scholarly journals EFFECTS OF COOLING RATE ON THE VOLUME FRACTION OF RETAINED AUSTENITE IN FORGINGS FROM HIGH-STRENGTH Mn-Si STEELS

2019 ◽  
Vol 25 (2) ◽  
pp. 93 ◽  
Author(s):  
Dagmar Bublíková ◽  
Hana Jirková ◽  
Kateřina Rubešová ◽  
Michal Peković ◽  
Julie Volkmannová ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Cooling Rate ◽  
Retained Austenite ◽  
Physical Simulation ◽  
Volume Fraction ◽  
High Strength ◽  
Hot Water ◽  
Quenching Temperature ◽  
Soaking Temperature

<p class="AMSmaintext"><span lang="EN-GB">Various ways are sought today to increase mechanical properties of steels while maintaining their good strength and ductility. Besides effective alloying strategies, one method involves preserving a certain amount of retained austenite in a martensitic matrix. The steel which was chosen as an experimental material for this investigation contained 2.5% manganese, 2.09% silicon and 1.34% chromium, with additions of nickel and molybdenum. An actual closed-die forged part was made of this steel. This forged part was fitted with thermocouples attached to its surface and placed in its interior and then treated using the Q&amp;P process. Q&amp;P process is characterized by rapid cooling from a soaking temperature to a quenching temperature, which is between the Ms and the Mf, and subsequent reheating to and holding at a partitioning temperature where retained austenite becomes stable. The quenchant was hot water. Cooling took place in a furnace. Heat treatment profiles were constructed from the thermocouple data and the process was then replicated in a thermomechanical simulator. The specimens obtained in this manner were examined using metallographic techniques. The effects of cooling rate on mechanical properties and the amount of retained austenite were assessed. The resultant ultimate strength was around 2100 MPa. Elongation and the amount of retained austenite were 15% and 17%, respectively. Microstructures and mechanical properties of the specimens were then compared to the real-world forged part in order to establish whether physical simulation could be employed for laboratory-based optimization of heat treatment of forgings.</span></p>

Effects of Heat Treatment on Microstructure of High-Strength Manganese-Silicon Steels

2017 ◽  
Vol 270 ◽  
pp. 239-245
Author(s):  
Dagmar Bublíková ◽  
Štěpán Jeníček ◽  
Kateřina Opatová ◽  
Bohuslav Mašek
Keyword(s):  
Heat Treatment ◽  
Cooling Rate ◽  
Microstructure Evolution ◽  
Retained Austenite ◽  
Volume Fraction ◽  
High Strength ◽  
Quenching And Partitioning ◽  
Alloying Additions ◽  
New Procedures ◽  
Strength And Ductility

Today’s advanced steels are required to possess high strength and ductility. This can be accomplished by producing appropriate microstructures with a certain volume fraction of retained austenite. The resulting microstructure depends on material’s heat treatment and alloying. High ultimate strengths and sufficient elongation levels can be obtained by various methods, including quenching and partitioning (Q&P process). The present paper introduces new procedures aimed at simplifying this process with the use of material-technological modelling. Three experimental steels have been made and cast for this investigation, whose main alloying additions were manganese, silicon, chromium, molybdenum and nickel. The purpose of manganese addition was to depress the Ms and Mf temperatures. The Q&P process was carried out in a thermomechanical simulator for better and easier control. The heat treatment parameters were varied between the sequences and their effect on microstructure evolution was evaluated. They included the cooling rate, partitioning temperature and time at partitioning temperature. Microstructures including martensite with strength levels of more than 2000 MPa and elongation of 10–15 % were obtained.

scholarly journals NEW TREATMENT ROUTE FOR CLOSED-DIE FORGINGS OF STEELS WITH 2.5% MANGANESE

2018 ◽  
Vol 24 (2) ◽  
pp. 119
Author(s):  
Dagmar Bublíková ◽  
Štěpán Jeníček ◽  
Michal Peković ◽  
Hana Jirková
Keyword(s):  
Heat Treatment ◽  
Retained Austenite ◽  
Volume Fraction ◽  
High Strength ◽  
Quenching Temperature ◽  
Treatment Processes ◽  
Martensitic Microstructure ◽  
Heat Treated ◽  
Forged Parts ◽  
New Treatment

