scholarly journals Mapping of mechanical properties at microstructural length scale in WC-Co cemented carbides: Assessment of hardness and elastic modulus by means of high speed massive nanoindentation and statistical analysis

Author(s):  
J.J. Roa ◽  
P. Sudharshan Phani ◽  
W.C. Oliver ◽  
L. Llanes
2011 ◽  
Vol 409 ◽  
pp. 544-549 ◽  
Author(s):  
Luca Sorelli ◽  
Daniel Vallée ◽  
Aali R. Alizadeh ◽  
James Beaudoin ◽  
Nicholas Randall

In order to reduce CO2emissions, the cement industry has developed a new class cements. The Calcium-Silicate-Hydrates (CSH) that form are generally characterized by a low stoichiometric ratio for CaO and SiO2. This low C/S ratio affects the C-S-H layer structure and has a significant effect on the mechanical properties. This work exploits a novel statistical nanoindentation technique (SNT) to study the effect of the C/S ratio on the mechanical properties of synthetic CSH. Different CSH types were prepared by varying the C/S ratio of the starting materials. After undertaking a grid nanoindentation approach for each sample, the statistical analysis allowed extracting the mechanical properties, such as elastic modulus, hardness and creep. The results of this preliminary work shed new light on the implications of C-S-H stoichiometry on mechanical properties.


2012 ◽  
Vol 512-515 ◽  
pp. 1746-1750 ◽  
Author(s):  
Z.J. Shou ◽  
H.R. Le ◽  
S.Y. Qu ◽  
R.A. Rothwell ◽  
R.E. Mackay

Chitosan has found various applications in gastrointestinal stent, biomedical implants as well as an effective absorbent in waste water treatment. However, the material suffers from low strength and large shrinkage upon dehydration. The current project is aimed to develop a process to fabricate chitosan composites with the addition of functionalised montmorillonite nanoparticles and to examine the effect of ceramic content on the mechanical behavior of the composites. This paper describes the fabrication of chitosan with montmorrillonite composites and the mechanical testing of the samples and the mechanical behaviour of the composites, as well as the observations of the microstructure. The effects of composition and microstructure on the mechanical properties of the composite are investigated. The results indicate that the nanoparticles are dispersed uniformly in the matrix up to 40wt% using high speed homogeniser. The elastic modulus increases monotonically with the addition of nanoparticles, but the fracture strength drops due to the defects introduced by the nanoparticles.


Author(s):  
Medard Makrenek

The paper presents the methodology behind the statistical selection of input parameters using the example of spraying two cold-sprayed coatings. The Ti and Cr3C2-25(Ni20Cr)-Gr coatings were tested. Despite the large difference in the structure of these coatings, nanoindentation studies were carried out focusing on the nano hardness H and elastic modulus E. Based on the four input parameters and two output parameters, a 2-level factorial 2(k-p) experimental design was performed. The conducted analysis showed the significant influence of the spray distance on the H and E values in the case of the Ti coating. The input parameters of the spray distance and the type of carrier gas used turned out to be statistically significant in the case of the cermet coating. Taking into account the statistical analysis, the coatings were sprayed with modified values of the input parameters.


2016 ◽  
Vol 693 ◽  
pp. 586-593 ◽  
Author(s):  
Y.Z. Pan ◽  
Jun Zhao ◽  
J. Zhang

The chemical compositions and microstructures of several different cemented carbides were checked by XRD, XRF, SEM, metallographic microscope and stereomicroscope. The influences of phase compositions and microstructures on mechanical properties were investigated. The results show that improving the Co content and refining WC grain properly are effective means to acquire the excellent mechanical properties of cemented carbide. A series of friction and wear tests were carried out in a high-speed tribometer to explore the tribological behavior of three cemented carbides with different Co content and WC grain size against aluminum alloy 7050-T7451. It was found that the tribological behaviors of cemented carbides are largely dependent on their microstructures and mechanical properties. The enhancement of flexural strength and fracture toughness can be ascribed to deformation buffering effects of Co binder, but the improved hardness depends on the rigid skeleton of WC-WC grains.


2010 ◽  
Vol 163-167 ◽  
pp. 1192-1197 ◽  
Author(s):  
Deng Xiang Zhang ◽  
Wei Jun Yang

Based on large numbers of experiment results, this paper carries out statistical analysis and proposes the probability distribution properties of the random process of strength and elastic modulus and their coefficient of variation, and develops a new prediction model of early-age strength and elastic modulus and their coefficient of variation respectively. The model can provide good prediction of the development of mechanical properties of concrete structures in aging, and it is important to evaluate the concrete structure safety and reliability in the construction period.


