Investigating mechanical and thermo-physical properties of binder jet 3D printed elements using a statistical experiment approach

2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Bharath Seshadri ◽  
Kaushik Selva Dhanush Ravi ◽  
Illias Hischier ◽  
Arno Schlueter

Purpose With a growing list of available materials and processes, the inherent mechanical and thermophysical properties of three-dimensional (3D) prints are important design targets. This paper aims to study the functionality of binder jet 3D printed objects for thermally activated building construction elements and recyclable formwork for concrete structures. Design/methodology/approach Binder jet printed sand samples with various material and post-processing parameters (infiltration and baking) are prepared and studied. Using a statistical experiment design, the mechanical (flexural and compressive strength) and thermal (conductivity and specific capacity) characteristics are quantified. Findings Relative to the unprocessed “green” print samples, post-processing improved the flexural and compressive strength of the samples by factors of 6.9 and 21.6, respectively; the thermal conductivity and specific heat capacity were improved by factors of 7.7 and 1.2, respectively. For the investigated temperature range (20°C–200°C), the “green” prints showed excellent stability while the stability of post-processed samples depended on the infiltrate used. Microscopic images of the microstructures offered evidence to support improvement in the mechanical and thermo-physical characteristics of the 3D printed sand elements. Research limitations/implications The literature review concluded that optimal printing parameters and infiltration under vacuum could further improve the mechanical and thermo-physical properties of the binder jet printed elements. However, both these factors were not explored in this research. The statistical experimental design approach provided more flexibility to choose the number of experiments for a fixed amount of time and resources. However, for future work, a more extensive number of experiments and reproducibility testing for each combination of binder-infiltrate is recommended. Practical implications 3D printing has been identified as a promising opportunity to reduce material usage and improve construction efficiency in the field of architecture and building engineering. The emerging fabrication technologies are further expected to significantly reduce the operational energy of buildings through performance integration, i.e. multi-functional building elements with integrated heat- and mass-transfer capabilities to replace conventional systems. Originality/value This study has quantified the impact of infiltration on the mechanical and thermo-physical characteristics of sand-printed elements and, as such, reports reproducible functional performance maps for sand-print applications. The research demonstrates a way to achieve the desired functional characteristics of 3D prints through combinations of material selection and process/post-processing parameters.

2019 ◽  
Vol 801 ◽  
pp. 365-370
Author(s):  
Vivek Sood ◽  
S.K. Negi ◽  
B.M. Suman

In the present study, use of marble dust an inert filler produced by the marble cutting industries in the development of light weight block (LWB) of density 800 kg/m3 by non-auto clave method has been studied. Various mechanical and thermo-physical properties have been evaluated. It has been possible to replace cement by up to 20% when no additive is used. With the use of activator and super plasticizer at 50% replacement of cement by marble dust, compressive strength and water absorption are well within the Indian standard code 2185. With the use of accelerator and super plasticizer it is possible to reduce the de moulding time from 48 hrs to 6 hrs. Thermal conductivity of blocks varies from 1.16 to 2.30 [W/mK]. The variation in thermal conductivity depends upon its density which varies from 800 kg/m3 to 2400 kg/m3.


2020 ◽  
Vol 30 (12) ◽  
pp. 5143-5167
Author(s):  
Moataz Alosaimi ◽  
Daniel Lesnic ◽  
Jitse Niesen

Purpose This study aims to at numerically retrieve five constant dimensional thermo-physical properties of a biological tissue from dimensionless boundary temperature measurements. Design/methodology/approach The thermal-wave model of bio-heat transfer is used as an appropriate model because of its realism in situations in which the heat flux is extremely high or low and imposed over a short duration of time. For the numerical discretization, an unconditionally stable finite difference scheme used as a direct solver is developed. The sensitivity coefficients of the dimensionless boundary temperature measurements with respect to five constant dimensionless parameters appearing in a non-dimensionalised version of the governing hyperbolic model are computed. The retrieval of those dimensionless parameters, from both exact and noisy measurements, is successfully achieved by using a minimization procedure based on the MATLAB optimization toolbox routine lsqnonlin. The values of the five-dimensional parameters are recovered by inverting a nonlinear system of algebraic equations connecting those parameters to the dimensionless parameters whose values have already been recovered. Findings Accurate and stable numerical solutions for the unknown thermo-physical properties of a biological tissue from dimensionless boundary temperature measurements are obtained using the proposed numerical procedure. Research limitations/implications The current investigation is limited to the retrieval of constant physical properties, but future work will investigate the reconstruction of the space-dependent blood perfusion coefficient. Practical implications As noise inherently present in practical measurements is inverted, the paper is of practical significance and models a real-world situation. Social implications The findings of the present paper are of considerable significance and interest to practitioners in the biomedical engineering and medical physics sectors. Originality/value In comparison to Alkhwaji et al. (2012), the novelty and contribution of this work are as follows: considering the more general and realistic thermal-wave model of bio-heat transfer, accounting for a relaxation time; allowing for the tissue to have a finite size; and reconstructing five thermally significant dimensional parameters.