<p>The requirements placed on closed-die-forged parts of advanced steels have been increasing recently. Such forgings demand an innovative approach to both design and heat treatment. It is important to obtain high strength and sufficient ductility in closed-die forgings. High strength, mostly associated with martensitic microstructure, is often to the detriment of ductility. Ductility can be improved by incorporating a certain volume fraction of retained austenite in the resulting microstructure. Among heat treatment processes capable of producing martensite and retained austenite, there is the Q&amp;P process (Quenching and Partitioning). This process is characterized by rapid cooling from the soaking temperature to the quenching temperature, which is between Ms and Mf, and subsequent reheating and holding at the partitioning temperature. Thus, strength levels of more than 2000 MPa combined with more than 10% elongation can be obtained. This experimental programme involved steels with 2.5% manganese. Forgings of these steels were heat treated using an innovative process in order to obtain an ultimate strength of more than 2000 MPa combined with sufficient elongation. Thanks to a higher manganese level, the Mf was depressed as low as 78°C, and therefore quenching was carried out not only in air but also in boiling water. Holding at the partitioning temperature of 180°C, when carbon migrates from super-saturated martensite to retained austenite, took place in a furnace. The effects of heat treatment parameters on the resulting mechanical properties and microstructure evolution in various locations of the forging were studied.</p>

Microstructure and Tensile Properties of TRIP-Aided Steel Sheet Subjected to Hot-Rolling and Austempering

2021 ◽  
Vol 1016 ◽  
pp. 732-737
Author(s):  
Junya Kobayashi ◽  
Hiroto Sawayama ◽  
Naoya Kakefuda ◽  
Goroh Itoh ◽  
Shigeru Kuraoto ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Hot Rolling ◽  
Manufacturing Process ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Isothermal Holding ◽  
High Strength ◽  
Isothermal Transformation ◽  
Transformation Process ◽  
Steel Sheets

Various high strength steel sheets for weight reduction and safety improvement of vehicles have been developed. TRIP-aided steel with transformation induced plasticity of the retained austenite has high strength and ductility. Conventional TRIP-aided steels are subjected to austempering process after austenitizing. Generally, elongation and formability of TRIP-aided steel are improved by finely dispersed retained austenite in BCC phase matrix. The finely dispersed retained austenite and grain refinement of TRIP-aided steel can be achieved by hot rolling with heat treatment. Therefore, the improvement of mechanical properties of TRIP-aided steel is expected from the manufacturing process with hot rolling and then isothermal transformation process. In this study, thermomechanical heat treatment is performed by combining hot rolling and isothermal holding as the manufacturing process of TRIP-aided steel sheets. The complex phase matrix is obtained by hot rolling and then isothermal holding. Although the hardness of the hot rolled and isothermal held TRIP-aided steel is decreased, the volume fraction of retained austenite is increased.

Microstructure and Mechanical Properties of a Nb-Microalloyed Medium Carbon Steel Treated by Quenching-Partitioning Process

2012 ◽  
Vol 531-532 ◽  
pp. 596-599
Author(s):  
Kai Zhang ◽  
Shang Wen Lu ◽  
Yao Hui Ou ◽  
Xiao Dong Wang ◽  
Ning Zhong
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Electron Microscope ◽  
Carbon Steel ◽  
Retained Austenite ◽  
High Strength ◽  
Medium Carbon Steel ◽  
Orientation Relationships ◽  
Medium Carbon ◽  
Microstructure And Mechanical Properties

The recently developed “quenching and partitioning” heat treatment and “quenching-partitioning-tempering” heat treatment are novel processing technologies, which are designed for achieving advanced high strength steels (AHSS) with combination of high strength and adequate ductility. In present study, a medium carbon steel containing Nb was subjected to the Q-P-T process, and both the microstructure and mechanical properties was studied. The experimental results show that the Nb-microalloyed steel demonstrates high tensile strength and relatively high elongation. The microstructure of the steel was investigated in terms of scanning electron microscope and transmission electron microscope, and the results indicate that the Q-P-T steel consist of fine martensite laths with dispersive carbide precipitates and the film-like interlath retained austenite. The orientation relationships between martensite and retained austenite is as well-known Kurdjurmov-Sachs relationship and Nishiyama-Wasserman relationship.

