scholarly journals Synthesis and Characterization of Biodegradable Plastic with Basic Materials of “Singkong Onggok” - Pectin Peel of “Jeruk Bali” (Citrus Maxima) – Plasticizer

2019 ◽  
Vol 2 ◽  
pp. 201-205
Author(s):  
Laelatun Maghfiroh ◽  
Kartini Fauziah Hanum ◽  
Endaruji Sedyadi ◽  
Irwan Nugraha ◽  
Fatchul Anam Nurlaili
Keyword(s):  
Tensile Strength ◽  
Extraction Methods ◽  
Biodegradable Plastics ◽  
Biodegradable Plastic ◽  
Synthesis And Characterization ◽  
Citrus Maxima ◽  
Starch Composition ◽  
Biodegradation Test

Biodegradable plastic made from pectin pell of “jeruk bali” has been carried out. Pectin is obtained by extraction methods and for the manufacture of biodegradable plastics with hot-blending methods. The characteristics of the mechanical biodegradable plastics are determined  by  tensile  strength  and  elongation,  and  biodegradation  test  of  biodegradable  plastics.  The  results  of  manufacture biodegradable plastic with the addition of pectin 5g was the best result with a tensile strength value of 195.35 MPa, and an elongation value of around 15.73 - 33.40%. Plastics with the variation of sorbitol starch composition as much as 1.5 g with 1 ml sorbitol each having a tensile strength of 61.29 MPa and elongation value of 14.30%. Plastic with a variation of 1.5 ml sorb itol has a tensile strength value of 118.93 MPa and an elongation value of 16.73%. Plastic with a variation of 2 ml sorbitol has a tensile strength value of 79.67 MPa and an elongation value of 17.63%.

scholarly journals Pengaruh Penambahan Tepung Tapioka Pada Pati Ubi Kayu (Manihot esculenta) Terhadap Pembuatan Plastik Biodegradable dan Karakterisasinya

2019 ◽  
Vol 2 (2) ◽  
pp. 66-73
Author(s):  
Abdul Rahim ◽  
Rustam Musta
Keyword(s):  
Tensile Strength ◽  
Manihot Esculenta ◽  
Base Material ◽  
Physical And Mechanical Properties ◽  
Biodegradable Plastics ◽  
Cassava Starch ◽  
Biodegradable Plastic ◽  
Percent Elongation ◽  
Tapioca Flour

Research on Biodegradable Plastic Characterization of Cassava Wastes (manihot esculenta) Substitution of Tapioca Flour. As Biodegradable Plastics Base Material. This study aims to determine the ratio of cassava starch to tapioca starch which produces the best biodegradable plastic which is then used for testing the physical and mechanical properties of biodegradable plastic film using 5% acetic acid. Comparison of cassava starch with tapioca flour used is 1 : 1; 1 : 1,5; 1 : 2; 1 : 2,5; 1 : 3. The best plastics are obtained by comparison of cassava starch with tapioca flour is 1 : 3. The characteristics of biodegradable plastics include physical characteristics consisting of thickness with value 0,273 mm, 0,286 mm, 0,413 mm, 0,280 mm, dan 0,510 mm. While the mechanical characteristics consist of tensile strength with value 0,22138 MPa, 2,10724 MPa, 0,78896 MPa, 3,25933 Mpa, dan 0,508 Mpa. Percent lengthening with value 42%, 32,8%, 55,6%, 20%, dan 31,6%. Based on the result of research, it can be concluded that the value of thickness, percent elongation, and tensile strength are influenced by the comparative formula used.Keywords:  Biodegradable plastic, physical properties, mechanics, cassava starch, tapioca flour

scholarly journals The Performance and Characterization of Biodegradable Plastic from Tapioca Starch: Effect of Modified Chitosan

2020 ◽  
Vol 15 (1) ◽  
pp. 45-52
Author(s):  
Lia Ernita ◽  
Medyan Riza ◽  
Syaubari Syaubari
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Water Absorption ◽  
Thin Sheet ◽  
Biodegradable Plastics ◽  
Biodegradable Plastic ◽  
Tapioca Starch ◽  
Modified Chitosan

