scholarly journals Studi Awal Sintesis dan Karakterisasi Bi(Pb)-Sr-Ca-Cu-O dengan Penambahan Carbon Nanotube dan TiO2 Menggunakan Metoda Reaksi Padatan dan Proses Sintering Berulang [Preliminary Study Synthesis and Characterization of Bi(Pb)-Sr-Ca-Cu-O By Addition of Carbon Nanotube and TiO2 Using Solid Reaction Method and Recurrent Sintering Process]

Metalurgi ◽  
2017 ◽  
Vol 32 (3) ◽  
pp. 137 ◽  
Author(s):  
Rizki Syahfina ◽  
Bintoro Siswayanti ◽  
Sigit Dwi Yudanto ◽  
Agung Imaduddin ◽  
Nurul Suhada ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Carbon Nanotube ◽  
Volume Fraction ◽  
Morphological Structure ◽  
Solid State Reaction Method ◽  
Sintering Process ◽  
Reaction Method ◽  
X Ray ◽  
Scanning Electron

Bi1.6Pb0.4Sr2Ca2Cu3O10+δ with the addition of carbon nanotubes (CNT) and TiO2 have been synthesized using solid state reaction method with the repeated sintering process. 0.1 wt % of CNT and 5 wt% of TiO2 have been added to analyze the effect on the synthesizing of 2223 phases. The samples were analyzed using XRD (X-ray diffractometer) and SEM (Scanning Electron Microscopy). Based on the XRD results, 2223 and 2212 were formed. The addition of CNTs and TiO2 reduced the intensity of 2223 phases. This is due to the addition of CNTs and TiO2 as an impurity and prevent the formation of the phases. Also, the repeated sintering process led to the increase of 2223 phase, and the decrease of 2212 phase. However, the repeated sintering process in the B-CNT and B-TiO samples eliminates the impurities phase thus increasing the volume fraction 2223 and decreasing the volume fraction 2212. Based on morphological structure through SEM observation, the addition of CNT in the Bi(Pb)-2223 samples formed longer plates with large porosity spaces while the addition of TiO2 formed clumps on the Bi(Pb)-2223 morphological structure. However, the repeated sintering process improves the morphological structure of B-CNT and B-TiO becomes increasingly denser and the smaller porosity space.AbstrakTelah dilakukan sintesis Bi1,6Pb0,4Sr2Ca2Cu3O10+δ dengan penambahan CNT (carbon nanotube) dan penambahan TiO2 menggunakan metode reaksi padatan dengan proses sintering berulang. Penambahan CNT sebesar 0,1 %berat dan TiO2 sebesar 5 %berat dan sintering berulang dilakukan untuk mempelajari pengaruhnya terhadap pembentukan fasa 2223 beserta pengotornya, dan mempelajari perubahan morfologi Bi1,6Pb0,4Sr2Ca2Cu3O10+δ. Bi1,6Pb0,4Sr2Ca2Cu3O10+δ yang dibuat dianalisis dengan XRD (x-ray diffractometer) dan SEM (scanning electron microscopy). Berdasarkan hasil XRD, penambahan 0,1 %berat CNT dan TiO2 sebesar 5 %berat pada superkonduktor Bi(Pb)-2223 diketahui menghasilkan fasa 2223, fasa 2212, dan juga fasa pengotor. Namun proses sintering berulang mampu mengurangi fasa impuritas, meningkatkan fraksi volume 2223, serta menurunkan fraksi volume 2212.   Berdasarkan pengamatan struktur morfologi melalui SEM, penambahan CNT pada superkonduktor Bi(Pb)-2223 membentuk serpihan memanjang dengan ruang porositas yang besar sedangkan penambahan TiO2 membentuk gumpalan pada struktur morfologi Bi(Pb)-2223. Proses sintering berulang mampu memperbaiki struktur morfologi B-CNT dan B-TiO menjadi semakin rapat dan ruang porositas yang semakin kecil.  

scholarly journals Pengaruh Suhu Sintering Terhadap Sintesis Silicon Carbide (SiC) Berbahan Dasar Abu Sekam Padi dan Grafit Pensil 2B

2015 ◽  
Vol 5 (01) ◽  
pp. 31
Author(s):  
Resky Irfanita ◽  
Asnaeni Ansar ◽  
Ayu Hardianti Pratiwi ◽  
Jasruddin J ◽  
Subaer S
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Silicon Carbide ◽  
Rice Husk Ash ◽  
Sintering Temperature ◽  
Solid State Reaction Method ◽  
X Ray Diffraction ◽  
Reaction Method ◽  
X Ray ◽  
Scanning Electron

