Effect of Incorporating Zirconia Powder into a Primer on the Resin Bond Strength to Zirconia Ceramic

2020 ◽  
Vol 20 (9) ◽  
pp. 5575-5578
Author(s):  
Eunkyung Lee ◽  
Yangho Lee ◽  
Young Kyung Kim ◽  
Chan Ho Park ◽  
Tae-Yub Kwon
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Mean Value ◽  
Zirconia Ceramic ◽  
Test Results ◽  
Zirconia Powder ◽  
Scanning Calorimetry ◽  
The Mean ◽  
Ftir Spectrophotometry

The adhesion property of zirconia powder-incorporated primers was investigated in vitro with the aim of enhancing the resin bond strength to zirconia ceramic. A commercial zirconia primer was modified through the addition of 0 (control), 5, 10, 25, and 50 wt% of a zirconia powder (codes: ZP0, ZP5, ZP10, ZP25, and ZP50, respectively). Prior to primer modification, the powder was characterized via differential scanning calorimetry (DSC) and Fourier-transform infrared (FTIR) spectrophotometry. The surfaces of dental zirconia ceramic discs were air-abraded and treated with one of the five primers. One resin composite cylinder (diameter: 2.38 mm) was bonded on one specimen surface (n = 12/group). The bonded specimens were all stored for 24 h in distilled water at 37 °C and subjected to 5000 thermal cycles prior to shear bond strength (SBS) testing. The DSC and FTIR analyses confirmed that the zirconia powder contained an organic binder. The SBS test results showed that the groups could be arranged as follows, ZP25 > ZP10 > ZP5 > ZP0, i.e., in descending order of the mean value. The lowest SBS value was obtained for the ZP50 group. The results suggest that the incorporation of a zirconia powder into a primer represents a promising modification method for improving the resin bond strength to zirconia ceramic.

scholarly journals Shear bond strength evaluation of bonded molar tubes on fluorotic molars

2012 ◽  
Vol 83 (1) ◽  
pp. 152-157 ◽  
Author(s):  
Erika L. Silva-Benítez ◽  
Veronica Zavala-Alonso ◽  
Gabriel A. Martinez-Castanon ◽  
Juan P. Loyola-Rodriguez ◽  
Nuria Patiño-Marin ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Dental Fluorosis ◽  
In Vitro Study ◽  
Mean Value ◽  
Fixed Appliance ◽  
Adhesive Remnant Index ◽  
The Mean ◽  
Electronic Microscope

Abstract Objective: To study the shear bond strength (SBS), sites of failure, and micromorphology of bonded molar tubes used on teeth affected by dental fluorosis. Materials and Methods: This in vitro study included 140 first molars classified according to Dean's index for dental fluorosis. Samples were divided into seven groups: (1) healthy teeth etched for 15 seconds, (2) teeth with moderate fluorosis (MOF) etched for 15 seconds, (3) teeth with MOF etched for 150 seconds, (4) teeth with MOF microabrasion etched for 15 seconds, (5) teeth with severe fluorosis (SEF) etched for 15 seconds, (6) teeth with SEF etched for 150 seconds, and (7) teeth with SEF microabrasion etched for 15 seconds. All samples were incubated and were then submitted to the SBS test and evaluated with the modified adhesive remnant index (ARI) and analyzed by using a scanning electronic microscope. Results: The SBS mean value for healthy enamel was 20 ± 10.2 MPa. For the group with MOF, the etched 150-second mean value was the highest (19 ± 7.6 MPa); for the group with SEF treated with microabrasion and etched for 15 seconds, the mean value was (13 ± 4.1 MPa). Significant differences (P ≤ .05) were found in the ARI between healthy and fluorosed groups. Conclusions: Fluorotic enamel affects the adhesion of bonded molar tubes. The use of overetching in cases of MOF and the combination of microabrasion and etching in SEF provides a suitable adhesion for fixed appliance therapy.

