scholarly journals Metamaterials with engineered failure load and stiffness

2019 ◽  
Vol 116 (48) ◽  
pp. 23960-23965 ◽  
Author(s):  
Sai Sharan Injeti ◽  
Chiara Daraio ◽  
Kaushik Bhattacharya
Keyword(s):  
Mechanical Properties ◽  
Sensitivity Analysis ◽  
Critical Load ◽  
Failure Load ◽  
Weight Ratio ◽  
Fracture Load ◽  
Specific Load ◽  
Load To Failure ◽  
Failure Location ◽  
Theoretical Results

Architected materials or metamaterials have proved to be a very effective way of making materials with unusual mechanical properties. For example, by designing the mesoscale geometry of architected materials, it is possible to obtain extremely high stiffness-to-weight ratio or unusual Poisson’s ratio. However, much of this work has focused on designing properties like stiffness and density, and much remains unknown about the critical load to failure. This is the focus of the current work. We show that the addition of local internal prestress in selected regions of architected materials enables the design of materials where the critical load to failure can be optimized independently from the density and/or quasistatic stiffness. We propose a method to optimize the specific load to failure and specific stiffness using sensitivity analysis and derive the maximum bounds on the attainable properties. We demonstrate the method in a 2D triangular lattice and a 3D octahedral truss, showing excellent agreement between experimental and theoretical results. The method can be used to design materials with predetermined fracture load, failure location, and fracture paths.

scholarly journals Indentation Response and Contact Damage of Hard T-B-N Films Deposited by Magnetron Sputtering

2010 ◽  
Vol 13 (1-2) ◽  
pp. 81 ◽  
Author(s):  
P. Karuna Purnapu Rupa ◽  
P.C. Chakraborti ◽  
Suman K. Mishra
Keyword(s):  
Mechanical Properties ◽  
Boron Nitride ◽  
Magnetron Sputtering ◽  
Critical Load ◽  
Reactive Magnetron ◽  
Instrumented Indentation ◽  
Indentation Technique ◽  
Load To Failure ◽  
Indentation Response ◽  
Depth Curves

<p>Titanium-boron-nitride (Ti-B-N) films were deposited by reactive magnetron sputtering using a single TiB<sub>2</sub> target. The films were deposited under different Ar:N<sub>2</sub> ratios. The instrumented indentation technique (nanoindentation), is used to evaluate the mechanical properties of the films. A methodology is presented to evaluate the critical load to failure directly from the load depth curves. Significant effect of Ar:N<sub>2</sub> ratio was observed on the mechanical properties of the Ti-B-N films.</p>

scholarly journals Mechanical Properties of the Composite Material consisting of β-TCP and Alginate-Di-Aldehyde-Gelatin Hydrogel and Its Degradation Behavior

Materials ◽  
2021 ◽  
Vol 14 (5) ◽  
pp. 1303
Author(s):  
Michael Seidenstuecker ◽  
Thomas Schmeichel ◽  
Lucas Ritschl ◽  
Johannes Vinke ◽  
Pia Schilling ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Compressive Strength ◽  
Protein Concentration ◽  
Failure Load ◽  
Testing Machine ◽  
Experimental Period ◽  
Flow Chamber ◽  
Degradation Behavior ◽  
Gelatin Hydrogel ◽  
Universal Testing