2017 ◽  
Vol 908 ◽  
pp. 118-122 ◽  
Author(s):  
Giedrius Balčiūnas ◽  
Viktor Kizinievič ◽  
Justinas Gargasas

Scientific literature mostly aims at investigation of composites with fibre hemp shives (FHS) aggregate and lime binder, although, such materials are characterised by pretty low mechanical properties. In order to obtain higher mechanical properties of a composite, it is appropriate to use cementitious binder. This work investigates physical properties of blocks from hemp shives aggregate and cementitious binder, manufactured in the expanded clay production line using vibro pressing technology. Following properties of the blocks are determined: freeze-thaw resistance, compressive strength, thermal conductivity and density. Thermal resistance according to EN ISO 6946 for the block with cavities is calculated as well. It is found that compressive strength of FHS-cement blocks may be up to 3.18 MPa when the density is of ~850 kg/m3 and thermal conductivity up to 0.135 W/(m∙K). It is found as well that the decrease of compressive strength is 8.7% after 25 freeze-thaw cycles.


Author(s):  
Anwar Ilmar RAMADHAN ◽  
Wan Hamzah AZMI ◽  
Rizalman MAMAT

In recent years, research has focused on enhancing the thermo-physical properties of a single component nanofluid. Therefore, hybrid or composite nanofluids have been developed to improve heat transfer performance. The thermo-physical properties of the Al2O3-TiO2-SiO2 nanoparticles suspended in a base of water (W) and ethylene glycol (EG) at constant volume ratio of 60:40 and different volume concentrations were investigated. The experiment was conducted for the volume concentrations of 0.05, 0.1, 0.2, and 0.3% of Al2O3-TiO2-SiO2 nanofluids at different temperatures of 30, 40, 50, 60, and 70 °C. Thermal conductivity and dynamic viscosity measurements were carried out at temperatures ranging from 30 to 70 °C by using KD2 Pro Thermal Properties Analyzer and Brookfield LVDV III Ultra Rheometer, respectively. The highest thermal conductivity for tri-hybrid nanofluids was obtained at 0.3% volume concentration, and the maximum enhancement was increased up to 9% higher than the base fluid (EG/W). Tri-hybrid nanofluids with a volume concentration of 0.05% gave the lowest effective thermal conductivity of 4.8 % at 70 °C temperature. Meanwhile, the dynamic viscosity of the tri-hybrid nanofluids was influenced by volume concentration and temperature. Furthermore, tri-hybrid nanofluids behaved as a Newtonian fluid for volume concentrations from 0.05 to 3.0%. The properties enhancement ratio (PER) estimated that the tri-hybrid nanofluids will aid in heat transfer for all samples in the present. The new correlations for thermal conductivity and dynamic viscosity of tri-hybrid nanofluids were developed with minimum deviation. As a conclusion, the combination of the enhancement in thermal conductivity and dynamic viscosity for tri-hybrid at 0.3% volume concentration was found the optimum condition with more advantage for heat transfer than other concentrations.