The objective of this study is to investigate the effect of sintering temperature on the synthesis of SiC produced from rice husk ash (RHA) and 2B graphite pencils. The SiC was synthesized by using solid state reaction method sintered at temperatures of 750°C, 1000°C and 1200°C for 26 hours, 11.5 hours and 11.5 hours, respectively. The quantity and crystallinity level of SiC phase were measured by means of Rigaku MiniFlexII X-Ray Diffraction (XRD). The microstructure of SiC was examined by using Tescan Vega3SB Scanning Electron Microscopy (SEM). The XRD results showed that the concentration (wt%) of SiC phase increases with the increasing of sintering temperature. SEM results showed that the crystallinity level of SiC crystal is improving as the sintering temperature increases

THE INFLUENCE OF SINTERING AND Sb CONTENT ON THE FORMATION OF HIGH TEMPERATURE SUPERCONDUCTING PHASE IN Bi(Pb)-Sr-Ca-Cu-O SYSTEM

1995 ◽  
Vol 09 (28) ◽  
pp. 3697-3713 ◽  
Author(s):  
S. A. SIDDIQI ◽  
BILQUEES AKHTAR ◽  
A. MAQSOOD
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Solid State Reaction Method ◽  
Superconducting Phase ◽  
Reaction Method ◽  
X Ray ◽  
Sintering Time ◽  
Different Temperatures ◽  
Time Periods ◽  
Scanning Electron

Six different compositions in ( Bi 1.5 Pb 0.5−x Sb x) Sr 2 Ca 2 Cu 3 O y (with x = 0.0, 0.1, 0.2, 0.3, 0.4 and 0.5) have been prepared by the solid state reaction method. Sintering at different temperatures (between 800–860° C) and time periods has been carried out in order to study its effect on T c values. The samples have been characterized by x ray powder diffraction (XRD), Scanning Electron Microscopy (SEM) and measurement of resistance at various temperatures. The study reveals that the incorporation of Sb up to x = 0.2 promotes the formation of a high-T c 2223 phase and large sintering time helps in reducing the number of unwanted phases. Compositions with x ≥ 0.3 result in the formation of a new monoclinic "4441 phase" (along with 2223 and 2212 minor phases) which is non-superconducting down to 77 K. Sintering time at 860°C for samples with x = 0.0, 0.1, 0.2 and 0.3 affects the respective T c values and the maximum values observed are 94 K, 96 K, 100 K and 87 K, respectively. The samples with x = 0.4 and 0.5 do not superconduct up to 77 K.

scholarly journals Investigations of M3Al8O15:Eu3+,Dy3+ (M = Ba, Ca, Mg) phosphors

2016 ◽  
Vol 34 (2) ◽  
pp. 412-417
Author(s):  
Esra Öztürk
Keyword(s):  
Electron Microscopy ◽  
Solid State Reaction Method ◽  
Morphological Characterization ◽  
X Ray Diffraction ◽  
Reaction Method ◽  
X Ray ◽  
Three Samples ◽  
Scanning Electron ◽  
The Eu

AbstractIn this work, aluminate type phosphorescence materials were synthesized via the solid state reaction method and the photoluminescence (PL) properties, including excitation and emission bands, were investigated considering the effect of trace amounts of activator (Eu3+) and co-activator (Dy3+). The estimated thermal behavior of the samples at certain temperatures (> 1000 °C) during heat treatment was characterized by differential thermal analysis (DTA) and thermogravimetry (TG). The possible phase formation was characterized by X-ray diffraction (XRD). The morphological characterization of the samples was performed by scanning electron microscopy (SEM). The PL analysis of three samples showed maximum emission bands at around 610 nm, and additionally near 589 nm, 648 nm and 695 nm. The bands were attributed to typical transitions of the Eu3+ ions.