This work aimed to determine the influence of two hydrogels (alginate, alginate-di-aldehyde (ADA)/gelatin) on the mechanical strength of microporous ceramics, which have been loaded with these hydrogels. For this purpose, the compressive strength was determined using a Zwick Z005 universal testing machine. In addition, the degradation behavior according to ISO EN 10993-14 in TRIS buffer pH 5.0 and pH 7.4 over 60 days was determined, and its effects on the compressive strength were investigated. The loading was carried out by means of a flow-chamber. The weight of the samples (manufacturer: Robert Mathys Foundation (RMS) and Curasan) in TRIS solutions pH 5 and pH 7 increased within 4 h (mean 48 ± 32 mg) and then remained constant over the experimental period of 60 days. The determination surface roughness showed a decrease in the value for the ceramics incubated in TRIS compared to the untreated ceramics. In addition, an increase in protein concentration in solution was determined for ADA gelatin-loaded ceramics. The macroporous Curasan ceramic exhibited a maximum failure load of 29 ± 9.0 N, whereas the value for the microporous RMS ceramic was 931 ± 223 N. Filling the RMS ceramic with ADA gelatin increased the maximum failure load to 1114 ± 300 N. The Curasan ceramics were too fragile for loading. The maximum failure load decreased for the RMS ceramics to 686.55 ± 170 N by incubation in TRIS pH 7.4 and 651 ± 287 N at pH 5.0.

Scanning Scratch Tests for Evaluating the Adhesion of Thin Oxide Films on Stainless Steel

1994 ◽  
Vol 356 ◽  
Author(s):  
V. A. C. Haanappel ◽  
H. D. van Corbach ◽  
T. Fransen ◽  
P. J. Gellings
Keyword(s):  
Mechanical Properties ◽  
Growth Rate ◽  
Stainless Steel ◽  
Film Thickness ◽  
Critical Load ◽  
Deposition Temperature ◽  
Chemical Vapour ◽  
Organic Chemical ◽  
Thin Oxide Films ◽  
Type Aisi

AbstractAmorphous alumina films were deposited by metal-organic chemical vapour deposition (MOCVD) on stainless steel, type AISI 304. The MOCVD experiments were performed in nitrogen at low pressure (0.17 kPa (1.25 torr)).The effect of deposition temperature (200 − 380 °C), growth rate, film thickness, and post-deposition thermal treatment on the mechanical properties was studied. The experiments were performed with a scanning-scratch tester. The experiments are based on the estimation of the film adhesion to the substrate by determining a critical load, Lc: the load where the film starts to spall or to delaminate.The best mechanical properties were obtained with unannealed samples. After thermal annealing the critical load decreases. Regarding the unannealed samples, the critical load increased with increasing film thickness. The deposition temperature and the growth rate had no effect on the critical load.

scholarly journals Fabrication and Characterization of Electrospun Polycaprolactone Blended with Chitosan-Gelatin Complex Nanofibrous Mats

2014 ◽  
Vol 2014 ◽  
pp. 1-7 ◽  
Author(s):  
Yongfang Qian ◽  
Zhen Zhang ◽  
Laijiu Zheng ◽  
Ruoyuan Song ◽  
Yuping Zhao
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Weight Ratio ◽  
Degree Of Crystallinity ◽  
X Ray Diffraction ◽  
Tissue Engineering Scaffolds ◽  
Elongation At Break ◽  
Nanofibrous Scaffolds ◽  
Two Peaks

Design and fabrication of nanofibrous scaffolds should mimic the native extracellular matrix. This study is aimed at investigating electrospinning of polycaprolactone (PCL) blended with chitosan-gelatin complex. The morphologies were observed from scanning electron microscope. As-spun blended mats had thinner fibers than pure PCL. X-ray diffraction was used to analyze the degree of crystallinity. The intensity at two peaks at 2θof 21° and 23.5° gradually decreased with the percentage of chitosan-gelatin complex increasing. Moreover, incorporation of the complex could obviously improve the hydrophilicity of as-spun blended mats. Mechanical properties of as-spun nanofibrous mats were also tested. The elongation at break of fibrous mats increased with the PCL content increasing and the ultimate tensile strength varied with different weight ratios. The as-spun mats had higher tensile strength when the weight ratio of PCL to CS-Gel was 75/25 compared to pure PCL. Both as-spun PCL scaffolds and PCL/CS-Gel scaffolds supported the proliferation of porcine iliac endothelial cells, and PCL/CS-Gel had better cell viability than pure PCL. Therefore, electrospun PCL/Chitosan-gelatin nanofibrous mats with weight ratio of 75/25 have better hydrophilicity mechanical properties, and cell proliferation and thus would be a promising candidate for tissue engineering scaffolds.