2010 ◽  
Vol 150-151 ◽  
pp. 144-149
Author(s):  
Hong Wei Xing ◽  
Jin Song Zhang ◽  
Xiao Ming Cao

Copper matrix composites reinforced with 3D-SiC network (15v% and 20v% SiC) were fabricated by squeezing copper alloy into 3D-SiC network preforms. The thermo-physical properties of the copper matrix composites were investigated. The specific heat capacities of the composites were about 0.39~0.50 J•g-1•K-1. The coefficients of thermal expansion (CTEs) of the composites were found to be lower than 6.9×10-6 -1 at Room Temperature. The composites exhibited high thermal stability for 3D-SiC network advent. The thermal conductivity of the composites was in the range of 50~80W•m−1•K−1. The thermo-physical properties of Cu matrix composites had a great relationship with the structures of 3D-SiC network preforms. The thermal conductivity of the composites decreased with an increase in the volume fraction of SiC or the structures of the limbs changing compacted, but the CTEs were not completely according this rule.


Author(s):  
Mazhar Hussain ◽  
Daniel Levacher ◽  
Nathalie Leblanc ◽  
Hafida Zmamou ◽  
Irini Djeran Maigre ◽  
...  

Crude bricks are composite materials manufactured with sediments and natural fibers. Natural fibers are waste materials and used in construction materials for reinforcement. Their reuse in manufacturing reinforced crude bricks is eco-friendly and improves mechanical and thermal characteristics of crude bricks. Factors such as type of fibers, percentage of fibers, length of fibers and distribution of fibers inside the bricks have significant effect on mechanical, physical and thermal properties of biobased composite materials. It can be observed by tests such as indirect tensile strength, compressive strength for mechanical characteristics, density, shrinkage, color for physical properties, thermal conductivity and resistivity for thermal properties, and inundation test for durability of crude bricks. In this study, mechanical and physical characteristics of crude bricks reinforced with palm oil fibers are investigated and effect of change in percentage and length of fibers is observed. Crude bricks of size 4*4*16 cm3 are manufactured with dredged sediments from Usumacinta River, Mexico and reinforced with palm oil fibers at laboratory scale. For this purpose, sediments and palm oil fibers characteristics were studied. Length of fibers used is 2cm and 3cm. Bricks manufacturing steps such as sediments fibers mixing, moulding, compaction and drying are elaborated. Dynamic compaction is opted for compaction of crude bricks due to energy control. Indirect tensile strength and compressive strength tests are conducted to identify the mechanical characteristics of crude bricks. Physical properties of bricks are studied through density and shrinkage. Durability of crude bricks is observed with inundation test. Thermal properties are studied with thermal conductivity and resistivity test. Distribution and orientation of fibers and fibers counting are done to observe the homogeneity of fibers inside the crude bricks. Finally, comparison between the mechanical characteristics of crude bricks manufactured with 2cm and 3cm length with control specimen was made.


Materials ◽  
2020 ◽  
Vol 13 (18) ◽  
pp. 4066
Author(s):  
Marta Czajkowska ◽  
Ewa Walejewska ◽  
Łukasz Zadrożny ◽  
Monika Wieczorek ◽  
Wojciech Święszkowski ◽  
...  

This study was conducted to test possibilities of application of 3D printed dental models (DMs) in terms of their accuracy and physical properties. In this work, stone models of mandibles were cast from alginate impressions of 10 patients and scanned in order to obtain 3D printed acrylic replicas. The diagnostic value was tested as matching of model scans on three levels: peak of cusps, occlusal surface, and all teeth surfaces. The mechanical properties of acrylic and stone samples, specifically the impact strength, shore D hardness, and flexural and compressive strength were investigated according to ISO standards. The matching of models’ surfaces was the highest on the level of peaks of cusps (average lack of deviations, 0.21 mm) and the lowest on the level of all teeth surfaces (average lack of deviations, 0.64 mm). Acrylic samples subjected to mechanical testing, as expected, showed higher mechanical properties as compared to the specimens made of dental stone. In the present study we demonstrated that 3D printed acrylic models could be ideal representatives in the case of use as a diagnostic tool and as a part of medical records. The acrylic samples exhibited not only higher mechanical properties, but also showed better accuracy comparing to dental stone.