scholarly journals High Versatility of Niobium Alloyed AHSS

2017 ◽  
Vol 62 (3) ◽  
pp. 1485-1491 ◽  
Author(s):  
L. Kučerová ◽  
K. Opatová ◽  
J. Káňa ◽  
H. Jirková
Keyword(s):  
Heat Treatment ◽  
Retained Austenite ◽  
Volume Fraction ◽  
High Strength ◽  
Processing Parameters ◽  
High Ductility ◽  
Processing Strategies ◽  
Cooling Schedules ◽  
Final Microstructure ◽  
Steel Processing

AbstractThe effect of processing parameters on the final microstructure and properties of advanced high strength CMnSiNb steel was investigated. Several processing strategies with various numbers of deformation steps and various cooling schedules were carried out, namely heat treatment without deformation, conventional quenching and TRIP steel processing with bainitic hold or continuous cooling. Obtained multiphase microstructures consisted of the mixture of ferrite, bainite, retained austenite and M-A constituent. They possessed ultimate tensile strength in the range of 780-970 MPa with high ductility A5mmabove 30%. Volume fraction of retained austenite was for all the samples around 13%. The only exception was reference quenched sample with the highest strength 1186 MPa, lowest ductility A5mm= 20% and only 4% of retained austenite.

scholarly journals Effect of Quenching and Partitioning Heat Treatment on the Fatigue Behavior of 42SiCr Steel

Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1699
Author(s):  
Marco Thomä ◽  
Guntram Wagner
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Heat Treatment ◽  
Material Properties ◽  
Retained Austenite ◽  
Fatigue Behavior ◽  
High Strength Steels ◽  
High Strength ◽  
Advanced High Strength Steels ◽  
Scanning Electron

The manufacturing of advanced high-strength steels with enhanced ductility is a persistent aim of research. The ability of a material to absorb high loads while showing a high deformation behavior is a major task for many industrial fields like the mobility sector. Therefore, the material properties of advanced high-strength steels are one of the most important impact factors on the resulting cyclic fatigue behavior. To adjust advanced material properties, resulting in high tensile strengths as well as an enhanced ductility, the heat treatment process of quenching and partitioning (QP) was developed. The quenching takes place in a field between martensite start and martensite finish temperature and the subsequent partitioning is executed at slightly elevated temperatures. Regarding the sparsely investigated field of fatigue research on quenched and partitioned steels, the present work investigates the influence of a QP heat treatment on the resulting microstructure by light and scanning electron microscopy as well as on the mechanical properties such as tensile strength and resistance against fatigue regarding two different heat treatment conditions (QP1, QP2) in comparison to the cold-rolled base material of 42SiCr steel. Therefore, the microscopic analysis proved the presence of a characteristic quenched and partitioned microstructure consisting of a martensitic matrix and partial areas of retained austenite, whereas carbides were also present. Differences in the amount of retained austenite could be observed by using X-ray diffraction (XRD) for the different QP routes, which influence the mechanical properties resulting in higher tensile strength of about 2000 MPa for QP1 compared to about 1600 MPa for QP2. Furthermore, the transition for the fatigue limit was approximated by using stepwise load increase tests (LIT) and afterwards verified by constant amplitude tests (CAT) in accordance with the staircase method, whereas the QP 1 condition reached the highest fatigue strength of 900 MPa. Subsequent light and scanning electron microscopy of selected fractured surfaces and runouts showed a different behavior regarding the size of the fatigue fracture area and also differences in the microstructure of these runouts.

Effect of Cooling Rate below Ms Temperature on Hydrogen Embrittlement of TRIP-Aided Martensitic Steels

2021 ◽  
Vol 1016 ◽  
pp. 654-659
Author(s):  
Naoya Kakefuda ◽  
Shintaro Aizawa ◽  
Ryo Sakata ◽  
Junya Kobayashi ◽  
Goroh Itoh ◽  
...  
Keyword(s):  
Hydrogen Embrittlement ◽  
Cooling Rate ◽  
Trip Steel ◽  
Retained Austenite ◽  
Volume Fraction ◽  
High Strength ◽  
Martensitic Steels ◽  
The Matrix ◽  
Embrittlement Resistance ◽  
Hydrogen Embrittlement Resistance

Low alloy TRIP steel is expected to be applied to automobile bodies because of its high strength, high ductility, and excellent impact properties and press formability. It has been reported that the low alloy TRIP steel of hydrogen embrittlement resistance is improved by utilizing the hydrogen storage characteristics of highly stable retained austenite. Therefore, for the purpose of increasing the volume fraction of retained austenite, it was produced at various cooling rates below the martensite transformation start temperature. As a result, the volume fraction of retained austenite increased, and then the effect of hydrogen embrittlement decreased. The matrix phase and retained austenite is refined with decrees of the cooling rate. It is considered that the size and surface area of the retained austenite also affected the improvement of hydrogen embrittlement resistance.

