Mechanical properties and erosive behaviour of 10TiO2-Cr2O3 coated CA6NM turbine steel under accelerated conditions

2019 ◽  
Vol 16 (1) ◽  
pp. 64-70 ◽  
Author(s):  
Khushdeep Goyal
Keyword(s):  
Mechanical Properties ◽  
Mass Loss ◽  
Average Particle Size ◽  
Average Particle ◽  
Slurry Erosion ◽  
Experimental Conditions ◽  
Content Type ◽  
Uncoated Steel ◽  
Erosion Test ◽  
Turbine Steel

Purpose This paper aims to evaluate the mechanical properties and slurry erosion behaviour of 10TiO2-Cr2O3 coated turbine steel. Design/methodology/approach Slurry erosion experiments were performed on the coated turbine steel specimens using slurry erosion test rig under accelerated conditions such as rotational speed, average particle size and slurry concentration. Surface roughness tester, Vickers microhardness tester and scanning electron microscope were used to analyse erosion mechanism. Findings Under all experimental conditions, 10TiO2-Cr2O3 coated steel showed better slurry erosion resistance in comparison with Al2O3 coated and uncoated steel specimens. Each experimental condition indicated a significant effect on the erosion rate of both coatings and uncoated steel. The surface analysis of uncoated eroded specimen revealed that plastic deformation, ploughing and deep craters formation were the reasons for mass loss, whereas microchipping, ploughing and microcutting were the reasons for mass loss of coated specimens. Originality/value The present investigation provides novel insight into the comparative slurry erosion performance of high velocity oxy fuel deposited 10TiO2-Cr2O3 and Cr2O3 coatings under various environmental conditions. To form modified powder, 10 Wt.% TiO2 was added to 90 Wt.% Cr2O3.

Slurry erosion performance study of HVFS sprayed Ni-20Al2O3 and Ni-15Al2O3-5TiO2 coatings under hydro accelerated conditions

2018 ◽  
Vol 70 (4) ◽  
pp. 805-817 ◽  
Author(s):  
Rajeev Kumar ◽  
Sanjeev Bhandari ◽  
Atul Goyal ◽  
Yogesh Kumar Singla
Keyword(s):  
Particle Size ◽  
Rotational Speed ◽  
Average Particle Size ◽  
Synergetic Effect ◽  
Average Particle ◽  
Flame Spray ◽  
Slurry Erosion ◽  
Content Type ◽  
Slurry Concentration ◽  
Ca6nm Steel

Purpose This paper aims to cover all the aspects of development, investigation and analysis phases to evaluate the slurry erosion performance of test coatings. The powders having composition of Ni-20Al2O3 and Ni-15Al2O3-5TiO2 were deposited on CA6NM grade turbine steel by using high velocity flame spray (HVFS) technique. The characterization of the coatings was done with the help of SEM/EDS and XRD techniques. Various properties such as micro-hardness and bonding strength of the coatings were also evaluated. Thereafter, these coatings were subjected to an indigenously developed high speed slurry erosion tester at different levels of rotational speed, erodent particle size and slurry concentration. The effect of these parameters on the erosion behavior of coatings was also evaluated. The slurry erosion tests and SEM of the eroded surfaces revealed remarkable improvement in slurry erosion resistance of Ni-15Al2O3-5TiO2 coating in comparison with Ni-20Al2O3 coating. Design/methodology/approach Two different compositions of HVFS coating were developed onto CA6NM steel. Subsequently, these coatings were evaluated by means of mechanical and microstructural characterization. Further, slurry erosion testing was done to analyze the erosive wear behavior of developed coatings. Findings The coatings were successfully developed by HVFS process. Cross-sectional microscopic analysis of sprayed coatings revealed a continuous and defect-free contact between substrate and coating. Ni-15Al2O3-5TiO2 coating showed higher value of bond strength in comparison with Ni-20Al2O3 coating. Under all the testing conditions, Ni-15Al2O3-5TiO2 coatings showed higher resistance to slurry erosion in comparison with Ni-20Al2O3 coatings. Rotational speed, average particle size of erodent and slurry concentration were found to have proportional effect on specific mass loss of coatings. The mixed behavior (brittle as well as ductile) of the material removal mechanism was observed for the coatings. Originality/value From the literature review, it was found that researchers have documented the various studies on Ni-Al2O3, Ni-TiO2 and Al2O3-TiO2 coatings. No one has ascertained the synergetic effect of Alumina and Titania on the slurry erosion performance of Nickel-based coating. In view of this, the authors have developed Ni-Al2O3 and Ni-Al2O3-TiO2 coatings, and an attempt has been made to compare their mechanical, microstructural and slurry erosion characteristics.

