In Situ Measurement of the Young’s Modulus of an Embedded Inclusion by Acoustic Microscopy

1997 ◽  
Vol 119 (2) ◽  
pp. 143-147 ◽  
Author(s):  
S. Canumalla ◽  
G. A. Gordon ◽  
R. N. Pangborn
Keyword(s):  
Aluminum Alloy ◽  
Rayleigh Wave ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Target Material ◽  
Acoustic Microscopy ◽  
Alloy Matrix ◽  
Cross Sectional ◽  
Rayleigh Wave Speed

Alumina-silicate inclusions (shot) have been found to adversely affect the mechanical properties of a short alumina-silicate fiber reinforced aluminum alloy (A356). To better understand the differences between the responses of the shot and fibers to applied loads, the Young’s modulus of the shot is measured and compared to that of the fibers. The Rayleigh wave speed in the shot particle (cross-sectional area of 200 μm × 150 μm), measured in situ to be 4041 m/s using a scanning acoustic microscope, was used to calculate the Young’s modulus of the shot particle (132 GPa). The accuracy of the technique and the experimental arrangement used was verified to be better than four percent by independent measurements of the Rayleigh wave speeds in the aluminum alloy matrix and an embedded sapphire fiber. The fiber modulus was estimated to be 225 GPa based on a comparison of previously measured composite modulus with micromechanical predictions. Thus, shot was found to have a Young’s modulus 40 percent lower than that of the fibers. The applicability of the V(z) technique has been demonstrated for measuring the elastic properties over a microscopic area, even when the target material is an embedded inclusion.

scholarly journals Determination of Young’s modulus of Sb2S3 nanowires by in situ resonance and bending methods

2016 ◽  
Vol 7 ◽  
pp. 278-283 ◽  
Author(s):  
Liga Jasulaneca ◽  
Raimonds Meija ◽  
Alexander I Livshits ◽  
Juris Prikulis ◽  
Subhajit Biswas ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Young’S Modulus ◽  
Cross Section ◽  
Young's Modulus ◽  
Cross Sectional ◽  
Bending Tests ◽  
Young’S Moduli ◽  
Increasing Trend

In this study we address the mechanical properties of Sb2S3 nanowires and determine their Young’s modulus using in situ electric-field-induced mechanical resonance and static bending tests on individual Sb2S3 nanowires with cross-sectional areas ranging from 1.1·104 nm2 to 7.8·104 nm2. Mutually orthogonal resonances are observed and their origin explained by asymmetric cross section of nanowires. The results obtained from the two methods are consistent and show that nanowires exhibit Young’s moduli comparable to the value for macroscopic material. An increasing trend of measured values of Young’s modulus is observed for smaller thickness samples.

Mechanical Properties of Pyrolytic "SiOCN" Thin Coatings

1993 ◽  
Vol 308 ◽  
Author(s):  
Sandrine Bec ◽  
André Tonck ◽  
Jean-Luc Loubet
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Ceramic Coatings ◽  
Optical Observation ◽  
Thin Coatings ◽  
Polymer Precursors ◽  
Polymeric State

ABSTRACTPyrolysis of polymer precursors (polysilazane) is a technologically and economically interesting way to produce thin ceramic coatings. However, many cracks appear and decohesion occurs during pyrolysis when the ceramic coatings (SiOCN) are thicker than 0.5 micrometers. In order to understand these cracking phenomena, the coatings are mechanically characterized by nanoindentation at different stages of the pyrolysis heat treatment.During pyrolysis, the cracking temperature is detected by in-situ optical observation. The thickness of the coatings varies during pyrolysis from 3 micrometers at the polymeric state to 1 micrometer at the ceramic state. The coatings' properties, hardness and Young's modulus are evaluated after heat treatment, taking into account the substrate's influence. A large variation of these properties occurs at the cracking temperature. Both the hardness and the Young's modulus are multiplied by a factor of 10. By analysing these results, we show that cracking is correlated with the evolution of the coatings' mechanical properties during the transformation.

scholarly journals Young’s Modulus of Polycrystalline Titania Microspheres Determined by In Situ Nanoindentation and Finite Element Modeling

2014 ◽  
Vol 2014 ◽  
pp. 1-5 ◽  
Author(s):  
Peida Hao ◽  
Yanping Liu ◽  
Yuanming Du ◽  
Yuefei Zhang
Keyword(s):  
Finite Element ◽  
Finite Element Simulation ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Deformation Mechanisms ◽  
Displacement Curve ◽  
Element Simulation ◽  
Nanoindentation Experiment ◽  
Force Displacement

In situ nanoindentation was employed to probe the mechanical properties of individual polycrystalline titania (TiO2) microspheres. The force-displacement curves captured by a hybrid scanning electron microscope/scanning probe microscope (SEM/SPM) system were analyzed based on Hertz’s theory of contact mechanics. However, the deformation mechanisms of the nano/microspheres in the nanoindentation tests are not very clear. Finite element simulation was employed to investigate the deformation of spheres at the nanoscale under the pressure of an AFM tip. Then a revised method for the calculation of Young’s modulus of the microspheres was presented based on the deformation mechanisms of the spheres and Hertz’s theory. Meanwhile, a new force-displacement curve was reproduced by finite element simulation with the new calculation, and it was compared with the curve obtained by the nanoindentation experiment. The results of the comparison show that utilization of this revised model produces more accurate results. The calculated results showed that Young’s modulus of a polycrystalline TiO2microsphere was approximately 30% larger than that of the bulk counterpart.

