New Routine to Determine Microstructures of Metallic Interconnectors Using SEM-EBSD Technique

2021 ◽  
Author(s):  
Jiang Wu ◽  
Eugene Choo
Keyword(s):  
Ebsd Technique

Investigation of the Deformation Twins on the Bending Cross Section of TA2 Titanium Sheet

2020 ◽  
Vol 837 ◽  
pp. 41-45
Author(s):  
Shuai Sun ◽  
Kai Hua Liu
Keyword(s):  
Electron Backscatter Diffraction ◽  
Testing Machine ◽  
Pure Titanium ◽  
Titanium Sheet ◽  
Bending Tests ◽  
Three Point Bending ◽  
Deformation Twins ◽  
Ebsd Technique ◽  
Backscatter Diffraction ◽  
Deformation Area

In order to determine the evolution features of deformation twins for TA2 commercial pure titanium (cp-TA2), the TA2 samples were bent under different bending angles in three-point bending tests via a universal testing machine. The electron backscatter diffraction (EBSD) technique was applied to identify the grain boundaries (GBs) and twin boundaries (TBs) in the bending areas. The results reveal that the type of deformation area would effect the evolution of different deformation twins. It is inferred that the state of stress would promote the multiplication of the same type of deformation twins.

scholarly journals On the through-process texture evolution assessment in grain oriented Fe-3 wt% Si steel produced by a novel directional inoculation technique

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Snehashish Tripathy ◽  
Sandip Ghosh Chowdhury
Keyword(s):  
Magnetic Field ◽  
Hot Rolling ◽  
Texture Evolution ◽  
Lattice Parameter ◽  
Soft Magnetic ◽  
Oriented Growth ◽  
Inoculation Technique ◽  
Hot Band ◽  
Ebsd Technique ◽  
Cast Microstructure

AbstractA novel directional inoculation technique has been designed to cast thin slab ingots containing Goss (or near Goss) oriented components in the as cast microstructure under the combined effect of oriented nucleation and oriented growth. The same has been targeted so as to retain Goss orientations and simultaneously develop γ fiber components (ranging from {111}<$$1\overline{1}0$$ 1 1 ¯ 0 > to {111}<112>) during hot rolling. The designed scheme of directional inoculation achieved oriented nucleation by the effect of exogenously added soft magnetic inoculants under magnetic field and oriented growth by the effect of fast cooling rates prevailing in the mould. The choice of 65Fe–35Co (wt%) system as soft magnetic inoculants was made taking into account the similarity in crystal structure and lattice parameter. The chemically synthesized inoculants under the effect of external magnetic field during solidification were able to exhibit directional inoculation. Variation in the cast microstructure and microtexture by varying the extent of inoculant addition was studied by EBSD technique. The ingots cast under different conditions were subjected to a designed hot rolling schedule and the through process microstructural and microtextural evolution was assessed. It was observed that fine equiaxed grains with initial cube orientations in the as cast structure could lead to the most desirable microstructural as well as microtextural gradient in the hot band.

scholarly journals Symmetry Breakdown Related Fracture in 42CrMo4 Steel

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 344
Author(s):  
Jian Feng ◽  
Stefan Barth ◽  
Marc Wettlaufer
Keyword(s):  
Orientation Distribution ◽  
High Symmetry ◽  
Symmetry Breakdown ◽  
Pole Figures ◽  
Crystallographic Symmetry ◽  
42Crmo4 Steel ◽  
Austenite Grains ◽  
Ebsd Technique ◽  
Complete Transformation ◽  
Start Temperature

Austenite grains that underwent the f.c.c. to b.c.c. (or b.c.t.) transformation are typically composed of 24 Kurdjumov–Sachs variants that can be categorized by three axes of Bain transformations; thus, a complete transformation generally displays 3-fold symmetry in (001) pole figures. In the present work, crystallographic symmetry in 42CrMo4 steel austempered below martensite start temperature was investigated with the help of the orientation distribution function (ODF) analysis based on the FEG-SEM/EBSD technique. It is shown that, upon phase transformations, the specimens contained 6-fold symmetry in all (001), (011), and (111) pole figures of an ODF. The ODF analysis, verified by theoretical modeling, showed that under plane-strain conditions cracks prefer to propagate through areas strongly offset by the high symmetry. The origin of high symmetry was investigated, and the mechanism of the symmetry breakdown was explained.

