Mechanistic Studies on Type 300 Stainless Steels Manufactured by Hot Isostatic Pressing: The Impact of Oxygen Involvement on Fracture Behaviour

Author(s):  
Adam J. Cooper ◽  
Jean Dhers ◽  
Andrew H. Sherry

With near-net shape technology becoming an increasingly desirable route toward component manufacture due to its ability to create components with increasingly complex geometries, minimizing the number of potential welded joints, as well as reducing machining time and associated costs, it is important to demonstrate that components fabricated via Hot Isostatic Pressing (HIP) are able to perform to similar standards as those set by equivalent forged materials. Hot Isostatically Pressed (HIP’d) materials are typically accredited with displaying enhanced yield strengths, ultimate tensile strengths, and ductility over their forged counterparts. In this paper we explore the effects of oxygen, which resides in the austenite matrix during the HIP manufacture process, on a material’s fracture toughness properties. We quantify the influence of different concentrations of oxygen on both the microstructural and mechanical properties of HIP’d 304L and 316L stainless steel, highlighting the benefit of reducing the oxygen as much as possible. Various mechanical tests have been performed on materials containing a range of oxygen contents (between 100 ppm and 200 ppm) and over a large temperature range, including J1C fracture toughness testing, instrumented Charpy, and tensile, and the mechanistic involvement of residual oxygen on the results is discussed. The effects of oxygen become more apparent at cryogenic temperatures, whereas the fracture behavior of HIP’d and forged variants of 304L and 316L at elevated temperatures appears to be comparable.

2021 ◽  
Author(s):  
Karolina E. Mazur ◽  
Aleksandra Borucka ◽  
Paulina Kaczor ◽  
Szymon Gądek ◽  
Stanislaw Kuciel

Abstract In the study, polylactide-based (PLA) composites modified with natural particles (wood, bamboo, and cork) and with different levels of infilling (100%, 80%, and 60%) obtained by additive methods were tested. The effect of type fiber, infill level and crystallization rate on the mechanical properties were investigated by using tensile, flexural, and impact tests. The materials were subjected to mechanical tests carried out at 23 and 80 °C. Furthermore, hydrothermal degradation was performed, and its effect on the properties was analyzed. The addition of natural fillers and different level of infilling result in a similar level of reduction in the properties. Composites made of PLA are more sensitive to high temperature than to water. The decrease in Young's modulus of PLA at 80 °C was 90%, while after 28 days of hydrodegradation ~ 9%. The addition of fibers reduced this decrease at elevated temperatures. Moreover, the impact strength has been improved by 50% for composites with cork particles and for other lignocellulosic composites remained at the same level as for resin.


2016 ◽  
Vol 821 ◽  
pp. 464-470
Author(s):  
Ľubomír Gajdoš ◽  
Martin Šperl

For standard fracture mechanical tests flat specimens (principally CT or SENB) are required. When investigating fracture mechanical properties of thin – walled pipes this brings about a problem because it is necessary to straighten pipe bands. However, this operation causes internal stresses to be induced not only in the semi-product subjected to straightening but also in finished specimens. A question therefore arises to what extent are then the magnitudes of the fracture toughness determined representative for the actual cylindrical wall. To solve this problem fracture mechanics tests were caried out on flat (straightened) CT specimens as well as on curved CT specimens with the natural curvature. The R – curves as well as the resulting parameters of the fracture toughness, obtained for both types of CT specimens, were compared and it was concluded that the fracture toughness of the pipe material determined on straightened CT specimens was practically the same as that obtained on curved CT specimens.


2010 ◽  
Vol 62 ◽  
pp. 197-202
Author(s):  
Hirota Ken ◽  
Takaoka Katsuya ◽  
Murase Yasushi ◽  
Kato Masaki

Synthesis of dense materials with the compositions of Al2O3/Mo2N=100/0 ~ 40/60 vol% has been attempted directly from Al2O3/Mo mixed raw powder compacts using capsule-free N2 hot isostatic pressing (HIP). During HIPing [1500°C/(16~20)MPa]/1h], solid/gas reaction between Mo and N2 was introduced to form Mo2N. Most sintered composites consisting of only Al2O3 and Mo2N phases reached a higher relative density than 98.0% with closed pores nevertheless capsule-free HIPing. Distribution of Mo2N particles just formed suppressed the grain growth of Al2O3 during sintering. Mechanical properties, such as bending strength (Σb), Vickers hardness (HV), fracture toughness (K1C), and other properties have been evaluated as a function of their compositions. The best mechanical values of Σb (c.a. 573 MPa), HV (c.a. 20.3 GPa) and K1C (c.a. 5.00 MPa・m1/2) were attained at the composition of Al2O3/Mo2N=90/10 vol%, due to a high density (98.6%) and small grain size of Al2O3 matrix (Gs c.a. 4.70 μm). Further addition of Mo2N reduced the sinterability of matrix grains, resulting in low densities of around 90% at the 40/60 vol% composition.