2020 ◽  
Vol 26 (9) ◽  
pp. 1647-1656
Author(s):  
Weiwei Wu ◽  
Zhouzhou Wang ◽  
Shuang Ding ◽  
Aiping Song ◽  
Dejia Zhu

Purpose The effects of infiltrant-related factors during post-processing on mechanical performance are fully considered for three-dimensional printing (3DP) technology. The factors contain infiltrant type, infiltrating means, infiltrating frequency and time interval of infiltrating. Design/methodology/approach A series of printing experiments are conducted and the parts are processed with different conditions by considering the above mentioned four parameters. Then the mechanical performances of the parts are tested from both macroscopic and microscopic papers. In the macroscopic view, the compressive strength of each printed part is measured by the materials testing machine – Instron 3367. In the microscopic view, scanning electron microscope and energy dispersion spectrum are used to obtain microstructure images and element content results. The pore size distributions of the parts are measured further to illustrate that if the particles are bound tightly by infiltrant. Then, partial least square (PLS) is used to conduct the analysis of the influencing factors, which can solve the small-sample problem well. The regression analysis and the influencing degree of each factor are explored further. Findings The experimental results show that commercial infiltrant has an outstanding performance than other super glues. The infiltrating action will own higher compressive strength than the brushing action. The higher infiltrating frequency and inconsistent infiltrating time interval will contribute to better mechanical performance. The PLS analysis shows that the most important factor is the infiltrating method. When compare the fitted value with the actual value, it is clear that when the compressive strength is higher, the fitting error will be smaller. Practical implications The research will have extensive applicability and practical significance for powder-based additive manufacturing. Originality/value The impact of the infiltrating-related post-processing on the performance of 3DP technology is easy to be ignored, which is fully taken into consideration in this paper. Both macroscopic and microscopic methods are conducted to explore, which can better explain the mechanical performance of the parts. Furthermore, as a small-sample method, PLS is used for influencing factors analysis. The variable importance in the projection index can explain the influencing degree of each parameter.


2020 ◽  
Vol 10 (4) ◽  
pp. 1314
Author(s):  
Haihua Wu ◽  
Kui Chen ◽  
Yafeng Li ◽  
Chaoqun Ren ◽  
Yu Sun ◽  
...  

The 3D graphite/ceramic composite prototyping parts directly prepared by selective laser sintering (SLS) were porous, which led to poor strength and low thermal conductivity. In order to obtain low thermal conductivity and high strength, its thermal conductivity and compressive strength were adjusted by changing the mixture powder composition and adding post-processing. The result showed that the addition of silicon powder in the mixture powder could significantly improve the compressive strength and thermal conductivity. The addition of expanded graphite was beneficial to the formation of the closed pores in the matrix, which slightly reduced the compressive strength but significantly reduced the thermal conductivity. The 3D graphite/ceramic composite part showed an order of magnitude improvement in compressive strength (from 1.25 to 13.87 MPa) but relatively small change in thermal conductivity (from 1.40 to 2.12 W·m−1K−1) and density (from 0.53 to 1.13 g·cm−3) by post-processing. Reasonable mixture powder composition and post-processing were determined and realized the possibility of fabricating a 3D graphite/ceramic composite part with low thermal conductivity but high compressive strength. Furthermore, it could be used for the repeated casting of steel castings, and through the comparative analysis of casting defects, the prepared graphite/ceramic composite part was expected to replace water glass sand mold.


2019 ◽  
Vol 25 (4) ◽  
pp. 744-751 ◽  
Author(s):  
Xiaomiao Niu ◽  
Hongyao Shen ◽  
Guanhua Xu ◽  
Linchu Zhang ◽  
Jianzhong Fu ◽  
...  

Purpose Mg-Al powder mixture was used to manufacture Mg-Al alloy by laser powder bed fusion (LPBF) process. This study aims to investigate the influence of initial Al content and processing parameters on the formability, microstructure and consequent mechanical properties of the laser powder bed fused (LPBFed) component. Design/methodology/approach In this study, Al powder with different weight ratio ranged from 3 to 9 per cent was mixed with pure Mg powder, and the powder mixture was processed using different LPBF parameters. Microstructure and compressive properties of the LPBFed components were examined. Findings It was found that the presence of Al significantly modified the microstructure and improved the mechanical properties of the LPBFed components. Higher volume of ß-Al12Mg17 precipitates was produced at higher initial Al content and higher laser energy density. For this reason, the a-Mg was significantly refined and the compressive strength was improved. The highest yield compressive strength achieved was 279 MPa when using Mg-9 Wt. % Al mixture. Originality/value This work demonstrates that LPBF of Mg-Al powder mixture was a viable way to additively manufacture Mg-Al alloy. Both Al content and processing parameters can be modified to control the microstructure and mechanical properties of the LPBFed components.


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