scholarly journals Microstructure Evaluation Study of Al5083 Alloy Using EBSD Technique after Processing with Different ECAP Processes and Temperatures

Crystals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 862
Author(s):  
Muneer Baig ◽  
Asiful H. Seikh ◽  
Ateekh Ur Rehman ◽  
Jabair A. Mohammed ◽  
Faraz Hussain Hashmi ◽  
...  
Keyword(s):  
Grain Refinement ◽  
Evaluation Study ◽  
Coarse Grained ◽  
Angular Pressing ◽  
Microstructure Evaluation ◽  
Microstructural Evaluation ◽  
Higher Temperature ◽  
Ebsd Technique ◽  
Number Of Passes ◽  
Positive Effect

The temperature effects on the microstructural evolution of a coarse-grained Al5083 alloy during equal channel angular pressing (ECAP), were studied at ambient and high temperatures. The microstructural evaluation was done using an EBSD (electron backscattering diffraction) process. The grain refinement occurred as the number of passes increased, which had a positive effect on its strength. Additionally, increasing the pressing temperature leads to a decrease in the new grain’s formation and an increase in the normal grain size in the third pass. This can be ascribed to the unwinding of strain similarity between the grains because of the continuous activity of dynamic recuperation and the grain limit sliding occurring at a higher temperature. The attainment of grain refinement is examined exhaustively in this study.

Direct Observations of Cube Nucleation from Intergranular Cube Segments in Cold Rolled Al-Mn

2012 ◽  
Vol 715-716 ◽  
pp. 354-359
Author(s):  
Adeline Albou ◽  
S. Raveendra ◽  
P. Karajagikar ◽  
Indradev Samajdar ◽  
Julian H. Driver ◽  
...  
Keyword(s):  
Local Deformation ◽  
Direct Observations ◽  
Deformation Substructure ◽  
Cold Rolled ◽  
Ebsd Technique

Two major types of Cube bands/segments have been observed in heavily (90%) cold rolled Al-0.1wt %Mn using the EBSD technique with a FEG SEM: i) intergranular transition bands as thin cube segments aligned along RD between S and Cu oriented grains and ii) as transgranular strain localized bands situated in some particular grains. Their evolution is studied by light annealing at 275°C and 300°C and EBSD observations of exactly the same areas to directly correlate local deformation substructure with recrystallization. Only the intergranular cube transition bands give rapid recrystallization nucleation to cube grains of dimension >10µm. In particular the fastest growing cube grains have a near 40°<111> relation with part of their surroundings.

Microstructural Studies of NiCoMnIn Magnetic Shape Memory Ribbons

2013 ◽  
Vol 738-739 ◽  
pp. 436-440 ◽  
Author(s):  
Krystian Prusik ◽  
Katarzyna Bałdys ◽  
Danuta Stróż ◽  
Tomasz Goryczka ◽  
Józef Lelątko
Keyword(s):  
Melt Spinning ◽  
Room Temperature ◽  
Parent Phase ◽  
Magnetic Shape Memory ◽  
Melt Spun ◽  
Columnar Grains ◽  
Ebsd Technique ◽  
Microstructural Studies ◽  
Melt Spinning Technique ◽  
Scanning Electron

In present paper two ribbons of the Ni44Co6Mn36In14 (at.%) were prepared under different melt-spinning technique conditions. Microstructure of the ribbons was studied by scanning electron microscopy (SEM). Depending on the liquid ejection overpressure two types of ribbons microstructures were observed. Ribbon T1 for which ejection overpressure was 1.5 bar showed typical melt-spun ribbon microstructure consisting of a top layer of small equi-axial grains and columnar grains below. For T2 ribbon (ejection overpressure 0.2 bar) only a small fraction of the columnar grains were observed. Structure analysis of the ribbons performed by XRD showed that at room temperature both ribbons have B2 parent phase superstructure. No gamma phase precipitates were observed. In order to determine the orientation of the grains the EBSD technique was applied.

scholarly journals On the Use of EBSD and Microhardness to Study the Microstructure Properties of Tungsten Samples Prepared by Selective Laser Melting