Light Burning Condition of Preparing Dolomite Clinker Using Natural Dolomite

2018 ◽  
Vol 281 ◽  
pp. 156-162
Author(s):  
Wang Nian Zhang ◽  
Xi Tang Wang ◽  
Zhou Fu Wang
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Grain Size ◽  
Sintering Process ◽  
X Ray Diffraction ◽  
Burning Temperature ◽  
X Ray ◽  
Temperature Range ◽  
Scanning Electron

The influence of the light burning temperature on the sintering property of nature dolomite has been investigated by two-step sintering process in the temperature range 1500 °C to 1600 °C. The resulting bulk densities and apparent porosities of the sintered dolomite samples were examined, and analyzing the sintered dolomite by scanning electron microscopy and X-ray diffraction were performed. The results showed light burned at 850 °C for 3 h, the main phases of the dolomite with 3-5 grain size were MgO, CaO and little CaCO3, and then fired at 1600 °C,the density of sintering dolomite reached to 3.38 g/cm3, the apparent property was 1.2 %, the size of MgO grain up to 3.75 μm . However when dolomite light burned at 1050 °C for 3 h, the main phases were MgO and CaO, and then fired at 1600 °C,the density of sintering dolomite only was 3.30 g/cm3, the apparent property was 2.3 %, the size of MgO only was 3.05 μm .

scholarly journals Double Reinforcement of Al–Fe Intermetallic Composites Fabricated by Friction Stir Processing

Metals ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 1002
Author(s):  
Chunping Huang ◽  
Yang Xia ◽  
Chun Xia ◽  
Fencheng Liu
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Friction Stir Processing ◽  
Volume Fraction ◽  
X Ray Diffraction ◽  
X Ray ◽  
Friction Stir ◽  
Metallurgical Bond ◽  
Aluminum Alloy Surface ◽  
Scanning Electron

A double reinforced layer on an aluminum alloy surface was produced using friction stir processing (FSP) by adding 34CrNiMo6 powder into Al (AA2024) substrate for better wear resistance and gradient transitions. The microstructures of the composites were analyzed using scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The phase composition was examined by X-ray diffraction (XRD). The results show that the double reinforced layer of the Al13Fe4 intermetallic compound could be successfully fabricated via FSP. The volume fraction of Al13Fe4 in the double reinforced layer was higher than in the single reinforced layer due to adding 34CrNiMo6 powder and reinforced twice, and the Al13Fe4 particles were dispersed more homogeneously in the double reinforced layer. The interfaces between the double and single reinforced layer had a good metallurgical bond. The microhardness of the double reinforcement layer was significantly increased. Compared with the AA2024 substrate, the microhardness of the double and single reinforced layers increased five- (576 HV) and two-fold (254 HV), respectively.

Research on Friction and Wear Properties of Ti(C,N)/Fe Composites

2013 ◽  
Vol 650 ◽  
pp. 326-332
Author(s):  
Yang Li ◽  
Zhi Ping Sun ◽  
Rui Feng Wang ◽  
Li Yan Zou
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Friction And Wear ◽  
Adhesive Wear ◽  
Sintering Process ◽  
X Ray Diffraction ◽  
Wear Properties ◽  
X Ray ◽  
Friction And Wear Properties ◽  
Scanning Electron

The effect of different load, revolving speed ,content of Ti(C,N) and sintering process on the friction coefficient and wear rate of Ti(C,N)/Fe composites was investigated systemically. Besides, the wear morphology of Ti(C,N)/Fe composites were researched with an environment scanning electron microscopy(SEM),and the phase composition were studied by X-ray diffraction(XRD).The research shows that the wear mechanism of Ti(C,N)/Fe composites are abrasive wear and adhesive wear.

Microstructures and Textures During Annealing in Low Carbon Al-Killed Steels with Low Finishing Temperatures and High Coiling Temperatures

2011 ◽  
Vol 194-196 ◽  
pp. 52-55 ◽  
Author(s):  
Bao Cai Wu ◽  
Feng Shi ◽  
Xin Yu Cheng ◽  
Rui Min Lin ◽  
Chun Ming Liu
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Optical Microscopy ◽  
Volume Fraction ◽  
Low Carbon ◽  
Coiling Temperature ◽  
X Ray ◽  
Obvious Advantage ◽  
Equiaxed Grain ◽  
Scanning Electron

Microstructures and textures after annealing at 680°C in low carbon Al-killed steels with low finishing temperature and high coiling temperature were investigated by means of optical microscopy (OM), scanning electron microscopy (SEM) and X-Ray Diffractometer (XRD). The results show that higher coiling temperature and lower finishing temperature can both cause the appearance of equiaxed grain and line cementite. The equiaxed grain in 2# steel with higher coiling temperature is the more obvious. Advantage textures are weak in the steels with higher coiling temperature and lower finishing temperature and volume fraction of {111}fiber in 2# steel with higher coiling temperature is only 7.17%, so the stamping property should be worse.

