Testing Procedures on Materials to Formulate the Ink for 3D Printing

2020 ◽  
Vol 2674 (2) ◽  
pp. 21-32 ◽  
Author(s):  
Malo Charrier ◽  
Claudiane Ouellet-Plamondon
Keyword(s):  
3D Printing ◽  
Yield Stress ◽  
Three Dimensional ◽  
Testing Procedure ◽  
Full Potential ◽  
Cement Pastes ◽  
Slump Test ◽  
Testing Procedures ◽  
Transportation Sector ◽  
Printing Ink

Three-dimensional (3D) printing has been used in various fields to tackle applications difficult for conventional manufacturing. To realize the full potential of this technology in the transportation sector, it is imperative to identify suitable tests and mixtures for printing “inks” made of mortar. In this study, several conventional and non-conventional tests on mortars and cement pastes were conducted. This work highlights the correlation between the results of slump test and the deformation test that indicates the comportment of the mixture under a stack of printed layers. Moreover, a strong connection between yield stress and mini-slump is observed, demonstrating a simplification of the testing procedure, and a link between the mortar and the cement paste is developed. In the printing ink design phase, this association enables the prediction of flowability. The yield stress and the final radius of the mini-slump tests were very well correlated for the admixture tested. The use of the mini-slump test simplifies the testing procedure and allows for quicker formulations of admixtures in the printing ink.

3 D printing technology and experimental study of chitosan gel using atomized solidification liquid-assisted extrusion molding

2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Yangwei Wang ◽  
Peilun Lv ◽  
Jian Li ◽  
Liying Yu ◽  
Guodong Yuan ◽  
...  
Keyword(s):  
3D Printing ◽  
Three Dimensional ◽  
Theoretical Research ◽  
Error Sources ◽  
Printing Technology ◽  
Content Type ◽  
Printing Ink ◽  
Printing Parameters ◽  
Chitosan Gel ◽  
Printing Method

Purpose This paper aims to propose a suitable atomizing solidification chitosan (CS) gel liquid extrusion molding technology for the three dimensional (3D) printing method, and experiments verify the feasibility of this method. Design/methodology/approach This paper mainly uses experimental means, combined with theoretical research. The preparation method, solidification forming method and 3D printing method of CS gel solution were studied. The CS gel printing mechanism and printing error sources are analyzed on the basis of the CS gel ink printing results, printing performance with different ratios of components by constructing a gel print prototype, experiments evaluating the CS gel printing technology and the effects of the process parameters on the scaffold formation. Findings CS printing ink was prepared; the optimal formula was found; the 3 D printing experiment of CS was completed; the optimal printing parameters were obtained; and the reliability of the forming prototype, printing ink and gel printing process was verified, which allowed for the possibility to apply the 3 D printing technology to the manufacturing of a CS gel structure. Originality/value This study can provide theoretical and technical support for the potential application of CS 3 D printed gels in tissue engineering.

scholarly journals Recent Cell Printing Systems for Tissue Engineering

2017 ◽  
Vol 3 (1) ◽  
Author(s):  
Hyeongjin Lee ◽  
YoungWon Koo ◽  
Miji Yeo ◽  
SuHon Kim ◽  
Geun Hyung Kim
Keyword(s):  
Tissue Engineering ◽  
Growth Factors ◽  
3D Printing ◽  
Cell Damage ◽  
Three Dimensional ◽  
Human Tissues ◽  
Printing Process ◽  
Cell Printing ◽  
3D Space ◽  
Printing Ink

 Three-dimensional (3D) printing in tissue engineering has been studied for the bio mimicry of the structures of human tissues and organs. Now it is being applied to 3D cell printing, which can position cells and biomaterials, such as growth factors, at desired positions in the 3D space. However, there are some challenges of 3D cell printing, such as cell damage during the printing process and the inability to produce a porous 3D shape owing to the embedding of cells in the hydrogel-based printing ink, which should be biocompatible, biodegradable, and non-toxic, etc. Therefore, researchers have been studying ways to balance or enhance the post-print cell viability and the print-ability of 3D cell printing technologies by accommodating several mechanical, electrical, and chemical based systems. In this mini-review, several common 3D cell printing methods and their modified applications are introduced for overcoming deficiencies of the cell printing process.