scholarly journals Repair Bond Strength of Composite to Zirconia Ceramic Using Two Types of Zirconia Primers

2020 ◽  
Author(s):  
Hoseinali Mahgoli ◽  
Mahnaz Arshad ◽  
Kamran Rasouli ◽  
Ali Akbar Sobati ◽  
Ahmad Reza Shamshiri
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Composite Resin ◽  
Zirconia Ceramic ◽  
Adhesive Failure ◽  
Cohesive Failure ◽  
Simultaneous Application ◽  
All Ceramic ◽  
The Mean

  Objectives: This study aimed to assess the effect of application of two types of zirconia primers on repair bond strength of composite to zirconia ceramic. Materials and Methods: In this in vitro, experimental study, 60 zirconia blocks were divided into five groups and subjected to the application of Z-Prime Plus (ZPP), Monobond Plus (MBP), Porcelain Bonding Resin (PBR), ZPP followed by PBR (ZPP+PBR) and MBP followed by PBR (MBP+PBR). They were then bonded to Z100 composite. The samples were then immersed in water at 37°C for 24 hours, thermocycled for 1000 cycles between 5-55°C and subjected to shear bond strength (SBS) test. The mode of failure was determined under a stereomicroscope and a scanning electron microscope (SEM). Results: The mean bond strength was the highest in ZPP+PBR group followed by MBP+PBR, ZPP, PBR and MBP group (22.29±8.86, 15.75±2.81, 12.02±3.24, 3.60±2.92 and 2.92±1.78 MPa, respectively). The effects of type of zirconia primer and use/no use of PBR on SBS were significant (P<0.05). The frequency of adhesive failure in MBP and PBR groups was significantly higher than that in MBP+PBR and ZPP+PBR groups (P<0.05). The cohesive failure was significantly more frequent in ZPP+PBR group than in ZPP, MBP and PBR groups (P<0.05). Conclusion: Simultaneous application of zirconia primer and PBR is the most efficient technique for repair of all-ceramic zirconia restorations with composite resin.

scholarly journals Evaluation of Microshear Bond Strength of Self-Adhesive Versus Conventional Flowable Resin Composite to Sound and Affected Dentin: An In Vitro Study

2021 ◽  
Vol 11 (4) ◽  
pp. 306-312
Author(s):  
Dalia M. Abouelmagd ◽  
Hanan K. Abouelseoud
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
In Vitro Study ◽  
Vitro Study ◽  
Flowable Composite ◽  
Significant Difference ◽  
The Mean ◽  
Microshear Bond Strength ◽  
Vertise Flow

Objectives: This study aimed to compare the microshear bond strength (µSBS) of self-adhesive flowable composite and conventional bonded flowable composite to sound and caries affected dentin. Materials and Methods: In this in vitro study, a total of freshly extracted 40 human molar teeth were used. The occlusal surface was sectioned to expose dentin for µSBS test. The teeth were randomly divided into 2 groups according to the type of flowable composite used into two groups (n=20): group A: self- adhesive flowable composite (Vertise flow), group B: Filtek Z350-XT flowable composite and one-step self-etch adhesive Adper Easy One. A plastic cylindrical mold was used to construct resin composite cylinders (0.8mm diameter x 1mm length) on the sound and caries affected exposed dentin and filled with flowable composite restorative materials according to manufacturer’s instructions. The samples were then immersed in distilled water at 37°C for 24 hours, and underwent µSBS test at a crosshead speed of 0.5 mm/min. Data were analyzed using Student's t-test to compare between the two materials as well as to compare between sound and caries affected dentin. Results: The mean values of µSBS of Filtek Z-350XT to sound and caries affected were 26.6 and 26.7 MPa respectively. The mean µSBS of Vertise Flow to sound and affected were 13.2 and 17.9 MPa respectively. With sound dentin FiltekZ-350XT showed statistically significant higher µSBS than Vertise flow. With caries affected dentin, there was no statistically significant difference between the two materials. There was no statistically significant difference between µSBS of sound and caries affected dentin within each material. The significance level was set at P ≤ 0.05. Conclusions: Within the limitations of this study, the conventional flowable composite yielded the highest µSBS to sound dentin. There was no statistical significant difference in µSBS of self-adhesive and conventional flowable to caries affected dentin. Key words: Composite Resins; Dentin; microshear.