Slurry erosion behavior of plasma sprayed coating on turbine steel

2019 ◽  
Vol 71 (1) ◽  
pp. 1-9 ◽  
Author(s):  
Sarbjeet Kaushal ◽  
Satnam Singh
Keyword(s):  
Abrasive Wear ◽  
Rotational Speed ◽  
Silica Sand ◽  
Average Particle ◽  
Slurry Erosion ◽  
Content Type ◽  
Erosion Behavior ◽  
Turbine Steel ◽  
Sprayed Coating ◽  
Plasma Sprayed

PurposeThe purpose of this paper is to study the effect of slurry erosion at different parameters on plasma sprayed Cr3C2coated 13Cr4Ni turbine steel and compare the results of coated steel with bare steel.Design/methodology/approachCr3C2+ 25NiCr coating was successfully developed on 13Cr4Ni turbine steel using plasma spraying method. The slurry erosion test was performed using a simulated erosion testing rig. The commercially available silica sand was used as abrasive media and the effect of concentration (ppm), average particle sizes and rotational speed on the slurry erosion behavior were studied at 300 and 900 impact angles. Developed coatings were characterized by scanning electron microscope, XRD, EDS and micro hardness tests and study of erosion wear.FindingsResults revealed that three times higher hardness of coatings was obtained because of the hard phases of chromium carbide and nickel carbide, which restricted the abrasive wear in comparison to uncoated steel. Lower abrasive wear was observed at 900 impact angle coupled with lower levels of slurry concentration and rotational speed. Further, it was observed that initially cumulative mass loss rate was high which gets stabilized after the surface become smooth and on exposing for higher periods. Overall results indicated that erosive wear was reduced significantly by the application of developed coating.Originality/valueThe developed plasma sprayed coating is very useful to enhance the service life of turbine steel by lowering the effect of slurry erosion.

Erosive Wear Study of HVOF Spray Cr3C2–NiCr Coated CA6NM Turbine Steel

2014 ◽  
Vol 136 (4) ◽  
Author(s):  
Deepak Kumar Goyal ◽  
Harpreet Singh ◽  
Harmesh Kumar ◽  
Varinder Sahni
Keyword(s):  
High Speed ◽  
Protective Coatings ◽  
Average Particle Size ◽  
Erosive Wear ◽  
Average Particle ◽  
Slurry Erosion ◽  
Spray Process ◽  
Hvof Spray ◽  
Turbine Steel ◽  
Ca6nm Steel

Degradation of surfaces of hydroturbine components caused by impact of abrasive particles carried by flowing water is a serious issue. To counteract the same, surface modification of turbine materials by the application of protective coatings is gaining popularity these days. In this work, Cr3C2–NiCr coating was deposited on CA6NM turbine steel by the HVOF spray process and studied with regard to its performance under different slurry erosion conditions. The effect of three parameters, namely average particle size of slurry particles, speed (rpm), and slurry concentration on slurry erosion of this coating material, was studied by using a high speed erosion test rig. The analysis of the surfaces of the samples before and after slurry erosion tests was done by using SEM. The HVOF sprayed Cr3C2–NiCr coating showed very good performance under slurry erosion in comparison with uncoated CA6NM steel.

Physicochemical characterization of cow horn ash and its effect as filler material on the mechanical property of polyester-banana fibre composite

2020 ◽  
Vol 17 (6) ◽  
pp. 823-829
Author(s):  
Ernest Mbamalu Ezeh ◽  
O.D. Onukwuli
Keyword(s):  
Mechanical Properties ◽  
Fibre Composite ◽  
Average Particle Size ◽  
Physicochemical Characterization ◽  
Spectrometric Analysis ◽  
Average Particle ◽  
Matrix Composites ◽  
Content Type ◽  
X Ray ◽  
Banana Fibre

