An Investigation on Microstructural Evolution of X70 Steel Pipe During Hot Induction Bending

Author(s):  
Moe Meschian ◽  
Andy Duncan ◽  
Matt Yarmuch ◽  
Fred Myschuk

It is generally accepted that hot induction bending (HIB) results in a decrease in strength and an increase in fracture toughness in bend area, heat affected zone (HAZ) and weld metal (WM). As the result, Post bend heat treatment (PBHT) is not considered to be a requirement and could be waived for saving money and time. This research work raises the concern that factual verification of proper microstructure and no localized brittle zone is vitally necessary prior to waving PBHT. Evaluation of the steel microstructure and mechanical properties as the result of various pipe chemistries during pipe bending has been verified in this experimental work. It is emphasized that knowledge and control of prior steel pipe chemistry, control of temperature, cooling rate and bending speed assures the reliability and repeatability of induction bends, especially in critical environments such as low temperature application. In the present work, qualitative and quantitative microstructural analysis, hardness and impact test performed and evaluated on samples from X70 line pipe with 3 different steel chemistries. The samples prepared from different locations on body, weld and HAZ in the as received and as bent condition. It was found that the final microstructure and mechanical properties in the as bent condition is dependent on the chemistry, steel cleanliness and microstructural uniformity. It was observed that small localized brittle zone with traces of upper Bainite and Martensite islands could be transformed in the microstructure with rich chemistry containing non-homogenous central segregation. It is concluded that factual verification of proper microstructure with no localized hard zone is required prior to waving PBHT.

Nanomaterials ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 1024 ◽  
Author(s):  
Milad Haghighi ◽  
Mohammad Shaeri ◽  
Arman Sedghi ◽  
Faramarz Djavanroodi

The effect of graphene nanosheet (GNS) reinforcement on the microstructure and mechanical properties of the titanium matrix composite has been discussed. For this purpose, composites with various GNS contents were prepared by cold pressing and sintering at various time periods. Density calculation by Archimedes’ principle revealed that Ti/GNSs composites with reasonable high density (more than 99.5% of theoretical density) were produced after sintering for 5 h. Microstructural analysis by X-ray diffraction (XRD) and a field emission scanning electron microscope (FESEM) showed that TiC particles were formed in the matrix during the sintering process as a result of a titanium reaction with carbon. Higher GNS content as well as sintering time resulted in an increase in TiC particle size and volume fraction. Microhardness and shear punch tests demonstrated considerable improvement of the specimens’ mechanical properties with the increment of sintering time and GNS content up to 1 wt. %. The microhardness and shear strength of 1 wt. % GNS composites were enhanced from 316 HV and 610 MPa to 613 HV and 754 MPa, respectively, when composites sintered for 5 h. It is worth mentioning that the formation of the agglomerates of unreacted GNSs in 1.5 wt. % GNS composites resulted in a dramatic decrease in mechanical properties.


2010 ◽  
Vol 638-642 ◽  
pp. 3479-3484 ◽  
Author(s):  
Roberta O. Rocha ◽  
Tulio M.F. Melo ◽  
Dagoberto Brandao Santos

The influence of continuous annealing variables on the microstructure and mechanical properties of a C-Mn Dual Phase (DP) steel was studied. The annealing cycles were simulated using a Gleeble machine. Some specimens were quenched at different stages of the annealing cycle in order to evaluate the microstructural evolution during the annealing process. Tensile tests and microstrutural analysis were carried out. The results showed that high heating rates increased the final recrystallization temperature and as a consequence the microstructure obtained was refined. Austenite grain nucleation and growth were also influenced by the heating rates. Soaking temperature was the most influent variable on the mechanical properties, i. e., the yield strength increased and the tensile strength decreased with an increase in the soaking temperature. Microstructural analysis showed that not only martensite, but also bainite and martensite-retained autenite constituent (MA) were formed. Undissolved carbides were also detected by transmission electron microscopy.


2011 ◽  
Vol 674 ◽  
pp. 165-170 ◽  
Author(s):  
Anna Kula ◽  
Ludwik Blaz ◽  
Makoto Sugamata

Rapid solidification (RS) combined with following mechanical consolidation of RS powders is considered as a valuable commercial method for the production of a wide range of metallic materials having fine-grained structures. Reported research results for various alloys demonstrate better compositional homogeneity, smaller grain size and relatively fine precipitates distributed homogenously in RS alloys than that for the materials produced by conventional metallurgical processing. The effect of rapid solidification on the microstructure and mechanical properties of selected Al-Fe-Ni-Mg alloys have been investigated. The basic item of the research work was obtaining aluminum PM materials strengthened by highly-dispersed transition metal compounds and aluminum-magnesium solid solution. Rapid solidification (RS) of Al-4Fe-4Ni and Al-4Fe-4Ni-5Mg alloys was performed by means of gas atomizing of the molten alloy and the spray deposition on the rotating water-cooled copper roll. Using typical powder metallurgy (PM) methods, i.e. cold pressing, vacuum degassing and hot extrusion, the RS-flakes were consolidated to the bulk PMmaterials. For comparison purposes, the conventionally cast and hot extruded Al-4Fe-4Ni and Al-4Fe-4Ni-5Mg alloys were studied as well. Mechanical properties of as-extruded materials were examined by compression tests performed at 293 K – 873 K. It was found that relatively high strength of as-extruded PM materials was accompanied by high ductility of samples deformed by hot compression test. Structural observations confirmed beneficial influence of rapid solidification on effective refining of intermetallic compounds, although some inhomogeneity of fine precipitates distribution was observed. Nevertheless, it was considered that an effective increase of the microhardness and strength of tested RS materials mostly result from achieved dispersion of structural components and can be intensified by solid solution hardening due to Mg-addition.


2013 ◽  
Vol 13 (4) ◽  
pp. 43-48
Author(s):  
E. Guzik ◽  
M. Łagowski ◽  
A. Nowak-Dudek ◽  
B. Niedzielski

Abstract In the scope of existing cooperation with the Foundry of Cast Iron ZM “WSK Rzeszów” Ltd. there was carried out research work of microstructure and mechanical properties in the walls of a cone casting made of ductile cast iron. The particular attention was being put to the search of the potential brittle phases which have deleterious effect on ductility and dynamic properties of highly strained use of the casting prone to the potential risk of cracks during the highly strained use.


Metals ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1414
Author(s):  
Yong Guk Son ◽  
Sung Soo Jung ◽  
Yong Ho Park ◽  
Young Cheol Lee

This study reports the microstructural changes and mechanical properties of high-strength aluminum alloy chips prepared in the semi-solid state at different temperatures, pressures, and holding times. In semi-solid processes, these processing parameters must be optimized because they affect the microstructure and mechanical properties of the chips. In microstructural analysis, these parameters clearly influenced the spheroidization of the aluminum matrix. The aluminum matrix was uniformly spheroidized after semi-solid processing, and the densities of the final samples increased with the holding time. After 30 min holding time at a given temperature, the density approached the theoretical density, but the compressive strength of the samples seriously deteriorated. Meanwhile, fracture surface investigation revealed a deformed Mg2Si phase, which is formed through a eutectic reaction. The strength of this phase significantly decreased after increasing the holding time of the semi-solid processing from 10 to 30 min. Therefore, deformation of the Mg2Si phase caused by diffusion of aluminum into this phase can be a key factor for the decrease in the mechanical properties of samples fabricated with 30 min holding time.


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