scholarly journals Micro Push-Out Bond Strength of Resin Composite to Dentin in Primary Dentition Using Three Universal Adhesives with Different pH: An In Vitro Study

2021 ◽  
Vol 11 (14) ◽  
pp. 6349
Author(s):  
Regina María Del Río Carrillo ◽  
Pedro Molinero-Mourelle ◽  
Vicente Vera ◽  
Pablo Romero Villaba ◽  
Elizabeth Casañas ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
In Vitro Study ◽  
Primary Dentition ◽  
Vitro Study ◽  
Deciduous Tooth ◽  
Universal Adhesives ◽  
Type Of Failure ◽  
Push Out

To evaluate the bond strength of different universal adhesives on deciduous tooth dentineand their relationship with the composition and potential of hydrogen (pH). Methods: An in vitromicro push-out test on 150 samples (n = 50) per group per adhesive, namely, Adhese Universal(ADH; Ivoclar Vivadent), Futurabond U (FUT; Voco GmbH) (Test), and Scotchbond Universal withpre-conditioning (SCO; 3M) (Control), to record bond strength (BS) and type of adhesive failure.Results: The results of the different adhesives (megapascals (MPa)) varied, showing no statisticalsignificance. The corresponding averages are in MPa: ADH, 13.66 2.81; FUT, 14.48 2.88; SCO,14.98 3.96. Additionally, the frequency of type of failure was as follows: mixed (60.7%), adhesive(27.3%), and cohesive (12%). Conclusions: SCO, with a pH of 2.7, showed greater resistance tofracture, while FUT, with a pH of 2.3 and no pre-conditioning, approached the same values, being aone-step adhesive. No relationship was found between failure and type of adhesive.

scholarly journals Effects of Universal Adhesive on Shear Bond Strength of Resin Cement to Zirconia Ceramic with Different Surface Treatments

2021 ◽  
Vol 2021 ◽  
pp. 1-6
Author(s):  
Zohreh Moradi ◽  
Farnoosh Akbari ◽  
Sara Valizadeh
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
In Vitro Study ◽  
Surface Treatments ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Single Bond ◽  
Universal Adhesive

Aim. This study aimed to assess shear bond strength (SBS) of resin cement to zirconia ceramic with different surface treatments by using Single Bond Universal. Methods. In this in vitro study, 50 zirconia discs (2 × 6 mm) were divided into 5 groups of (I) sandblasting with silica-coated alumina (CoJet)  + silane + Single Bond 2, (II) sandblasting with CoJet + Single Bond Universal, (III) sandblasting with alumina + Single Bond Universal, (IV) sandblasting with alumina + Z-Prime Plus, and (V) Single Bond Universal with no surface treatment. Resin cement was applied in plastic tubes (3 × 5 mm2), and after 10,000 thermal cycles, the SBS was measured by a universal testing machine. The mode of failure was determined under a stereomicroscope at × 40 magnification. Data were analyzed using one-way ANOVA. Results. The maximum (6.56 ± 4.29 MPa) and minimum (1.94 ± 1.96 MPa) SBS values were noted in groups III and I, respectively. Group III had the highest frequency of mixed failure (60%). Group V had the maximum frequency of adhesive failure (100%). Conclusion. Single Bond Universal + sandblasting with alumina or silica-coated alumina particles is an acceptable method to provide a strong SBS between resin cement and zirconia.

scholarly journals COMPARATIVE EVALUATION OF THE SHEAR BOND STRENGTH OF THREE SELF-ETCH DENTIN BONDING AGENTS TO DENTIN: AN IN-VITRO STUDY

