Improvement in Mechanical Properties of Clay Filled Carbon-Epoxy Composite

2006 ◽  
Author(s):  
Yuanxin Zhou ◽  
Farhana Pervin ◽  
Jamese Hamilton ◽  
Shaik Jeelani
Keyword(s):  
Mechanical Properties ◽  
Epoxy Resin ◽  
High Speed ◽  
High Vacuum ◽  
Test Results ◽  
Trapped Air ◽  
Set Up ◽  
Flexural Tests ◽  
Mechanical Agitator ◽  
Mmt Clay

In the present investigation, a high intensity ultrasonic liquid processor was used to obtain a homogeneous molecular mixture of epoxy resin and K-10 MMT clay. The clay were infused into the part A of SC-15 (Diglycidylether of Bisphenol A) through sonic cavitations and then mixed with part B of SC-15 (cycloaliphatic amine hardener) using a high speed mechanical agitator. The trapped air and reaction volatiles were removed from the mixture using high vacuum. Flexural tests were performed on unfilled, 1wt. %, 2wt. %, 3 wt. % and 4 wt.% clay filled SC-15 epoxy to identify the loading effect on mechanical properties of the composites. The flexural test results indicate that 2.0 wt% loading of clay in epoxy resin showed the highest improvement in strength as compared to the neat systems. After that, the nanophased matrix with 2 wt.% clay is then utilized in a Vacuum Assisted Resin Transfer Molding (VARTM) set up with satin weave carbon preforms to fabricate laminated composites. The resulting structural composites have been tested under flexural and tensile loads to evaluate mechanical properties. 13.5% improvement in flexural strength and 5.8% improvement in tensile strength were observed in carbon/epoxy nanocomposite. TGA and DMA tests were also conducted to observe the thermal stability of the structural composite.

Effect of Nanosized Filler on Matrix Dominated Properties of Fiber Reinforced Epoxy

2011 ◽  
Author(s):  
Yuanxin Zhou ◽  
Shaik Jeelani
Keyword(s):  
Compression Strength ◽  
High Speed ◽  
High Vacuum ◽  
Trapped Air ◽  
Nano Fiber ◽  
Open Hole ◽  
Set Up ◽  
Mechanical Agitator ◽  
Laminar Shear ◽  
Nanosized Filler

In this study, a high-intensity ultrasonic liquid processor was used to obtain a homogeneous molecular mixture of epoxy resin and carbon nano fiber. The carbon nano fibers were infused into the part A of SC-15 (diglycidylether of Bisphenol A) through sonic cavitations and then mixed with part B of SC-15 (cycloaliphatic amine hardener) using a high-speed mechanical agitator. The trapped air and reaction volatiles were removed from the mixture using high vacuum. Nanophased epoxy with 2 wt.% CNF was then utilized in a vacuum assisted resin transfer molding (VARTM) set up with carbon fabric to fabricate laminated composites. The effectiveness of CNF addition on matrix dominated properties of composites has been evaluated by compression, open hole compression and inter-laminar shear. The compression strength, open hole compression strength and ILS were improved by 21%, 23% and 15%, respectively as compared to the neat composite.

Effect of Multiwalled Carbon Nanotube on Compression Properties of Carbon Fiber Reinforced Epoxy

2012 ◽  
Author(s):  
Yuanxin Zhou ◽  
Mahesh Hosur ◽  
Shaik Jeelani
Keyword(s):  
Epoxy Resin ◽  
Compression Strength ◽  
High Speed ◽  
High Vacuum ◽  
Compression Tests ◽  
Multiwalled Carbon ◽  
Compression Properties ◽  
Open Hole ◽  
Set Up ◽  
Mechanical Agitator

In this study, a high-intensity ultrasonic liquid processor was used to obtain a homogeneous mixture of epoxy resin and multi-walled carbon nanotubes (CNTs). The CNTs were infused into epon 862 epoxy resin through sonic cavitation and then mixed with W curing agent using a high-speed mechanical agitator. The trapped air and reaction volatiles were removed from the mixture using a high vacuum. Nanophased epoxy with 0.3 wt.% CNT was utilized in a vacuum assisted resin transfer molding (VARTM) set up with carbon fabric to fabricate laminated composites. The effectiveness of CNT addition on matrix dominated properties of composites has been evaluated by compression and open hole compression tests. The compression strength and open hole compression strength were improved by 31% and 39%, respectively, as compared to the neat composite.