Purpose The purpose of this paper is to observe the effect of cheap cow horn ash particles (CHAp) filler as a possible replacement for expensive fillers on the mechanical properties of polyester-banana peduncle fibre (BPF) composites were evaluated using standard procedures. Design/methodology/approach Composite was developed using CHAp as a filler component, polyester resin and BPF, with the filler of varying percentage weights (5%, 10%, 15% and 20%), at particle sizes of 125 µm, using hand lay-up technique. The physicochemical properties of CHAp were examined through x-ray fluorescence (XRF), X-ray diffractometer (XRD), transmission electron microscopy, scanning electron microscope, energy dispersion spectrometric analysis (EDS) and density. Mechanical properties of the developed composites were also examined. Findings The results showed that the tensile properties and impact strength of the composites reduced marginally with the incorporation of the cow horn ash particle as a filler. However, the flexural strength of the composites increased progressively with the incorporation of BPF as the fibre loading increased. The major constituents of CHAp were CaO from XRF study, calcite (CaCO3) from XRD study and Ca in EDS study in accordance with the analytical parameter, which showed a major component of calcium. The high value of CaCO3 in CHAp improved flexural and impact strengths of the composites. CHAp presented around solid and irregular shape particle characteristic of most fillers with an average particle size of 98.13 nm. The tensile and flexural strengths of the polyester matrix composites obtained at 7.5% BPF: 7.5% CHAp was 117.87 MPa depicting satisfactory mechanical characteristics. Originality/value Generally, cow horn ash particle exhibited adequate filler component potential in composite production in keeping with its property effects on the mechanical properties of polyester-BPF composites.

Erosion characteristics on surface texture of additively manufactured AlSi10Mg alloy in SiO2 quartz added slurry environment

2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Recep Demirsöz ◽  
Mehmet Erdl Korkmaz ◽  
Munish Kumar Gupta ◽  
Alberto Garcia Collado ◽  
Grzegorz M. Krolczyk
Keyword(s):  
Surface Roughness ◽  
Weight Loss ◽  
Wear Resistance ◽  
Erosive Wear ◽  
Oxide Ceramics ◽  
Slurry Erosion ◽  
Content Type ◽  
Test Setup ◽  
Quartz Sands ◽  
Erosion Test

Purpose The main purpose of this work is to explore the erosion wear characteristics of additively manufactured aluminium alloy. Additive manufacturing (AM), also known as three-dimensional (3D) manufacturing, is the process of manufacturing a part designed in a computer environment using different types of materials such as plastic, ceramic, metal or composite. Similar to other materials, aluminum alloys are also exposed to various wear types during operation. Production efficiency needs to be aware of its reactions to wearing mechanisms. Design/methodology/approach In this study, quartz sands (SiO2) assisted with oxide ceramics were used in the slurry erosion test setup and its abrasiveness on the AlSi10Mg aluminum alloy material produced by the 3D printer as selective laser melting (SLM) technology was investigated. Quartz was sieved with an average particle size of 302.5 µm, and a slurry environment containing 5, 10 and 15% quartz by weight was prepared. The experiments were carried out at the velocity of 1.88 (250 rpm), 3.76 (500 rpm) and 5.64 m/s (750 rpm) and the impact angles 15, 45 and 75°. Findings With these experimental studies, it has been determined that the abrasiveness of quartz sand prepared in certain particle sizes is directly related to the particle concentration and particle speed, and that the wear increases with the increase of the concentration and rotational speed. Also, the variation of weight loss and surface roughness of the alloy was investigated after different wear conditions. Surface roughness values at 750 rpm speed, 10% concentration and 75° impingement angle are 0.32 and 0.38 µm for 0 and 90° samples, respectively, with a difference of approximately 18%. Moreover, concerning a sample produced at 0°, the weight loss at 250 rpm at 10% concentration and 45° particle impact angle is 32.8 mg, while the weight loss at 500 rpm 44.4 mg, and weight loss at 750 rpm is 104 mg. Besides, the morphological structures of eroded surfaces were examined using the scanning electron microscope to understand the wear mechanisms. Originality/value The researchers verified that this specific coating condition increases the slurry wear resistance of the mentioned steel. There are many studies about slurry wear tests; however, there is no study in the literature about the quartz sand (SiO2) assisted slurry-erosive wear of AlSi10Mg alloy produced with AM by using SLM technology. This study is needed to fill this gap in the literature and to examine the erosive wear capability of this current material in different environments. The novelty of the study is the use of SiO2 quartz sands assisted by oxide ceramics in different concentrations for the slurry erosion test setup and the investigations on erosive wear resistance of AlSi10Mg alloy manufactured by AM.