2020 ◽  
Vol 8 (10) ◽  
pp. 454-459
Author(s):  
Bhalla V. ◽  
◽  
K. Goud M. ◽  
Chockattu S. ◽  
Khera A ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Testing Machine ◽  
Group Analysis ◽  
In Vitro Study ◽  
Bonding Agents ◽  
Mandibular Molar ◽  
Self Etch

Background:Dentin bonding is an ever-evolving field in adhesive dentistry. With the introduction of newer systems into the market, there is a crucial need to test their efficiency in terms of bond strength. Dual-cured adhesives in theory may provide for a better degree of conversion as compared to conventional light-cured adhesives .Thus, the aim of this study was to compare the shear bond strength of three different self-etch adhesives namely ClearfilSE bond (Kuraray), Tetric N Bond Universal (IvoclarVivadent) and Futura Bond DC (Voco) to dentin. Materials & Methods: Ninety extracted non-carious, intact human mandibular molar teeth were selected for this study. Each tooth was decoronated using a double-sided diamond disc with water coolant to a depth of 2mm from the cusp tip .The cut dentin surface was then abraded against 600-grit wet silicon carbide papers for 60 seconds to produce a uniform smear layer. The root portion of each tooth was mounted on a plastic ring using cold cure acrylic resin. Specimens were then divided into three adhesive groups of 30 teeth each, Group A: ClearfilSE Bond (Kuraray), Group B: Tetric N Bond Universal (IvoclarVivadent), Group C :Futura Bond DC (Voco). All bonding agents were used according to the manufacturers’ instructions, in combination with the resin composite Tetric N Ceram (IvoclarVivadent). The samples were thermocycled, followed by shear bond strength testing using a Universal testing machine (Hounsfield). Data were subjected to statistical analysis using one-way analysis of variance (ANOVA) (P<0.05) and Post hoc Tukey’s test for inter- and intra- group analysis respectively. Results: Clearfil SE Bond yielded the highest shear bond strength values (30.9 ±4.66 MPa) which were statistically significant, followed byTetric N Bond Universal group (29.8 ±4.34) and the lowest shear bond strength values were recorded for Futura Bond DC (18.2 ±3.13). Conclusion: Clearfil SE bond and Tetric N bond Universal can be considered as better options than Futura Bond DC.

scholarly journals Influence of Water Aging on Microtensile Bond Strength of a Flowable and a Packable Bulk-fill Resin Composites to Dentin

2020 ◽  
Vol 8 (D) ◽  
pp. 112-117
Author(s):  
Ayah Atif Selim ◽  
Ahmed Fawzy Abo Elezz ◽  
Rehab Khalil Safy
Keyword(s):  
Bond Strength ◽  
Storage Time ◽  
Resin Composite ◽  
Water Storage ◽  
Aging Effect ◽  
Mean Value ◽  
Control Group ◽  
Microtensile Bond Strength ◽  
Significant Difference ◽  
Influence Of Water