Evaluation of Thermal and Mechanical Properties of Carbon Nano Fiber Reinforced SC-15 Epoxy

Materials ◽  
2005 ◽  
Author(s):  
Farhana Pervin ◽  
Yuanxin Zhou ◽  
Vijay Rangaree ◽  
Shaikh Jelanee
Keyword(s):  
Mechanical Properties ◽  
Epoxy Resin ◽  
High Speed ◽  
Morphological Changes ◽  
High Vacuum ◽  
Thermal And Mechanical Properties ◽  
Entire Volume ◽  
Bending Tests ◽  
Nano Fiber ◽  
Mechanical Agitator

In the present investigation we have developed a novel technique to fabricate nanocomposite materials containing SC-15 epoxy resin and carbon nano fiber (CNF). A high intensity ultrasonic liquid processor was used to obtain a homogeneous molecular mixture of epoxy resin and carbon nano fiber. The carbon nano fibers were infused into the part A of SC-15 (Diglycidylether of Bisphenol A) through sonic cavitations and then mixed with part B of SC-15 (cycloaliphatic amine hardener) using a high speed mechanical agitator. The trapped air and reaction volatiles were removed from the reaction mixture using high vacuum. TGA, DMA and 3-point bending tests were performed on unfilled, 1wt. %, 2wt. % and 4wt. % CNF filled SC-15 epoxy to identify the loading effect on thermal and mechanical properties of the composites. The flexural results indicate that both modulus and strength increased with increasing loading percentage of CNF. DMA studies also revealed that filling the carbon nano fiber into epoxy can improve storage modulus and Tg compared to neat system. However, TGA results show that thermal stability of composite insensitive to the fiber content. The fracture surfaces, dispersions and morphological changes of composites were studied by scanning electron microscope (SEM). These results indicate that the carbon nano fiber is about 200nm in the diameter and 20–100um in the length and are nearly uniformly dispersed over the entire volume of the resin.

Effect of Carbon Nanotube on Electrical, Thermal and Mechanical Properties of Epoxy

2007 ◽  
Author(s):  
Yuanxin Zhou ◽  
Peixuan Wu ◽  
Zhongyang Cheng ◽  
Biddut Kanti Dey ◽  
Shaik Jeelani
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Carbon Nanotube ◽  
High Speed ◽  
Mechanical Test ◽  
High Vacuum ◽  
Mechanical Analysis ◽  
Thermal And Mechanical Properties ◽  
Multi Walled Carbon Nanotubes ◽  
Mechanical Agitator

In this study, electrical, thermal and mechanical properties of multi-walled carbon nanotubes (CNTs) reinforced Epon 862 epoxy have been evaluated. Firstly, 0.1 wt%, 0.2 wt%, 0.3 wt%, and 0.4 wt% CNT were infused into epoxy through a high intensity ultrasonic liquid processor and then mixed with EpiCure curing agent W using a high speed mechanical agitator. The trapped air and reaction volatiles were removed from the mixture using a high vacuum. Neat epoxy sample also was made as reference. Electrical conductivity, dynamic mechanical analysis (DMA, three point bending tests and fracture tests were performed on unfilled, CNT-filled epoxy to identify the loading effect on the properties of composites. Experimental results show significant improvement in electric conductivity. The resistivity of epoxy decreased to 15Ωm with 0.4% CNT. DMA studies revealed that filling the carbon nanotube into epoxy can produce a 90% enhancement in storage modulus and a 17° C increase in Tg, but CNT has little effect on decomposing temperature. Mechanical test results showed that modulus increased with higher CNT loading percentages, but the 0.3 wt% CNT-infusion system showed the maximum strength and fracture toughness enhancement. The decrease in strength and fracture toughness in 0.4% CNT/epoxy was attributed to poor dispersions of nanotubes in the composite.

Mechanichal Properties of DGEBA/TEPA Modified Epoxy Resin

2014 ◽  
Vol 775-776 ◽  
pp. 588-592
Author(s):  
Camila Rodrigues Amaral ◽  
Ruben Jesus Sanchez Rodriguez ◽  
Magno Luiz Tavares Bessa ◽  
Verônica Scarpini Cândido ◽  
Sergio Neves Monteiro
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
Epoxy Resin ◽  
Yield Stress ◽  
Diglycidyl Ether ◽  
Notch Toughness ◽  
Epoxy Network ◽  
Structural Network ◽  
Flexural Tests ◽  
Modified Epoxy

The correlation between the structural network of a diglycidyl ether of the bisphenol-A (DGEBA) epoxy resin, modified by two distinct aliphatic amines (tetraethylenepentamine TEPA and jeffamine D230), and its mechanical properties, was investigated as possible matrix for abrasive composites applications. Both flexural tests, to determine the yield stress and the elastic modulus, as well as impact tests to determine the notch toughness, were performed. The DGEBA/D230 presented the highest stiffness and toughness but lowest yield stress. This epoxy network also displayed a greater plastic deformation during fracture.