4D Printing of Complex Ceramic Structures via Controlling Zirconia Contents and Patterns

2021 ◽  
Author(s):  
Zhicheng Rong ◽  
Chang Liu ◽  
Yingbin Hu
Keyword(s):  
3D Printing ◽  
Shape Memory ◽  
Shape Change ◽  
Three Dimensional ◽  
Ceramic Materials ◽  
Full Potential ◽  
Sintering Process ◽  
4D Printing ◽  
3D Printed ◽  
Dynamic Components

Abstract In recent years, more and more attentions have been attracted on integrating three-dimensional (3D) printing with fields (such as magnetic field) or innovating new methods to reap the full potential of 3D printing in manufacturing high-quality parts and processing nano-scaled composites. Among all of newly innovated methods, four-dimensional (4D) printing has been proved to be an effective way of creating dynamic components from simple structures. Common feeding materials in 4D printing include shape memory hydrogels, shape memory polymers, and shape memory alloys. However, few attempts have been made on 4D printing of ceramic materials to shape ceramics into intricate structures, owing to ceramics’ inherent brittleness nature. Facing this problem, this investigation aims at filling the gap between 4D printing and fabrication of complex ceramic structures. Inspired by swelling-and-shrinking-induced self-folding, a 4D printing method is innovated to add an additional shape change of ceramic structures by controlling ZrO2 contents and patterns. Experimental results evidenced that by deliberately controlling ZrO2 contents and patterns, 3D-printed ceramic parts would undergo bending and twisting during the sintering process. To demonstrate the capabilities of this method, more complex structures (such as a flower-like structure) were fabricated. In addition, functional parts with magnetic behaviors were 4D-printed by incorporating iron into the PDMS-ZrO2 ink.

scholarly journals Freeform 3D printing of vascularized tissues: Challenges and strategies

2021 ◽  
Vol 12 ◽  
pp. 204173142110572
Author(s):  
Hyun Lee ◽  
Tae-Sik Jang ◽  
Ginam Han ◽  
Hae-Won Kim ◽  
Hyun-Do Jung
Keyword(s):  
3D Printing ◽  
Three Dimensional ◽  
Vascular Networks ◽  
3D Objects ◽  
Advantages And Disadvantages ◽  
Printing Quality ◽  
And Performance ◽  
Material Information ◽  
Printing Ink ◽  
Selection Of

In recent years, freeform three-dimensional (3D) printing has led to significant advances in the fabrication of artificial tissues with vascularized structures. This technique utilizes a supporting matrix that holds the extruded printing ink and ensures shape maintenance of the printed 3D constructs within the prescribed spatial precision. Since the printing nozzle can be translated omnidirectionally within the supporting matrix, freeform 3D printing is potentially applicable for the fabrication of complex 3D objects, incorporating curved, and irregular shaped vascular networks. To optimize freeform 3D printing quality and performance, the rheological properties of the printing ink and supporting matrix, and the material matching between them are of paramount importance. In this review, we shall compare conventional 3D printing and freeform 3D printing technologies for the fabrication of vascular constructs, and critically discuss their working principles and their advantages and disadvantages. We also provide the detailed material information of emerging printing inks and supporting matrices in recent freeform 3D printing studies. The accompanying challenges are further discussed, aiming to guide freeform 3D printing by the effective design and selection of the most appropriate materials/processes for the development of full-scale functional vascularized artificial tissues.

scholarly journals 3D printing of hydrogel composite systems: Recent advances in technology for tissue engineering

2018 ◽  
Vol 4 (1) ◽  
Author(s):  
Tae-Sik Jang ◽  
Hyun-Do Jung ◽  
Houwen Matthew Pan ◽  
Win Tun Han ◽  
Shenyang Chen ◽  
...  
Keyword(s):  
Tissue Engineering ◽  
3D Printing ◽  
Mechanical Performance ◽  
Mechanical Stability ◽  
Three Dimensional ◽  
Hydrogel Composite ◽  
Composite Systems ◽  
Potential Applications ◽  
Hydrogel Composites ◽  
Printing Ink