AIM: Investigation of the aging effect on the microtensile bond strength (μTBS) of bulk-fill resin composite (RC) versus a conventionally incrementally applied one. MATERIALS AND METHODS: A total number of 45 sound human impacted third molars extracted molars have been selected to prepare specimens for the μTBS test. Teeth were randomly divided into three groups (C) according to type of RC material which used for restoring the teeth. Where nanohybrid RC (Grandio®SO) was used as the control Group (C1), packable bulk-fill RC (X-tra fil®) was used for restoring teeth in C2 group and flowable bulk-fill RC (X-tra base®) was used for restoring teeth in C3 group. Each group was further subdivided into 3 subgroups (n = 5) according to the water storage time, where in subgroup 1; teeth were stored for 24 h, subgroup 2; teeth were stored for 3 months while for subgroup 3; and teeth were stored for 6 months. After water storage, teeth were sectioned for preparation of μTBS testing beams. Maximum tensile stresses were recorded in megapascal (MPa). RESULTS: After 24 h of water storage, the X-tra base® showed a higher statistically significant μTBS to dentin (33.82 ± 9.84 MPa) than did the other two types of RCs. After 3 months, the X-tra fil® showed the lowest mean value of μTBS (10.90 ± 5.66 MPa), meanwhile, after 6 months of water storage Grandio®SO showed the highest mean value of μTBS (15.85 ± 6.76 MPa). Regardless of the time the X-tra fil® showed the lowest mean of μTBS (15.07 ± 11.73 MPa), while there is no significant difference between the X-tra base® and Grandio®SO. Furthermore, the water aging adversely affects μTBS values which deceased gradually by time. CONCLUSION: The packable bulk-fill RC characterized by lower μTBS to dentin in comparison to the flowable bulk fill and the incrementally applied nanohybrid RCs. Furthermore, the μTBS of the three tested materials decreased gradually by aging.

scholarly journals The Influence of Different Surface Cleansing Agents on Shear Bond Strength of Contaminated Lithium Disilicate Ceramic: An In Vitro Study

2021 ◽  
Vol 2021 ◽  
pp. 1-9
Author(s):  
Taksid Charasseangpaisarn ◽  
Pattarawadee Krassanairawiwong ◽  
Chanidapa Sangkanchanavanich ◽  
Atima Kurjirattikan ◽  
Kanyarak Kunyawatyuwapong ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Sodium Hydroxide Solution ◽  
Resin Composite ◽  
In Vitro Study ◽  
Lithium Disilicate ◽  
Surface Element ◽  
Similar Amount ◽  
Modes Of Failure

Background and Purpose. Contamination of the lithium disilicate (LDS) during the try-in procedure is unavoidable and may weaken the bond strength of restoration. The purpose of this study was to investigate the efficacy of different surface cleansing agents on the shear bond strength (SBS) of contaminated LDS. Materials and Methods. Seventy LDS specimens were randomly divided into seven groups. The first group was noncontaminated surface (PC). The six other groups were contaminated with the saliva and silicone disclosing medium and treated with no surface cleansing agent (NC); phosphoric acid (PO); Ivoclean (IV); sodium hydroxide solution (NA); Restorative Cleansing Agent (RC); and hydrofluoric acid (HF). Then, LDS specimens were cementated with Panavia V5 to resin composite rod. Each specimen was subjected to an SBS test. The modes of failure was inspected under light microscope. The surface element of each group was examined by SEM-EDS. Results. The results were analyzed with one-way ANOVA and Tamhane’s T2. The mean SBS value of NC was significantly lower than others ( p < 0.05 ), and HF was significantly higher than others ( p < 0.05 ). However, PC, PO, IV, NA, and RC were not significantly different from each other ( p > 0.05 ). The mode of failure was mostly adhesive failure in every group. The surface showed similar amount of elements in every group. Conclusions. The SBS of LDS was reduced by saliva and silicone disclosing medium contamination which can be restored using acid- and alkaline-based surface cleansing agents before the cementation procedure.

scholarly journals Antagonism at combined effects of chemical fertilizers and carbamate insecticides on the rice-field N2-fixing cyanobacterium Cylindrospermum sp. in vitro

2014 ◽  
Vol 7 (1) ◽  
pp. 5-11 ◽  
Author(s):  
Rabindra N. Padhy ◽  
Nabakishore Nayak ◽  
Shakti Rath
Keyword(s):  
Mean Value ◽  
Chemical Fertilizers ◽  
Carbamate Insecticides ◽  
Growth Inhibitory ◽  
Progressive Growth ◽  
The Mean ◽  
Growth Promoting ◽  
Reduced Toxicity ◽  
Ppm Level