Fe3O4 Magnetic Preparation by Bauxite Ore Washing Fine Mud

2014 ◽  
Vol 1010-1012 ◽  
pp. 961-965
Author(s):  
Jian Qiang Xiao ◽  
Guo Wei He ◽  
Yan Jin Hu
Keyword(s):  
Particle Size ◽  
Aging Time ◽  
Average Particle Size ◽  
Xrd Analysis ◽  
Test Methods ◽  
Raw Material ◽  
Molar Ratio ◽  
Average Particle ◽  
Experimental Conditions ◽  
Particle Size Analyzer

Bauxite waste sludge as a raw material, the use of reverse chemical coprecipitation synthesize Fe3O4. Researching temperature, precipitation concentration, aging time and Fe2+/Fe3+ molar ratio effect on the particle size, morphology. Optimal experimental conditions: temperature 70 °C, the precipitant NaOH mass ratio of 10%, aging time 3h, Fe2+/Fe3+ molar ratio of 2:3. Test methods using a laser particle size analyzer, XRD analysis of the products were characterized, the product is Fe3O4, the average particle size of 0.11mm.

Experimental Study on the Effects of Internal Erosion on the Physical and Mechanical Properties of Tailings Under Unsteady Seepage

2021 ◽  
Author(s):  
Rong Gui ◽  
Guicheng He
Keyword(s):  
Mechanical Properties ◽  
Particle Size ◽  
Shear Strength ◽  
Average Particle Size ◽  
Physical And Mechanical Properties ◽  
Internal Erosion ◽  
Average Particle ◽  
Sand Column ◽  
Sedimentary Characteristics ◽  
Seepage Erosion

Abstract In this paper, the hydraulic sedimentary model was established to investigate the effects of dry beach slope on the sedimentary characteristics of tailings, and the sand column model was built to investigate the effects of seepage erosion on the physical and mechanical properties of sedimentary tailings under unsteady seepage.The results show that the slope of dry beach have a great effect on the sedimentary characteristics of tailings, the average particle size of tailings decreases along the slope of dry beach, and the larger the slope, the more obvious the stratification of the tailings. The migration of fine-grained tailings caused by seepage erosion increases the permeability of the tailings and reduces the shear strength of the tailings. After seepage erosion,the average particle size of 1#tailings sample, 2#tailings sample and 3#tailings sample increased by 6.4%, 12.0% and 2.4% respectively, the hydraulic conductivity of 1# tailings sample, 2# tailings sample and 3# tailings increased by 27.2%,17.9%, and 15.3% respectively after internal erosion, and the shear strength of 1#tailings sample, 2#tailings sample and 3#tailings sample tailings sample decreased by 20.9 %, 15.1% and 12.4% respectively.

Study on Mechanical Properties of AA6061/SiC/B4C Hybrid Nano Metal Matrix Composites

2021 ◽  
Vol 1034 ◽  
pp. 35-42
Author(s):  
Shubhajit Das ◽  
M. Chandrasekaran ◽  
Sutanu Samanta
Keyword(s):  
Mechanical Properties ◽  
High Performance ◽  
Matrix Material ◽  
Average Particle Size ◽  
Volume Ratio ◽  
Casting Process ◽  
Hybrid Nanocomposites ◽  
Average Particle ◽  
Matrix Composites ◽  
Structural Applications

The present work investigates the mechanical characterization of aluminium alloy (AA) 6061 based hybrid nanometal matrix composites (MMCs) fabricated using conventional stir casting process. Two compositions viz., AA6061+1.5 wt.% B4C+0.5 wt.% SiC (Hybrid A) and AA6061+1.5 wt.% B4C+1.5 wt.% SiC (Hybrid B) was prepared and its mechanical properties such as microhardness, tensile, compressive, flexural and impact strength were investigated to compare with unreinforced AA6061. SiC and B4C ceramic particles (purity 99.89%) of average particle size of 50 nm were used as reinforcements. Significant enhancement in microhardness of 30.2% and 31.02% for hybrid A and B are observed respectively. The ultimate tensile strength (UTS) increased by 10.72% and 16.55% for hybrid A and B respectively. Improved interaction because of the enhanced surface to volume ratio at the interface resulted in improvement of mechanical properties. Field emission scanning electron microscopy (FESEM) of the fractured surface shows brittle fracture because of the incorporation of the ceramic reinforcements in the matrix material. The developed AA6061/SiC/B­4C hybrid nanocomposites show improved mechanical properties for high-performance structural applications.