The performance and characterization of biodegradable plastic from tapioca starch was studied. Modified the chitosan was one of the ingredients for produce  the biodegradable plastics. The produced biodegradable polastic were thin sheet plastic, elastic and transparent. The biodegradable plastic performance had tensile strength between 2,26-3.73 Mpa, elongation ranges from 17.24 to 76.76%, and water absorption ranges from 30.81-268.9%. In antioxidant analyze, apples are wrapped in plastic and had significant mechanical properties changes on 8th day.Morphology scanning result showed that in the chitosan-polyNIPAM there were no cavities may caused high hydrophilicity in the biodegradable plastic.

Synthesis and characterization of new poly(diketone imide)s derived from 1,4-bis(3,4-dicarboxybenzoyl)benzene dianhydride and various diamines

2020 ◽  
Vol 32 (9) ◽  
pp. 1043-1051
Author(s):  
Lu Kuang ◽  
Wei-Hong Wei ◽  
Xiao-Yan Sang ◽  
Yang Pan ◽  
Cheng Song
Keyword(s):  
Mechanical Property ◽  
Tensile Strength ◽  
Ring Opening ◽  
Tensile Modulus ◽  
Amic Acid ◽  
Synthesis And Characterization ◽  
Aromatic Diamines ◽  
Thermal Imidization ◽  
Stage Process

1,4-Bis(3,4-dicarboxybenzoyl)benzene dianhydride, an aromatic bis(ketone anhydride) monomer, was synthesized by the Friedel–Crafts reaction of terephthaloyl dichloride and o-xylene, followed by the oxidation of the intermediate tetramethylated compound and cyclodehydration of the resulting tetraacid. A series of new poly(diketone imide)s (PDKIs) were prepared from this dianhydride with various aromatic diamines via a conventional two-stage process that included ring-opening polyaddition to form the poly(amic acid)s followed by thermal or chemical imidization. Most of the PDKIs through chemical imidization were soluble in aprotic amide solvents, such as N, N-dimethylacetamide, N-methyl-2-pyrrolidone, m-cresol, and so on. The resulting PDKIs had good thermal property with the glass transition temperature of 203–275°C, the temperature at 5% weight loss of 500–539°C, and the residue of 51–60% at 800°C in nitrogen. Additionally, strong and flexible PDKI films obtained by thermal imidization exhibited outstanding mechanical property with the tensile strength of 88.8–158.5 MPa, tensile modulus of 1.9–3.5 GPa, and elongation at breakage of 7–21%.

scholarly journals Synthesis and Characterization of Bioplastic from Chitosan-Ganyong Starch (Canna edulis)

2017 ◽  
Vol 2 (1) ◽  
pp. 13 ◽  
Author(s):  
Agung Nugroho Catur Saputro ◽  
Arruum Linggar Ovita
Keyword(s):  
Tensile Strength ◽  
Group Analysis ◽  
Biodegradable Plastics ◽  
Strength Parameter ◽  
Thickness Swelling ◽  
Process Characterization ◽  
Functional Group Analysis ◽  
Degradation Ability ◽  
Bioplastic Film

<p>The purpose of this study was to produced bioplastic from chitosan-ganyong starch and compare its quality to commercial biodegradable plastic. This research was carried out by experimental method in laboratory. Making bioplastic film was done by dissolving, blending, printing, drying, and neutralizing process. Characterization of bioplastic film was performed by tensile strength test,% elongation, thickness, swelling, solubility, biodegradability and functional group analysis with FTIR. The produced bioplastic characterizations were compared to commercial biodegradable plastics. The results concluded that the qualities of bioplastic chitosan-ganyong starch are  higher than commercial biodegradable plastics on tensile strength parameter (53,9644 Mpa : 18,4109 MPa),% elongation (1,8066 % : 3,7025%), and degradation ability (5 days : 30 days); but lower in thickness parameters (0.0350 mm: 0.0140 mm), % swelling (0.275%: 0.010%), and solubility (0.10%: 0.05%).</p><p><strong> </strong></p><p> </p>

scholarly journals Preparation and Characterization of Conductive Plastics Using Cassava Peel Waste and Addition of CuSO4