Three-dimensional (3D) printing of hydrogels is now an attractive area of research due to its capability to fabricate intricate, complex and highly customizable scaffold structures that can support cell adhesion and promote cell infiltration for tissue engineering. However, pure hydrogels alone lack the necessary mechanical stability and are too easily degraded to be used as printing ink. To overcome this problem, significant progress has been made in the 3D printing of hydrogel composites with improved mechanical performance and biofunctionality. Herein, we provide a brief overview of existing hydrogel composite 3D printing techniques including laser based-3D printing, nozzle based-3D printing, and inkjet printer based-3D printing systems. Based on the type of additives, we will discuss four main hydrogel composite systems in this review: polymer- or hydrogel-hydrogel composites, particle-reinforced hydrogel composites, fiber-reinforced hydrogel composites, and anisotropic filler-reinforced hydrogel composites. Additionally, several emerging potential applications of hydrogel composites in the field of tissue engineering and their accompanying challenges are discussed in parallel.

scholarly journals Slump Test: A New Empirical Model for High Yield Stress Materials

2021 ◽  
Vol 11 (2) ◽  
pp. 107-112
Author(s):  
H. Kemer ◽  
R. Bouras ◽  
M. Sonebi ◽  
N. Mesboua ◽  
A. Benmounah
Keyword(s):  
Yield Stress ◽  
Present Model ◽  
High Yield ◽  
Flow Curves ◽  
Cement Pastes ◽  
Slump Test ◽  
High Yield Stress ◽  
Rate Controlled ◽  
Cylindrical Mold ◽  
Plate Geometry

Abstract In order to decrease the fitting deviation between rheometrical measurements and empirical parameters using slump test, this paper proposes a new analytical method to evaluate the high yield stress of materials (cement pastes).In doing so, an experimental study was performed for measuring the empirical characteristics by cylindrical mold with different water to binder ratios (w/b) by aiming to increase the yield stress. Parallelly, experimental observations showed clearly the unyielded zone at flow stoppage of high yield stress samples. Based on these results, an idea was formed to applied metallic element at inlet of mold in order to push the spreading of paste. The obtained results of the model proposed in this paper were compared with the yield stress evaluated from shear flow curves using AR2000-rheometer with plate-plate geometry at rate-controlled. In fact, this study demonstrates the applicability and novelty of the present model in the process of relating the empirical parameters to yield stress.

scholarly journals Binder Jet 3D Printing of Compound LEV-PN Dispersible Tablets: An Innovative Approach for Fabricating Drug Systems with Multicompartmental Structures

Pharmaceutics ◽  
2021 ◽  
Vol 13 (11) ◽  
pp. 1780
Author(s):  
Xiaoxuan Hong ◽  
Xiaolu Han ◽  
Xianfu Li ◽  
Jiale Li ◽  
Zengming Wang ◽  
...  
Keyword(s):  
3D Printing ◽  
Three Dimensional ◽  
Drug Dose ◽  
Solid Dosage Forms ◽  
Precise Control ◽  
Solid Dosage ◽  
Application Potential ◽  
Dispersible Tablets ◽  
Coffee Ring Effect ◽  
Printing Ink

Three-dimensional (3D) printing is an emerging technology that has high application potential for individualized medicines and complex solid dosage forms. This study is designed to explore binder jet 3D printing (BJ-3DP) for the development of high-precision and repeatable compound levetiracetam-pyridoxine hydrochloride (LEV-PN) multicompartmental structure dispersible tablets. PN was dissolved in printing ink directly and accurately jetted into the middle, nested layer of the tablet, and precise control of the drug dose was achieved through the design of printing layers. With modification of the drying method, the “coffee ring” effect caused by drug migration during the curing and molding of the tablets was overcome. Furthermore, 3D topography showed that the tablets have a promising surface morphology. Scanning electron microscopy and porosity results indicated that the tablets have a loose interior and tight exterior, which would ensure good mechanical properties while enabling the tablet to disintegrate quickly in the mouth and achieve rapid release of the two drugs. This study used BJ-3DP technology to prepare personalized multicompartmental structures of drug systems and provides a basis for the development of complex preparations.