Effect of Heat Treatment on the Properties and Precipitations of High Strength Steel Plate for Construction Machinery

2014 ◽  
Vol 971-973 ◽  
pp. 240-243
Author(s):  
Tao Zhang ◽  
Hua Xing Hou ◽  
Zhao Tan
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
High Strength Steel ◽  
Steel Plate ◽  
High Strength ◽  
Quenching Temperature ◽  
Tempering Temperature ◽  
Construction Machinery ◽  
Microstructure And Mechanical Properties ◽  
Tempering Resistance

The effect of heat treatment on the microstructure and mechanical properties of High Strength steel plate Q960E for construction machinery was investigated. The result shows the quenching temperature have obvious effects on the mechanical properties, DQ can improve the toughness and the enchance tempering resistance, precipitations become more and bigger with the rise of the tempering temperature.

scholarly journals The Effect of Heat Treatment on Microstructure and Mechanical Properties of Cast Bainitic Steel Used for Frogs in Railway Crossovers

2017 ◽  
Vol 62 (4) ◽  
pp. 2147-2151 ◽  
Author(s):  
S. Parzych
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Cast Steel ◽  
Pearlitic Steel ◽  
Strength Properties ◽  
Tensile Yield Strength ◽  
Bainitic Steel ◽  
Microstructure And Mechanical Properties

Abstract This work deals with the effect of heat treatment on a microstructure and mechanical properties of a selected cast steel assigned as a material used for frogs in railway crossovers. Materials used nowadays in the railway industry for frogs e.g. Hadfield cast steel (GX120Mn13) or wrougth pearlitic steel (eg. R260) do not fulfil all exploitation requirements indicated in the UIC (International Union of Railways) Decision No. 1692/96 in terms of train speed that should be reached on railways. One of the possible solution is using a cast steel with bainitic or bainitic-martensitic microstructure that allows to gain high strength properties the ultimate tensile strength (UTS) of 1400 MPa, the tensile yield strength (TYS) of 900 MPa and the hardness of up to 400 BHN. The tested material is considered as an alternative to Hadfield cast steel that is currently used for railway frogs. Results of an experimental analysis of the effect of conducted heat treatment on a microstructure, the volume fraction of retained austenite and mechanical properties of bainitic steel, are shown in this paper. It was found that, the heat treatment leads to a stabilization of retained austenite in grain boundaries area of the primary austenite. Additionally, the heat treatment according to the variant #3 results with an almost 3-times higher impact toughness to that exhibited by material subjected to the other treatments.

scholarly journals The Effects of Micro-Segregation on Isothermal Transformed Nano Bainitic Microstructure and Mechanical Properties in Laser Cladded Coatings

Materials ◽  
2020 ◽  
Vol 13 (13) ◽  
pp. 3017
Author(s):  
Yanbing Guo ◽  
Zhuguo Li ◽  
Liqun Li ◽  
Kai Feng
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Volume Fraction ◽  
High Strength ◽  
Isothermal Heat Treatment ◽  
Isothermal Temperature ◽  
Bainitic Microstructure ◽  
Microstructure Morphology ◽  
Tunable Mechanical Properties ◽  
The Stability

The design of metastable retained austenite is the key issue to obtain nano bainitic steel with high strength and toughness. In this study, nanostructured Fe-based bainitic coatings were fabricated using laser cladding and following isothermal heat treatment. The microstructures and mechanical properties of the laser cladded coating were investigated. The results show that the Mn, Cr, Co, and Al segregated at the solidified prior grain boundaries. The micro-segregation of the solutes strongly influenced the stability of the austenite. As the isothermal temperature decreases, the interface of the bainite and blocky retained austenite approach to the prior interdendritic regions with the decreasing isothermal temperature, and the final volume fraction also decreases. The volume fractions of each phase and microstructure morphology of the coatings were determined by the interdendritic micro-segregation and isothermal temperatures. The stability of the blocky retained austenite distributed at the interdendritic area was lower than that of film and island-like morphology. This phenomenon contributed to the ductile and tough nano bainitic coatings with tunable mechanical properties.

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