2020 ◽  
Vol 2 (1) ◽  
pp. 34-41
Author(s):  
Syahrul Humaidi
Keyword(s):  
Tensile Strength ◽  
Thermal Testing ◽  
Elongation At Break ◽  
Thermal Test ◽  
A Value ◽  
Root Starch ◽  
Starch Composition ◽  
Conductive Plastics ◽  
Cassava Peel

This study investigated the characteristics of a conductive plastic based on root starch and CuSO4 filler. The mixture variation was (95:5)%; (90:10)%; (85:15)%; (80:20)% and (75:25)%. Glycerol is used to change the material as desired (plasticizer) which is called a plasticizer. The method used in the manufacture of this material is melt intercalation. Mechanical testing includes tensile strength (tensile strength) and elongation at break. Thermal testing was done using DTA (Differential Thermal Analysis) and material conductivity testing. The characterization results showed that the optimum starch composition: CuSO4 (75:25)% had a conductivity value of 7.3 x 10-2S.m-1, a thermal test value of 410ºC. The optimum tensile strength value occurs in the composition (80:20)% with a value of 4.606 MPa

scholarly journals Pengaruh Penambahan Carboxymethyl Cellulose Terhadap Karakteristik Bioplastik Dari Pati Ubi Nagara (Ipomoea batatas L.)

2019 ◽  
Vol 7 (1) ◽  
pp. 77-85
Author(s):  
Dahlena Ariyani ◽  
Erni Puryati Ningsih ◽  
Sunardi Sunardi
Keyword(s):  
Tensile Strength ◽  
Carboxymethyl Cellulose ◽  
Ipomoea Batatas ◽  
Water Resistance ◽  
Transmission Rate ◽  
Synthesis And Characterization ◽  
Water Vapor Transmission Rate ◽  
Sweet Potatoes ◽  
Water Vapor Transmission

Synthesis and characterization of bioplastics from Nagara sweet potatoes (Ipomoea batatas L) starch with carboxymethyl cellulose (CMC) as a filler has been conducted. The purpose of this study was to evaluate the effects of CMC addition on the characteristic of bioplastics from Nagara sweet potato (Ipomoea batatas L) starch. Bioplastic synthesis was carried out by the melt intercalation method with variations in the amount of CMC 0-30% (w/w). Bioplastics were analyzed using FTIR spectrophotometer, thickness, solubility, water resistance, water vapor transmission rate, tensile strength and elongation. The values of the tensile strength of the bioplastic produced increases with increasing of CMC. The results also showed that the optimum CMC concentration in bioplastics production is 9% (w/w) with a tensile strength value 0.5281 N/mm2.

scholarly journals Synthesis and Characterization of Polysulfone (PSU)/Philippine Halloysite (PH-HAL) Nanostructured Membrane via Electrospinning

2018 ◽  
Vol 213 ◽  
pp. 03001 ◽  
Author(s):  
Ruth R. Aquino ◽  
Marvin S. Tolentino ◽  
Niel Karl G. Arcamo ◽  
John Patrick N. Gara ◽  
Blessie A. Basilia
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Fibrous Composite ◽  
Polymeric Materials ◽  
Composite Membranes ◽  
Electrospinning Process ◽  
Synthesis And Characterization ◽  
Separation Processes ◽  
Wide Range

Membrane technology is widely used in many separation processes because of its multi-disciplinary characteristics. One of the techniques that is used in the fabrication of membranes is the electrospinning process which can create nanofibers from a very wide range of polymeric materials. In this study, electrospun nanostructured fibrous composite membranes of polysulfone (PSU), commercial halloysite (COM-HAL), and Philippine halloysite (PH-HAL) were synthesized. The concentrations of COM-HAL and PH-HAL were both varied from 0.5%, 1%, and 2%. The FTIR results showed that there were changes in the intensity of the PSU-IR spectra which confirmed the presence of COM-HAL and PH-HAL in the synthesized membranes. The SEM revealed that nanofibers can be successfully produced by the addition of LiCl salt in PSU with varying HAL concentrations. Also, it was observed that the addition of HAL with varying concentrations have no significant effect on wettability due to the strong hydrophobic character of the PSU membrane. Moreover, it was found from the analysis of mechanical properties that the tensile strength of the membranes weakened by the addition of HAL due to its weak interaction with PSU.