scholarly journals Efficacy evaluation of three-dimensional printing assisted osteotomy guide plate in accurate osteotomy of adolescent cubitus varus deformity

2019 ◽  
Vol 14 (1) ◽  
Author(s):  
Yuan-Wei Zhang ◽  
Xin Xiao ◽  
Wen-Cheng Gao ◽  
Yan Xiao ◽  
Su-Li Zhang ◽  
...  
Keyword(s):  
3D Printing ◽  
Blood Loss ◽  
Three Dimensional ◽  
Operation Time ◽  
Varus Deformity ◽  
Conventional Group ◽  
Intraoperative Blood Loss ◽  
Cubitus Varus ◽  
Guide Plate ◽  
Significant Difference

Abstract Background This present study is aimed to retrospectively assess the efficacy of three-dimensional (3D) printing assisted osteotomy guide plate in accurate osteotomy of adolescent cubitus varus deformity. Material and methods Twenty-five patients (15 males and 10 females) with the cubitus varus deformity from June 2014 to December 2017 were included in this study and were enrolled into the conventional group (n = 11) and 3D printing group (n = 14) according to the different surgical approaches. The operation time, intraoperative blood loss, osteotomy degrees, osteotomy end union time, and postoperative complications between the two groups were observed and recorded. Results Compared with the conventional group, the 3D printing group has the advantages of shorter operation time, less intraoperative blood loss, higher rate of excellent correction, and higher rate of the parents’ excellent satisfaction with appearance after deformity correction (P < 0.001, P < 0.001, P = 0.019, P = 0.023). Nevertheless, no significant difference was presented in postoperative carrying angle of the deformed side and total complication rate between the two groups (P = 0.626, P = 0.371). Conclusions The operation assisted by 3D printing osteotomy guide plate to correct the adolescent cubitus varus deformity is feasible and effective, which might be an optional approach to promote the accurate osteotomy and optimize the efficacy.

scholarly journals Three-dimensional(3D) printing in forensic science–An emerging technology in India

2021 ◽  
Vol 1 ◽  
pp. 100006
Author(s):  
Gargi Jani ◽  
Abraham Johnson ◽  
Jeidson Marques ◽  
Ademir Franco
Keyword(s):  
3D Printing ◽  
Forensic Science ◽  
Three Dimensional ◽  
Emerging Technology

scholarly journals Efficient 3D printing via photooxidation of ketocoumarin based photopolymerization

2021 ◽  
Vol 12 (1) ◽  
Author(s):  
Xiaoyu Zhao ◽  
Ye Zhao ◽  
Ming-De Li ◽  
Zhong’an Li ◽  
Haiyan Peng ◽  
...  
Keyword(s):  
Additive Manufacturing ◽  
3D Printing ◽  
Visible Light ◽  
Light Exposure ◽  
Three Dimensional ◽  
3D Printer ◽  
Light Penetration ◽  
Viable Solution

AbstractPhotopolymerization-based three-dimensional (3D) printing can enable customized manufacturing that is difficult to achieve through other traditional means. Nevertheless, it remains challenging to achieve efficient 3D printing due to the compromise between print speed and resolution. Herein, we report an efficient 3D printing approach based on the photooxidation of ketocoumarin that functions as the photosensitizer during photopolymerization, which can simultaneously deliver high print speed (5.1 cm h−1) and high print resolution (23 μm) on a common 3D printer. Mechanistically, the initiating radical and deethylated ketocoumarin are both generated upon visible light exposure, with the former giving rise to rapid photopolymerization and high print speed while the latter ensuring high print resolution by confining the light penetration. By comparison, the printed feature is hard to identify when the ketocoumarin encounters photoreduction due to the increased lateral photopolymerization. The proposed approach here provides a viable solution towards efficient additive manufacturing by controlling the photoreaction of photosensitizers during photopolymerization.

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