scholarly journals Properties of Vulcanized Polyisoprene Rubber Composites Filled with Opalized White Tuff and Precipitated Silica

2014 ◽  
Vol 2014 ◽  
pp. 1-9 ◽  
Author(s):  
Suzana Samaržija-Jovanović ◽  
Vojislav Jovanović ◽  
Gordana Marković ◽  
Ivana Zeković ◽  
Milena Marinović-Cincović
Keyword(s):  
Mechanical Properties ◽  
Production Efficiency ◽  
Average Particle Size ◽  
Rubber Matrix ◽  
Average Particle ◽  
Cross Link ◽  
Rubber Composites ◽  
Precipitated Silica ◽  
Reinforcing Effects ◽  
Cure Characteristic

Opalized white tuff (OWT) with 40 μm average particle size and 39.3 m2/g specific surface area has been introduced into polyisoprene rubber (NR). Their reinforcing effects were evaluated by comparisons with those from precipitated silica (PSi). The cure characteristic, apparent activation energy of cross-link (Eac) and reversion (Ear), and mechanical properties of a variety of composites based on these rubbers were studied. This was done using vulcanization techniques, mechanical testing, and scanning electron microscopy (SEM). The results showed that OWT can greatly improve the vulcanizing process by shortening the time of optimum cure (tc90) and the scorch time (ts2) of cross-linked rubber composites, which improves production efficiency and operational security. The rubber composites filled with 50 phr of OWT were found to have good mechanical and elastomeric properties. The tensile strengths of the NR/OWT composites are close to those of NR/PSi composites, but the tear strength and modulus are not as good as the corresponding properties of those containing precipitated silica. Morphology results revealed that the OWT is poorly dispersed in the rubber matrix. According to that, the lower interactions between OWT and polyisoprene rubber macromolecules are obtained, but similar mechanical properties of NR/OWT (100/50) rubber composites compared with NR/PSi (100/50) rubber composites are resulted.

Fabrication of A356-based rolled composites reinforced by Ni–P-coated bimodal ceramic particles

2016 ◽  
Vol 232 (10) ◽  
pp. 803-815 ◽  
Author(s):  
R Kheirifard ◽  
N Beigi Khosroshahi ◽  
R Azari Khosroshahi ◽  
R Taherzadeh Mousavian ◽  
D Brabazon
Keyword(s):  
Mechanical Properties ◽  
Particle Size ◽  
Average Particle Size ◽  
Microstructural Characterization ◽  
Rolling Process ◽  
Stir Casting ◽  
Ceramic Particle ◽  
Average Particle ◽  
Ceramic Particles ◽  
Sic Particles

Three arrangements of reinforced A356-based composites were fabricated. Samples with 3 wt% Al2O3 (average particle size: 170 µm), 3 wt% SiC (average particle size: 15 µm), and 3 wt% of mixed Al2O3–SiC powders (each reinforcement 1.5 wt%) were fabricated. The novel fabrication process of two-step stir casting followed by rolling was utilized. Analysis of the effect of using bimodal-sized ceramic particles and process parameters on the microstructure and mechanical properties of the composites was examined. Electroless deposition of nickel was used to improve the wettability of the ceramic reinforcements by the molten metal. From microstructural characterization, it was found that fine SiC particles were agglomerated, including when coated with Ni–P. It was also revealed that the rolling process broke the fine silicon platelets within the A356 matrix, which were mostly observed around the Al2O3 particles. The processed microstructure of the composite was altered in comparison to conventionally cast A356 MMC by translocation of the fractured silicon particles, by improving the distribution of fine SiC particles, and by elimination of porosities remaining after casting. A good bonding quality at matrix–ceramic interface was formed during casting and no significant improvement was found in this regard after the rolling process. The mechanical properties of the composites tested showed that the samples, which contained the bimodal ceramic particle distribution of coarse Al2O3 and fine SiC particles produced the highest levels of composite strength and hardness.

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