Materials ◽  
2021 ◽  
Vol 14 (5) ◽  
pp. 1215
Author(s):  
Mirza Atif Abbas ◽  
Yan Anru ◽  
Zhi Yong Wang
Keyword(s):  
Selective Laser Melting ◽  
Electron Backscatter Diffraction ◽  
Fusion Reactors ◽  
Laser Melting ◽  
Kikuchi Pattern ◽  
Plasma Facing Components ◽  
Electron Backscatter ◽  
Ebsd Technique ◽  
Temperature Exposure ◽  
Backscatter Diffraction

Additively manufactured tungsten and its alloys have been widely used for plasma facing components (PFCs) in future nuclear fusion reactors. Under the fusion process, PFCs experience a high-temperature exposure, which will ultimately affect the microstructural features, keeping in mind the importance of microstructures. In this study, microhardness and electron backscatter diffraction (EBSD) techniques were used to study the specimens. Vickers hardness method was used to study tungsten under different parameters. EBSD technique was used to study the microstructure and Kikuchi pattern of samples under different orientations. We mainly focused on selective laser melting (SLM) parameters and the effects of these parameters on the results of different techniques used to study the behavior of samples.

Texture and Microstructure Evolution in Friction Stir Welded Cu-Al Sheets Characterized by EBSD

2011 ◽  
Vol 702-703 ◽  
pp. 574-577 ◽  
Author(s):  
Daniel Goran ◽  
G. Ji ◽  
M. N. Avettand-Fènoël ◽  
R. Taillard
Keyword(s):  
Microstructure Evolution ◽  
Electron Backscatter Diffraction ◽  
Texture Evolution ◽  
Weld Interface ◽  
Friction Stir ◽  
Electron Backscatter ◽  
Ebsd Technique ◽  
Backscatter Diffraction

Texture and microstructure of FSW joined Al and Cu sheets were investigated by means of electron backscatter diffraction (EBSD) technique. The analysis has revealed a strong texture evolution on both sides of the weld interface as well as a very complex microstructure. Grains were found to be fully recrystallized on both sides of the weld and with different average diameters at different specific zones of the weld.

Study of Texture Evolution of Pure Magnesium during ECAE Using EBSD

2008 ◽  
Vol 584-586 ◽  
pp. 343-348 ◽  
Author(s):  
Somjeet Biswas ◽  
Satyaveer Singh Dhinwal ◽  
Ayan Bhowmik ◽  
Satyam Suwas
Keyword(s):  
Equal Channel Angular Extrusion ◽  
Texture Evolution ◽  
Orientation Distribution ◽  
Fiber Texture ◽  
Electron Back Scatter Diffraction ◽  
Pure Magnesium ◽  
Material Texture ◽  
Two Temperatures ◽  
Ebsd Technique ◽  
Hot Rolled

Commercially Pure Magnesium initially hot rolled and having a basal texture was deformed by Equal Channel Angular Extrusion (ECAE). ECAE was carried out upto 8 passes in a 90° die following routes A and Bc through a processing sequence involving two temperatures, namely 523 and 473 K. Texture and microstructure formed were studied using electron back scatter diffraction (EBSD) technique. In addition to significant reduction in grain size, strong <0002> fiber texture inclined at an angle ~ 45o from the extrusion axis formed in the material. Texture was also analyzed by orientation distribution function (ODF) and compared vis-à-vis shear texture. A significant amount of dynamic recrystallization occurred during ECAE, which apparently did not influence texture.

Measuring Strains for Hematite Phase in Sinter Ore by Electron Backscattering Diffraction Method

2006 ◽  
Vol 326-328 ◽  
pp. 237-240 ◽  
Author(s):  
Yasushi Sasaki ◽  
Manabu Iguchi ◽  
Mitsutaka Hino
Keyword(s):  
Linear Relationship ◽  
Strain Gauge ◽  
Diffraction Method ◽  
Local Strain ◽  
Electron Backscattering ◽  
Hematite Phase ◽  
Compression Strain ◽  
Electron Backscattering Diffraction ◽  
Ebsd Technique ◽  
The Relationship

Based on the relationship between quantified blurring degree of Kikuchi bands obtained by an electron backscattering diffraction (EBSD) technique and macroscopic strains measured by a strain gauge, the local compression strain SEBSD in sinter ore has been evaluated under various conditions. There is a good linear relationship between the SEBSD and the strains measured by a strain gauge. The local strain SEBSD evaluated by EBSD patterns can be used as an index of local strains.

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