated in a Gleeble 3800 simulator at the heating rates of 25 °C/s and 500 °C/s to various temperatures up to 1150 °C for 10 s holding before cooling at a rate of 35 °C/s. Microstructures were characterized and the texture of the annealed samples determined by the electron backscatter diffraction method. It was established that the high heating rate of 500 °C/s promotes the nucleation of grains with the near {111}<uvw> orientations during the early state of the recrystallization. The maximum texture intensities were found at {554}<225>. The more effective nucleation of these grains resulted in a finer grain size and an increased intensity of the gamma-fibre texture which led to enhanced R-values. At high peak temperatures, the intense grain growth took place.


2019 ◽  
Vol 25 (4) ◽  
pp. 217
Author(s):  
Andrea Di Schino

<p class="AMSmaintext1"><span lang="EN-GB">Following nickel and molybdenum significant price increase, nowadays the stainless steel market is moving toward an increasing use of ferritic stainless steel instead of austenitic stainless and therefore to the development of advanced ferritic stainless steels grades aimed to substitute the more expensive austenitic materials in all applications allowing it. Super-ferritic stainless steels are higher chromium (Cr) and molybdenum (Mo) steels with properties similar to those of standard ferritic alloys. Such elements increase high temperature and corrosion resistance in strong environment. This paper deal about the corrosion resistance of super-ferritic stainless steels with a Cr content ranging from 21% to 24%. </span></p>


2007 ◽  
Vol 550 ◽  
pp. 65-74 ◽  
Author(s):  
R.D. Knutsen

The surface ridging behaviour during tensile straining has been characterised for two ferritic stainless steels possessing different austenite potentials (0.1 and 0.6 respectively). Microstructural and texture heterogeneities have been detected to different levels in each steel and are used to explain the extent of surface ridging by considering a ridging mechanism arising from differential transverse strains. Orientation images are presented to trace the development of orientation clusters during recrystallisation.


2013 ◽  
Vol 66 (4) ◽  
pp. 467-471
Author(s):  
André Itman Filho ◽  
Wandercleiton da Silva Cardoso ◽  
Leonardo Cabral Gontijo ◽  
Rosana Vilarim da Silva ◽  
Luiz Carlos Casteletti

The austenitic-ferritic stainless steels present a better combination of mechanical properties and stress corrosion resistance than the ferritic or austenitic ones. The microstructures of these steels depend on the chemical compositions and heat treatments. In these steels, solidification starts at about 1450ºC with the formation of ferrite, austenite at about 1300ºC and sigma phase in the range of 600 to 950ºC.The latter undertakes the corrosion resistance and the toughness of these steels. According to literature, niobium has a great influence in the transformation phase of austenitic-ferritic stainless steels. This study evaluated the effect of niobium in the microstructure, microhardness and charge transfer resistance of one austenitic-ferritic stainless steel. The samples were annealed at 1050ºC and aged at 850ºC to promote formation of the sigma phase. The corrosion testes were carried out in artificial saliva solution. The addition of 0.5% Nb in the steel led to the formation of the Laves phase.This phase, associated with the sigma phase, increases the hardness of the steel, although with a reduction in the values of the charge transfer resistance.


2017 ◽  
Vol 31 (16-19) ◽  
pp. 1744042
Author(s):  
Yijie Ji ◽  
Yuye Xie ◽  
Shuangchun Zhu ◽  
Biao Yan

With the promotion of fuel economy policy and automobile lightweight concept, ferritic stainless steels applied in vehicles’ exhaust hot end systems have been developed. This paper simulated the high-temperature environment at which the automobile exhaust system serviced in for high-temperature corrosion. Kinetic curves were conducted in isothermal environments at 1000[Formula: see text]C. X-ray diffraction, scanning electron microscope and energy dispersive spectrometer were used to study the oxidation behavior of ferritic stainless steels and the effects of tungsten (W) addition. The results show that, with increasing oxidation time, the rate of weight gains increase and the main failure is spalling of surface oxide layer. The addition of W has a complicated effect on the oxidation behavior of ferritic stainless steel weldment.


2016 ◽  
Vol 879 ◽  
pp. 1594-1599
Author(s):  
Daniella Gomes Rodrigues ◽  
Cláudio Moreira Alcântara ◽  
Dagoberto Brandão Santos ◽  
Tarcísio Reis de Oliveira ◽  
Berenice Mendonça Gonzalez

The ferritic stainless steels are materials used in several segments due to the excellent combination of mechanical properties and corrosion resistance. The mechanical properties of these alloys are strongly dependent on the microstructural characteristics and crystallography texture. The aim of this experimental study is to investigate the roles of the grain size of the hot rolled sample on the development of the microstructure, texture and formability of ferritic stainless steel. The main elements of chemical composition of the steel under investigation were 16.0 %Cr, 0.021 %C, 0.024 %N and 0.35 %Nb. Coarse and fine grains samples were cold rolled up to 90% thickness reduction and annealed at 880°C with soaking time of the 24 s. The texture measurements were performed by Electron Backscattered Diffraction (EBSD) in the longitudinal section. The formability was evaluated by the R-value and planar anisotropy (Δr) in tensile tests. The final microstructure after annealed was more homogenous for smaller initial grain size sample. This condition was favorable to develop γ-fiber, with sharpness intensity in 111121 components. The highest R-value and smallest planar anisotropy was obtained for a {111}/{001} ratio around 5.37. On the other hand, coarser initial grain size sample had showed a heterogeneous microstructure and texture, performing badly in mechanical tests (anisotropy).