scholarly journals Synthesis Growth and Characterization of Mn doped La1.8Sr0.20CuO4

2011 ◽  
Vol 8 (1) ◽  
pp. 97-100
Author(s):  
Manish Verma ◽  
N. P. Lalla ◽  
D. M. Phase ◽  
V. K. Ahire
Keyword(s):  
Electron Microscopy ◽  
Solid State Reaction Method ◽  
X Ray Diffraction ◽  
Phase Purity ◽  
Reaction Method ◽  
X Ray ◽  
Temperature Method ◽  
Mn Doped ◽  
Scanning Electron

Polycrystalline samples of La1.8Sr0.20Cu1-yMnyO4 (0≤y≤0.15) were synthesized by solid state reaction method. The phase purity was confirmed by powder X-ray diffraction. The scanning electron microscopy was done on the La1.8Sr0.20Cu1-yMnyO4 (0≤y≤0.15) samples. The superconductivity and Transition temperature were studied by four probe resistivity temperature method. The transition temperatures were measured nearly 37 k and were unchanged on Mn doping at Cu site in La1.8Sr0.20CuO4.

scholarly journals Chemical and Wetting Analysis of the Ni-Ti Coating on SiC Improved by a 2-Step Coating-Sintering Process

Materials ◽  
2020 ◽  
Vol 13 (22) ◽  
pp. 5235
Author(s):  
Yang Liu ◽  
Ying-Xin Wang ◽  
Qiang Yang ◽  
Fu Wang
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Sintering Process ◽  
X Ray Diffraction ◽  
Control Groups ◽  
X Ray ◽  
Surface Energies ◽  
Metal Ceramic ◽  
Sintering Conditions ◽  
Scanning Electron

A two-stepped coating-sintering process to prepare the qualified Ni–Ti transition applied in metal-ceramic bonding proved to be effective to improve the wetting abilities. The method was introduced in detail and compared with 2 control groups. To analyze the benefits, the morphology and composition were captured by field emission scanning electron microscopy (FE-SEM), energy dispersive spectroscopy (EDS), and X-ray diffraction (XRD). The comparisons of different coating depths and different sintering conditions were also recorded and analyzed. The influence of the EDS detecting depth was a concern in the discussions. Finally, the contact angle tests and surface energies were also estimated to verify the reliability of the transition layer. The results indicated that the coating-sintering process combined with protective sintering was preferred and necessary to increase the activeness.

scholarly journals Sintesis dan Karakterisasi CNT (Carbon Nanotube) Berdopan Logam Kobalt

2014 ◽  
Vol 17 (3) ◽  
pp. 80-85
Author(s):  
Nur Dwi Lestari ◽  
Pardoyo Pardoyo ◽  
Agus Subagio
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Fourier Transform ◽  
Carbon Nanotube ◽  
Energy Dispersive ◽  
Gas Sorption ◽  
X Ray ◽  
Infra Red ◽  
Ft Ir ◽  
Scanning Electron

Telah dilakukan penelitian sintesis dan karakterisasi CNT (Carbon Nanotube) dengan doping logam kobalt. Penelitian ini bertujuan untuk menentukan karakter CNT sebelum dan setelah didoping dengan variasi konsentrasi logam 10%, 20%, 30%, 40% dan 50%. Metode yang digunakan pada penelitian ini adalah impregnasi basah yang meliputi perendaman pada larutan logam dan kalsinasi. Hasil impregnasi dianalisis menggunakan Fourier Transform-Infra Red (FT-IR), GSA (Gas Sorption Analysis), Scanning Electron Microscopy (SEM) dan Energy Dispersive X-Ray Spectroscopy (EDS). Analisis FT-IR menunjukkan adanya vibrasi ulur dari ikatan Co-C dan Co-O.  Hasil GSA menunjukkan bahwa CNT loading 30% mempunyai luas permukaan tertinggi yaitu 69,192 m2/g. Hasil SEM-EDS menunjukkan bahwa morfologi permukaan dinding CNT ditutupi aggregat-aggregat kobalt. Pada hasil EDS fraksi kobalt dihasilkan adalah 1,96 % yang nilainya tidak jauh berbeda dari fraksi Fe yaitu 1,49%. Hal ini menunjukkan bahwa CNT doping logam Co menggunakan metode impregnasi basah tidak efektif.

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