Effects of cross-sessional area and aspect ratio coupled with orientation on mechanical properties and deformation behavior of Cu nanowires

2021 ◽  
Author(s):  
Hui Cao ◽  
Wenke Chen ◽  
Zhiyuan Rui ◽  
Changfeng Yan
Keyword(s):  
Mechanical Properties ◽  
Aspect Ratio ◽  
Yield Stress ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Cross Sectional Area ◽  
Sectional Area ◽  
Cross Sectional ◽  
Cu Nanowires ◽  
The Cross

Abstract Metal nanomaterials exhibit excellent mechanical properties compared with corresponding bulk materials and have potential applications in various areas. Despite a number of studies of the size effect on Cu nanowires mechanical properties with square cross-sectional, investigations of them in rectangular cross-sectional with various sizes at constant volume are rare, and lack of multifactor coupling effect on mechanical properties and quantitative investigation. In this work, the dependence of mechanical properties and deformation mechanisms of Cu nanowires/nanoplates under tension on cross-sessional area, aspect ratio of cross-sectional coupled with orientation were investigated using molecular dynamics simulations and the semi-empirical expressions related to mechanical properties were proposed. The simulation results show that the Young’s modulus and the yield stress sharply increase with the aspect ratio except for the <110>{110}{001} Cu nanowires/nanoplates at the same cross-sectional area. And the Young’s modulus increases while the yield stress decreases with the cross-sectional area of Cu nanowires. However, both of them increase with the cross-sectional area of Cu nanoplates. Besides, the Young’s modulus increases with the cross-sectional area at all the orientations. The yield stress shows a mildly downward trend except for the <111> Cu nanowires with increased cross-sectional area. For the Cu nanowires with a small cross-sectional area, the surface force increases with the aspect ratio. In contrast, it decreases with the aspect ratio increase at a large cross-sectional area. At the cross-sectional area of 13.068 nm2, the surface force decreases with the aspect ratio of the <110> Cu nanowires while it increases at other orientations. The surface force is a linearly decreasing function of the cross-sectional area at different orientations. Quantitative studies show that Young’s modulus and yield stress to the aspect ratio of the Cu nanowires satisfy exponent relationship. In addition, the main deformation mechanism of Cu nanowires is the nucleation and propagation of partial dislocations while it is the twinning-dominated reorientation for Cu nanoplates.

Parabolic-Apex Numerical Back-Analysis of Mechanics Parameters of Surrounding Rock

2012 ◽  
Vol 204-208 ◽  
pp. 196-201 ◽  
Author(s):  
Jian Cong Xu ◽  
Yi Wei Xu
Keyword(s):  
Young’S Modulus ◽  
Young's Modulus ◽  
Pressure Coefficient ◽  
Back Analysis ◽  
Surrounding Rock ◽  
In Situ Monitoring ◽  
Monitoring Data ◽  
3D Fem ◽  
Physical Mechanics

The parabolic-apex numerical back-analysis method (PNBM) was proposed to obtain such physical-mechanics parameters as Young's modulus and lateral pressure coefficient of surrounding rock by 3D FEM numerical analysis based on in-situ monitoring data. Taking Xiang-an Subsea Tunnel (located in Xiamen, Fujian Province, China) for example, adopting the PNBM using ABAQUS software, three dimensional elastic-plastic FEM-PNBM of tunnel surrounding rock was validated using in-situ monitoring data. The results show as follows: Using the PNBM, not only may high calculation precision be obtained, better meeting the demand of actual projects, but also more reasonable and reliable physical mechanics indices of surrounding rock such as Young's modulus and lateral confinement pressure coefficient, may be obtained. The applicability and the simplicity of this proposed method also support its usefulness.

High Frequency Acoustic Microscopy for the Determination of Porosity and Young’s Modulus in High Burnup Uranium Dioxide Nuclear Fuel

2016 ◽  
Vol 63 (3) ◽  
pp. 1520-1525 ◽  
Author(s):  
Mara Marchetti ◽  
Didier Laux ◽  
Fabiola Cappia ◽  
M. Laurie ◽  
P. Van Uffelen ◽  
...  
Keyword(s):  
Young’S Modulus ◽  
Nuclear Fuel ◽  
Uranium Dioxide ◽  
High Frequency ◽  
Young's Modulus ◽  
Acoustic Microscopy ◽  
High Burnup

scholarly journals Adhesive Joint Stiffness in the Aspect of FEM Modelling

Materials ◽  
2019 ◽  
Vol 12 (23) ◽  
pp. 3911 ◽  
Author(s):  
Anasiewicz ◽  
Kuczmaszewski
Keyword(s):  
Aluminum Alloy ◽  
Numerical Model ◽  
Young’S Modulus ◽  
Adhesive Joint ◽  
Structural Changes ◽  
Young's Modulus ◽  
Joint Stiffness ◽  
Experimental Tests ◽  
Boundary Zone ◽  
Adhesive Properties

The paper presents the results of nanoindentation testing, carried out along the thickness of the adhesive joint joining sheets of aluminum alloy. The purpose of the tests was to determine changes in the Young’s modulus in the joint resulting from the active impact of the joined aluminum alloy sheets on the adhesive during curing of the adhesive bond. Structural changes that take place during curing of the joint, especially in the boundary zone, can have a significant impact on the adhesive properties and consequently, on the adhesive joint strength. The Young’s modulus of the adhesive (Ek) in the joint assumes variable values as the distance from the connections changes. This phenomenon is called the apparent Young’s modulus. The problem is to define the size of the boundary zone in which the value of Ek significantly differs from the value in the so-called core. Based on the obtained results of experimental tests, a numerical model was built taking into account the observed differences in the properties of the joint material. The stress distribution in the adhesive joint, single-lap connection with the three-zone adhesive joint, was analyzed in comparison to the classical numerical model in which adhesive in the adhesive joint is treated as isotropic in terms of rigidity.

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