The effect of finite deformations in the elastic stability of plane frames

1962 ◽  
Vol 266 (1324) ◽  
pp. 47-67 ◽  
Keyword(s):  
Critical Load ◽  
Failure Load ◽  
Elastic Stability ◽  
Load Level ◽  
Load Factor ◽  
Proportional Loading ◽  
Arbitrary Load ◽  
Plane Frames ◽  
The Difference ◽  
Rigid Joints

The circumstances are discussed under which orthogonal relations exist between the elastic critical modes of plane frames subjected to proportional loading. Orthogonal relations may be obtained provided the loading does not produce any components of deformation associated with any of the critical modes at arbitrary levels of the load factor, and provided no part of the structure remains statically indeterminate due to bar forces when all rigid joints are replaced by pin joints. When at arbitrary load factors, the structure deforms with components associated with any of the buckling modes, the elastic failure load is not identical with the lowest elastic critical load, although for many frames the two loads may be very close. A general expression is obtained which reveals the relation between the deformations at an arbitrary load level and the deflexions given by linear analysis. The difference between the elastic failure load and the elastic critical load is discussed, and an approximate treatment applicable to certain types of frame and associated loading is developed.

Characterization of Hot-Pressed Silicon Nitride Ceramics with Alkoxide-Derived Oxide Mixtures As the Sintering Aid

1992 ◽  
Vol 287 ◽  
Author(s):  
Y. Sato ◽  
C. Sakurai ◽  
M. Ueki ◽  
K. Sugita
Keyword(s):  
Mechanical Properties ◽  
Room Temperature ◽  
Weight Ratio ◽  
Sintering Aids ◽  
Sintering Aid ◽  
Oxide Powders ◽  
Nitride Ceramics ◽  
Final Weight ◽  
Alkoxide Method

ABSTRACTA homogeneous mixture of Y2O3, CeO2 and MgO with a final weight ratio of 3:1: 2 was prepared by the alkoxide method. The powder mixture was then added into Si3N4 powder in amounts ranging from 4 to 12 wt%, andconsolidated by hot-pressing. Microstructure and mechanical properties of the sintered bodies were determined and compared to those of materials prepared by the conventional route of mixing the oxide powders as sintering aids individually in essentially same composition. The β-fraction (modification ratio) in same composition was higher in thesintered bodies made through the alkoxide method than those made through the conventional one. The room temperature flexural strength was maximized with 6wt% addition of the alkoxide derived oxide, whereas, 12wt% addition of the total oxide was required to maximize the strength by conventional processing.

Rainwater effect on bearing strength of glass–epoxy laminated composite pinned joints

2016 ◽  
Vol 50 (30) ◽  
pp. 4269-4278 ◽  
Author(s):  
Onur Sayman ◽  
Ümran Esendemir
Keyword(s):  
Room Temperature ◽  
Failure Modes ◽  
Failure Load ◽  
Weight Ratio ◽  
Laminated Composite ◽  
Hole Diameter ◽  
Plastic Container ◽  
Specimen Width ◽  
Bearing Load ◽  
Pinned Joints

Composite materials are used in areas that have varying environmental conditions due to their advantages such as generally higher stiffness- and strength-to-weight ratio, and corrosion resistance compared to metallic alloys. This experimental study is carried out to investigate the bearing strengths and failure modes of woven glass–epoxy composite pinned joints subjected to rainwater. The specimens were immersed in rainwater in a closed plastic container indoors for 20 month periods at room temperature. The ratio of edge-distance-to-hole diameter (E/D) and the ratio of the specimen width-to-hole-diameter (W/D) were selected as parameters. Failure modes were determined by observing the failure regions on the specimens. Damage of immersed and unimmersed specimens was examined using scanning electron misroscopy for the same failure load. Experimental results showed that the bearing load values obtained from the specimens immersed in rainwater decreased in comparison to unimmersed specimens.

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