Synthesis and Characterization of Biodegradable Starch-Based Bioplastics

2016 ◽  
Vol 846 ◽  
pp. 673-678 ◽  
Author(s):  
Nurul Aina Ismail ◽  
Syuhada Mohd Tahir ◽  
Yahya Norihan ◽  
Muhamad Firdaus Abdul Wahid ◽  
Nur Ezzati Khairuddin ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Synthesis And Characterization ◽  
Mechanical And Thermal Properties ◽  
Thermal And Mechanical Properties ◽  
Suitable Alternative ◽  
Soil Burial Test ◽  
Soil Burial ◽  
Starch Potato

This study was carried out to evaluate the potential of plastic synthesized using bio-based starch. The method began with extraction of starch from chosen tubers with high content of starch; potato and yam. The samples were first grated, grinded and strained to obtain crude starch, which then centrifuged and rinsed to get pure starch. The starch was then reacted with hydrochloric acid to breakdown amylopectin to prevent the starch from becoming plastic-like. Finally, propan-1,2,3-triol was added as a plasticizer to increase the elasticity of the product. The chemical, mechanical, and thermal properties of the products were analyzed using Fourier transform infrared (FTIR), tensile strength tester and Thermogravimetric analysis (TGA). The FTIR spectra of the product displayed the presence of O-H, C-H, C=O and C-O absorption peaks, which indicate the formation of bioplastic has already occured. The tensile strength obtained for potato and yam starch-based bioplastic are 0.6 MPa and 1.9 MPa, respectively. The result gained from TGA showed that 50% weight loss occurred at 250°C for potato and 310°C for yam-based plastic. The highly biodegradability of the plastic was proven using soil burial test, which observed the percentage of soil biodegradation for potato and yam-based bioplastic in 1 week duration is 43% and 26%, respectively. These bio-based plastics have exhibited good thermal and mechanical properties with high biodegradability that makes them a suitable alternative for the existing conventional plastics.

Synthesis and Characterization of Biodegradable Aliphatic-Aromatic Copolyesters Nanocomposites Containing POSS

2011 ◽  
Vol 236-238 ◽  
pp. 2028-2031
Author(s):  
Bing Tao Wang ◽  
Yan Zhang ◽  
Zheng Ping Fang
Keyword(s):  
Tensile Strength ◽  
Terephthalic Acid ◽  
Interfacial Adhesion ◽  
Synthesis And Characterization ◽  
Mechanical And Thermal Properties ◽  
Polyhedral Oligomeric Silsesquioxanes ◽  
Elongation At Break ◽  
The Matrix

Biodegradable aliphatic-aromatic copolyesters/POSS nanocomposites were synthesized via in situ melt copolycondensation of terephthalic acid (TPA), poly(L-lactic acid) oligomer (OLLA), 1,4-butanediol (BDO) and polyhedral oligomeric silsesquioxanes (POSS) reagents (POSS-NH2 and POSS-PEG). The morphologies and dispersions of two POSS reagents in the nanocomposites and their effects on the mechanical and thermal properties were investigated. TEM and XRD characterizations confirmed that POSS-NH2 formed crystalline microaggregates and took poor dispersions in the nanocomposite, while POSS-PEG had better dispersion in the matrix. Due to the good dispersion and interfacial adhesion of POSS-PEG with the copolyester PBTL matrix, the tensile strength and the Young’s modulus greatly increased for PBTL/POSS-PEG nanocomposite. Moreover, compared with POSS-NH2 the existence of POSS-PEG imparted PBTL good flexibility and increased the mobility of the chains, so the glass-transition temperature and the heat of melting as well as the elongation at break were obviously influenced for PBTL/POSS-PEG nanocomposite.

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