Abstract Effects of chemical fertilizers (urea, super phosphate and potash) on toxicities of two carbamate insecticides, carbaryl and carbofuran, individually to the N2-fixing cyanobacterium, Cylindrospermum sp. were studied in vitro at partially lethal levels (below highest permissive concentrations) of each insecticide. The average number of vegetative cells between two polar heterocysts was 16.3 in control cultures, while the mean value of filament length increased in the presence of chemical fertilizers, individually. Urea at the 10 ppm level was growth stimulatory and at the 50 ppm level it was growth inhibitory in control cultures, while at 100 ppm it was antagonistic, i.e. toxicity-enhancing along with carbaryl, individually to the cyanobacterium, antagonism was recorded. Urea at 50 ppm had toxicity reducing effect with carbaryl or carbofuran. At 100 and 250 ppm carbofuran levels, 50 ppm urea only had a progressive growth enhancing effect, which was marked well at 250 ppm carbofuran level, a situation of synergism. Super phosphate at the 10 ppm level only was growth promoting in control cultures, but it was antagonistic at its higher levels (50 and 100 ppm) along with both insecticides, individually. Potash (100, 200, 300 and 400 ppm) reduced toxicity due to carbaryl 20 and carbofuran 250 ppm levels, but potash was antagonistic at the other insecticide levels. The data clearly showed that the chemical fertilizers used were antagonistic with both the insecticides during toxicity to Cylindrospermum sp.

scholarly journals Evaluation of Shear-Bond-Strength of Dental Self-Adhering Flowable Resin-Composite versus Total-Etch One to Enamel and Dentin Surfaces: An In-Vitro Study

2019 ◽  
Vol 7 (13) ◽  
pp. 2162-2166 ◽  
Author(s):  
Rasha M. Abdelraouf ◽  
Manar Mohammed ◽  
Fatma Abdelgawad
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Testing Machine ◽  
Tooth Surface ◽  
Mean Values ◽  
Modes Of Failure ◽  
Group I ◽  
Permanent Molars

AIM: This study aimed to assess the shear bond strength of a self-adhering flowable resin composite versus a total-etch one to different surfaces of permanent-molars. MATERIAL AND METHODS: Thirty-six sound human permanent molars were used. The teeth were embedded in acrylic blocks, such that their buccal surfaces were shown. The teeth were divided into three groups: Group I: Uncut-Enamel, Group II: Cut-enamel-surfaces with minimal-grinding and Group III: dentin-surfaces. Half of the teeth in each group were used for bonding to a self-adhering flowable resin-composite (Dyad-flow, Kerr, USA). While the other half of each group was bonded to a total-etch flowable resin-composite (Filtek™Z350-XT,3M-ESPE, USA) which necessitate etching and bonding. Teflon-mold was used for constructing resin composite cylinders (3 × 3 mm) over the buccal surfaces. The Dyad-flow was applied in the central hole of the mould placed upon tooth-surface, and then light-cured for 20 seconds. The Filtek-Z350-XT was applied similarly after etching and bonding steps. The teeth were stored in 37°C distilled water for 24 hours. The strength was measured using a universal testing machine and statistically analysed. Modes of failure were studied using digital-microscope. RESULTS: Mean values of shear bond strength for the Dyad and Filtek-Z350-XT in the uncut-enamel were 3.5 and 24.6MPa respectively, while that for cut-enamel were 4.5 and 12.7MPa respectively (Both highly statistically significant P ≤ 0.01) and in dentin were 4.3 and 6.7MPa respectively (Statistically significant P ≤ 0.05). The failure mode for Dyad was mainly adhesive (un-cut or cut-enamel 83.3% adhesive and 16.7% mixed, while in dentin 100% adhesive). While the modes of failure for Filtek-Z350-XT in enamel, either cut or un-cut, were 50% cohesive and 50% mixed, whereas in dentin 100% adhesive. CONCLUSION: Bonding of self-etch ″Dyad-flow″ flowable resin-composite was lower than the total-etch one in enamel and dentin. Thus further material improvement may be required.

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