Author(s):  
Seyed Hamid Reza Sanei ◽  
F. Alisafaei ◽  
Chung-Souk Han

The two most common outputs of nanoindentation experiment are hardness and elastic modulus. Length scale dependent deformation in polymers has however been observed in different experiments such as microbeam bending, torsional thin wires and indentation testing which may affect the mechanical testing. Unlike in metals where the size dependency is attributed to necessary geometry dislocations, the origin of length scale dependent deformation in polymers is not well understood. In this study, elastic modulus of polydimethylsiloxane (PDMS) is determined using both Berkovich and spherical tips. Observing different trends for elastic modulus upon the change of indentation depth using these two different tips brings up the question which tip should be used to get the real mechanical properties of PDMS which is discussed here. Surface roughness, surface effects and the imperfection of the Berkovich indenter tip are negligible at the studied length scale.


2014 ◽  
Vol 66 (4) ◽  
pp. 520-524 ◽  
Author(s):  
Serkan Büyükdoğan ◽  
Süleyman Gündüz ◽  
Mustafa Türkmen

Purpose – The paper aims to provide new observations about static strain ageing in aluminium (Al) alloys which are widely used in structural applications. Design/methodology/approach – The present work aims to provide theoretical and practical information to industries or researchers who may be interested in the effect of static strain ageing on mechanical properties of Al alloys. The data are sorted into the following sections: introduction, materials and experimental procedure, results and discussion and conclusions. Findings – Tensile strength, proof strength (0.2 per cent) and percentage elongation measurement were used to investigate the effect of strain ageing on the mechanical properties. Wear tests were performed by sliding the pin specimens, which were prepared from as-received, solution heat-treated, deformed and undeformed specimens after ageing, on high-speed tool steel (64 HRC). It is concluded that the variations in ageing time improved the strength and wear resistance of the 6063 Al alloy; however, a plastically deformed solution-treated alloy has higher strength and wear resistance than undeformed specimens for different ageing times at 180°C. Practical implications – A very useful source of information for industries using or planning to produce Al alloys. Originality/value – This paper fulfils an identified resource need and offers practical help to the industries.


Polymers ◽  
2021 ◽  
Vol 13 (7) ◽  
pp. 1134
Author(s):  
Bo Seok Song ◽  
Jun Young Lee ◽  
Sun Hwa Jang ◽  
Wan-Gyu Hahm

High-speed melt spinning of thermotropic liquid crystalline polymer (TLCP) resin composed of 4-hydroxybenzoic acid (HBA) and 2-hydroxy-6-napthoic acid (HNA) monomers in a molar ratio of 73/27 was conducted to investigate the characteristic structure development of the fibers under industrial spinning conditions, and the obtained as-spun TLCP fibers were analyzed in detail. The tensile strength and modulus of the fibers increased with shear rate in nozzle hole, draft in spin-line and spinning temperature and exhibited the high values of approximately 1.1 and 63 GPa, respectively, comparable to those of industrial as-spun TLCP fibers, at a shear rate of 70,000 s−1 and a draft of 25. X-ray diffraction demonstrated that the mechanical properties of the fibers increased with the crystalline orientation factor (fc) and the fractions of highly oriented crystalline and non-crystalline anisotropic phases. The results of structure analysis indicated that a characteristic skin–core structure developed at high drafts (i.e., spinning velocity) and low spinning temperatures, which contributed to weakening the mechanical properties of the TLCP fibers. It is supposed that this heterogeneous structure in the cross-section of the fibers was induced by differences in the cooling rates of the skin and core of the fiber in the spin-line.


Energies ◽  
2021 ◽  
Vol 14 (8) ◽  
pp. 2303
Author(s):  
Congyu Zhong ◽  
Liwen Cao ◽  
Jishi Geng ◽  
Zhihao Jiang ◽  
Shuai Zhang

Because of its weak cementation and abundant pores and cracks, it is difficult to obtain suitable samples of tectonic coal to test its mechanical properties. Therefore, the research and development of coalbed methane drilling and mining technology are restricted. In this study, tectonic coal samples are remodeled with different particle sizes to test the mechanical parameters and loading resistivity. The research results show that the particle size and gradation of tectonic coal significantly impact its uniaxial compressive strength and elastic modulus and affect changes in resistivity. As the converted particle size increases, the uniaxial compressive strength and elastic modulus decrease first and then tend to remain unchanged. The strength of the single-particle gradation coal sample decreases from 0.867 to 0.433 MPa and the elastic modulus decreases from 59.28 to 41.63 MPa with increasing particle size. The change in resistivity of the coal sample increases with increasing particle size, and the degree of resistivity variation decreases during the coal sample failure stage. In composite-particle gradation, the proportion of fine particles in the tectonic coal sample increases from 33% to 80%. Its strength and elastic modulus increase from 0.996 to 1.31 MPa and 83.96 to 125.4 MPa, respectively, and the resistivity change degree decreases. The proportion of medium particles or coarse particles increases, and the sample strength, elastic modulus, and resistivity changes all decrease.


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