Author(s):  
Younggi Lee ◽  
Gyeongcheol Lee ◽  
Jaeseong Kim ◽  
Boyoung Lee

Ferritic stainless steels have excellent stress corrosion resistance and a low coefficient of thermal expansion compared to austenitic stainless steels. Ferritic stainless steels of the 400 series have been available for automotive exhaust systems, heat exchangers, radiators etc. in various industries. Automotive exhaust manifolds especially require good heat resistance because the typical operation temperature(800°C) of the exhaust system is exposed to during engine operation. In this study, the effects of high temperature(800°C) characteristics on the mechanical and microstructure properties were investigated for lap joint of ferritic stainless steel(STS 429) mainly used as the automotive exhaust manifolds. The microstructure of lap joint was characterized by optical microscopy(OM), scanning electron microscopy(SEM) and X-ray diffraction(XRD). The mechanical property of lap joint was evaluated by tensile test. The tensile test results show that a significant decrease in ultimate tensile strength(between 82 and 85%) was observed for aged STS 429 when tested at the evaluated temperature(800°C). The tensile strength was significantly influenced by growth of grain in the heat affected zone(HAZ). The XRD results show that chromium carbide and chromium nitride phases such as Cr23C6, Cr7C3, Cr2N and TiN were precipitated in the heat affected zone(HAZ).


Metals ◽  
2019 ◽  
Vol 9 (6) ◽  
pp. 664 ◽  
Author(s):  
Timo Juuti ◽  
Timo Manninen ◽  
Sampo Uusikallio ◽  
Jukka Kömi ◽  
David Porter

A large number of thermodynamic simulations has been used to design a new Nb-Ti dual stabilized ferritic stainless steel with excellent creep resistance at 1050 °C through an optimal volume fraction of Laves (η) phase stabilized by the alloying elements Nb, Si and Mo. By raising the dissolution temperature of the phase, which also corresponds to the onset of rapid grain growth, the steel will better maintain the mechanical properties at higher service temperature. Laves phase precipitates can also improve creep resistance through precipitation strengthening and grain boundary pinning depending on the dominant creep mechanism. Sag tests at high temperatures for the designed steel showed significantly better results compared to other ferritic stainless steels typically used in high temperature applications at present.


2014 ◽  
Vol 783-786 ◽  
pp. 807-812 ◽  
Author(s):  
Timo J. Juuti ◽  
Timo Manninen ◽  
L. Pentti Karjalainen ◽  
David A. Porter

High-chromium ferritic stainless steels have been developed for applications such as exhaust systems that require good formability. To improve formability, continuous yielding is preferred. However, in high-chromium ferritic stainless steels an upper yield point is often present as a result of free interstitials and Cottrell atmospheres. The upper yield point can be removed by temper rolling but it would be better to avoid it via a suitable heat treatment. This paper describes how this can be done in the case of a ferritic stainless steel containing 0.011%C, 0.012%N, 18%Cr, 2,1%Mo, 0.33%Nb, 0.15Ti%. Despite the presence of Nb and Ti, which should bind the free carbon and nitrogen as carbides and nitrides, an upper yield point was still observed. Previously it has been suspected that this is due to an intermetallic Laves phase present in this steel depleting the Nb in the matrix so that some carbon remains free. A series of short-term annealing experiments showed that the upper yield point diminishes, when the annealing temperature increases above 550 °C, finally disappearing after a heat treatment at 750 °C. On the basis of Thermo-Calc calculations and EDS analyses, free interstitials in the matrix could be related to depletion of MX or insufficient time to reach the equilibrium state.


2010 ◽  
Vol 163 ◽  
pp. 151-156 ◽  
Author(s):  
Janusz Ryś ◽  
Małgorzata Witkowska

The present examination is a part of project concerning a deformation behavior of duplex type ferritic-austenitic stainless steels. The investigations included the analysis of ferrite and austenite microstructures formed in cold-rolled sheet of super-duplex stainless steel, major deformation mechanisms operating in both constituent phases and changes in morphology of two-phase structure after the thermo-mechanical treatment and subsequent cold-rolling. Duplex type stainless steels develop the band-like ferrite-austenite morphology in the course of hot- and cold-rolling. This specific two-phase structure creates different conditions for plastic deformation in comparison to single phase steels. The interaction of both phases upon deformation exerts fairly significant influence on structure and texture formation in both constituent phases and in consequence affects the material properties and its behavior upon further processing.


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