Effect of alkali treatment on mechanical properties of jute fiber-reinforced partially biodegradable green composites using epoxy resin matrix

2019 ◽  
Vol 28 (6) ◽  
pp. 388-397
Author(s):  
Jai Inder Preet Singh ◽  
Sehijpal Singh ◽  
Vikas Dhawan
Keyword(s):  
Mechanical Properties ◽  
Epoxy Resin ◽  
Alkali Treatment ◽  
Matrix Material ◽  
Resin Matrix ◽  
Infrared Analysis ◽  
Test Results ◽  
Green Composites ◽  
Jute Fibers ◽  
Naoh Solution

In this work, partially biodegradable green composites have been developed with the help of compression molding technique. Jute fibers were selected as a reinforcement and epoxy resin as matrix material. The influence of alkali treatment on various mechanical properties of jute/epoxy composites was investigated, with concentrations ranging from 1%, 3%, 5%, 7%, and 9% NaOH solution. Various test results indicate that with an increase in concentration, tensile and flexural strength increases up to 5% concentration of NaOH, thereafter both the properties decrease, but impact strength increases up to 7% concentration and thereafter decreases. The results of mechanical characterizations were further validated through the study of morphology with scanning electron microscopy and Fourier transform infrared analysis. The optimal concentration of 5% concentration for alkali treatment of fibers have been suggested.

scholarly journals Improving Ballistic Performance of Polyurethane Foam by Nanoparticle Reinforcement

2009 ◽  
Vol 2009 ◽  
pp. 1-8 ◽  
Author(s):  
M. F. Uddin ◽  
H. Mahfuz ◽  
S. Zainuddin ◽  
S. Jeelani
Keyword(s):  
Energy Absorption ◽  
Polyurethane Foam ◽  
High Speed ◽  
Failure Modes ◽  
High Speed Camera ◽  
Test Results ◽  
Ballistic Performance ◽  
Gas Gun ◽  
Set Up ◽  
Control Samples

We report improving ballistic performance of polyurethane foam by reinforcing it with nanoscaleTiO2particles. Particles were dispersed through a sonic cavitation process and the loading of particles was 3 wt% of the total polymer. Once foams were reinforced, sandwich panels were made and impacted with fragment simulating projectiles (FSPs) in a 1.5-inch gas gun. Projectile speed was set up to have complete penetration of the target in each experiment. Test results have indicated that sandwich with nanophased cores absorbed about 20% more kinetic energy than their neat counterpart. The corresponding increase in ballistic limit was around 12% over the neat control samples. The penetration phenomenon was also monitored using a high-speed camera. Analyses of digital images showed that FSP remained inside the nanophased sandwich for about 7 microseconds longer than that of a neat sandwich demonstrating improved energy absorption capability of the nanoparticle reinforced core. Failure modes for energy absorption have been investigated through a microscope and high-speed images.

Mechanical and Thermal Properties of Carbon-Nanofiber Infused Polyurethane Foam

2008 ◽  
Author(s):  
Md. Atiqur Bhuiyan ◽  
Mahesh V. Hosur ◽  
Yaseen Farooq ◽  
Shaik Jeelani
Keyword(s):  
Mechanical Properties ◽  
Carbon Nanofibers ◽  
Polyurethane Foam ◽  
High Speed ◽  
Carbon Nanofiber ◽  
Mechanical Analysis ◽  
Mechanical And Thermal Properties ◽  
Diphenylmethane Diisocyanate ◽  
Thermal And Mechanical Properties ◽  
Mechanical Agitator