Author(s):  
Karolina E. Mazur ◽  
Aleksandra Borucka ◽  
Paulina Kaczor ◽  
Szymon Gądek ◽  
Rafał Bogucki ◽  
...  

AbstractIn the study, polylactide-based (PLA) composites modified with natural particles (wood, bamboo, and cork) and with different levels of infilling (100%, 80%, and 60%) obtained by fused deposition modeling were tested. The effect of fiber type, infill level and crystallization rate on the mechanical properties were investigated by using tensile, flexural, and impact tests. The materials were subjected to mechanical tests carried out at 23 and 80 °C. Differential scanning calorimetry were employed to analyze crystallization behavior of composite. Furthermore, hydrothermal degradation was performed, and its effect on the properties was analyzed. The addition of natural fillers and different levels of infilling result in a similar level of reduction in the properties. However, the addition of natural fillers resulted in a slightly lower drop than the lowered infilling rate − 40% and 50% for tensile strength, respectively. Moreover, it was found that, composites made of PLA are more sensitive to high temperatures than to water. The decrease in Young's modulus of PLA at 80 °C was 90%, while after 28 days of hydrodegradation ~ 9%. The addition of fibers reduced this decrease at elevated temperatures. Importantly, in the case of a brittle material such as PLA, the impact strength has been improved by 50% for composites with cork particles and other lignocellulosic composites remained at the same level as for resin. Generally, the thermal treatment of composites increased the degree of crystallinity of the materials, as reflected in the higher results of mechanical tests.


Materials ◽  
2020 ◽  
Vol 13 (22) ◽  
pp. 5249
Author(s):  
Tadeusz Szymczak ◽  
Katarzyna Makowska ◽  
Zbigniew L. Kowalewski

This paper focuses on the mechanical properties analysis of the high strength S700MC steel applied in welding joints. The research comprised mechanical tests for checking what the changes of tensile characteristics, mechanical parameters, resistance to impact, and fracture toughness look like in selected regions of the welding joint. Stress-strain curves have shown significant differences in the tensile characteristic shape and the values of Young’s modulus, yield stress, ultimate tensile strength, and ductility due to the welding process applied. In the case of Charpy tests, the courses of the accumulated energy, force, deflection, and project velocity are presented, indicating the maximum value of absorbed energy, the same level of force during the first contact of the projectile with the specimens, and the significant variation of the velocity for the impact energy ranging from 50 J up to 300 J. On the basis of the fracture toughness tests, the distributions of the CTOD (Crack Tip Opening Displacement) values are presented for the parent material, HAZ (Heat Affected Zone) and weld. Moreover, the characteristic features of the fatigue pre-crack, transient and crack propagation zones are identified and discussed.


2007 ◽  
Vol 336-338 ◽  
pp. 2300-2303 ◽  
Author(s):  
Martin Trunec ◽  
Karel Maca

Zirconia nanopowders (stabilized by 1.5 and 3 mol% Y2O3) with particle size below 10 nm were compacted by cold isostatic pressing. Pressureless sintering and hot isostatic pressing were applied to obtain dense nanocrystalline ceramics. The influence of the pore size in powder compacts on sintering behaviour was investigated. Green bodies pressed at 1000 MPa had a maximum pore size of 5 nm. These bodies were densified to a relative density of over 99.6% with an average grain size about 85 nm by pressureless sintering at 1100 °C. Indentation techniques were used to evaluate the hardness and fracture toughness of zirconia nanoceramics. The decrease in the yttria content from 3 to 1.5 mol% resulted in the toughness increasing from 5.3 to 11.1 MPa m1/2. The differences in fracture toughness of zirconia ceramics prepared with different yttria contents and by different sintering methods were discussed and their possible causes were proposed.


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