In this study, thermal and mechanical properties of carbon nanofiber infused polyurethane foam were investigated. Low density liquid polyurethane foam composed of Diphenylmethane Diisocyanate (Part A) and Polyol (Part B) was doped with carbon nanofibers (CNF). A high-intensity ultrasonic liquid processor was used to obtain a homogeneous mixture of Diphenylmethane Diisocyanate (Part A) and carbon nanofibers (CNF). The CNF were infused into the Part A of the polyurethane foam through sonic cavitation. The modified foams containing nanoparticles were mixed with Part B (Polyol) using a high-speed mechanical agitator. The mixture was then cast into pre-heated rectangular aluminum molds to form the nano-phased foam panels. Flexure, static and high strain rate compression, and dynamic mechanical analysis (DMA) were performed on neat, 0.2 wt%, 0.4 wt% and 0.6 wt% CNF filled polyurethane foam to identify the effect of adding CNF on the thermal and mechanical properties. The highest improvement on thermal and mechanical properties was obtained with 0.2 wt% loading of CNF. Morphology of the samples was studied through X-ray diffraction.

scholarly journals A novel technique for the assessment of mechanical properties of vascular tissue

2020 ◽  
Vol 19 (5) ◽  
pp. 1585-1594 ◽  
Author(s):  
Stefan N. Sanders ◽  
Richard G. P. Lopata ◽  
Lambert C. A. van Breemen ◽  
Frans N. van de Vosse ◽  
Marcel C. M. Rutten
Keyword(s):  
Mechanical Properties ◽  
Material Properties ◽  
High Speed ◽  
Vascular Tissue ◽  
Plaque Rupture ◽  
Tensile Tests ◽  
Accurate Estimation ◽  
Uniaxial Tensile ◽  
Inflation Experiment ◽  
Set Up

Abstract Accurate estimation of mechanical properties of the different atherosclerotic plaque constituents is important in assessing plaque rupture risk. The aim of this study was to develop an experimental set-up to assess material properties of vascular tissue, while applying physiological loading and being able to capture heterogeneity. To do so, a ring-inflation experimental set-up was developed in which a transverse slice of an artery was loaded in the radial direction, while the displacement was estimated from images recorded by a high-speed video camera. The performance of the set-up was evaluated using seven rubber samples and validated with uniaxial tensile tests. For four healthy porcine carotid arteries, material properties were estimated using ultrasound strain imaging in whole-vessel-inflation experiments and compared to the properties estimated with the ring-inflation experiment. A 1D axisymmetric finite element model was used to estimate the material parameters from the measured pressures and diameters, using a neo-Hookean and Holzapfel–Gasser–Ogden material model for the rubber and porcine samples, respectively. Reproducible results were obtained with the ring-inflation experiment for both rubber and porcine samples. Similar mean stiffness values were found in the ring-inflation and tensile tests for the rubber samples as 202 kPa and 206 kPa, respectively. Comparable results were obtained in vessel-inflation experiments using ultrasound and the proposed ring-inflation experiment. This inflation set-up is suitable for the assessment of material properties of healthy vascular tissue in vitro. It could also be used as part of a method for the assessment of heterogeneous material properties, such as in atherosclerotic plaques.

scholarly journals Mechanical Properties of Polypropylene Warp-Knitted Hernia Repair Mesh with Different Pull Densities

Polymers ◽  
2018 ◽  
Vol 10 (12) ◽  
pp. 1322
Author(s):  
Wanli Xu ◽  
Pibo Ma ◽  
Gaoming Jiang ◽  
Ailan Wan
Keyword(s):  
Mechanical Properties ◽  
Tensile Stress ◽  
High Speed ◽  
Vertical Direction ◽  
Horizontal Stress ◽  
Raw Material ◽  
Knitted Fabrics ◽  
Polypropylene Monofilament ◽  
Set Up ◽  
Warp Knitted Fabric

The medical polypropylene monofilament with a diameter of 0.10 mm was used as the material. Four different pull densities and two different warp run-ins were set up on the electronic traverse high-speed Tricot warp knitting machine, with the gauge of E28. The raw material was used to knit four variations of single bar plain knitted fabrics with 1 in-1 miss setting. Each variation required eight samples. The mechanical properties of the above 32 warp-knitted fabric samples are tested, including their tensile stress (in both vertical and horizontal directions), tearing stress (in both vertical and horizontal directions) and bursting stress. The results obtained shows that the relationship between the vertical, the horizontal stress, and the pull density are not monotonic. The tensile stress in the vertical direction firstly decreases and then increases with an increase of the pull density; however, the tensile stress in the horizontal direction firstly increases and then slightly decreases with an increase of the pull density; again the vertical tensile stress of all fabrics was always higher than the horizontal tensile stress. The bursting stress has a positive linear relation to the pull density. The vertical tearing stresses of four samples were greater than the horizontal tearing stress.

Sign in / Sign up

Export Citation Format

Share Document