scholarly journals A new methodological approach (QEMSCAN®) in the mineralogical study of Polish loess: Guidelines for further research

2020 ◽  
Vol 12 (1) ◽  
pp. 342-353
Author(s):  
Piotr Kenis ◽  
Jacek Skurzyński ◽  
Zdzisław Jary ◽  
Rafał Kubik

AbstractThis article presents in detail the methodology dedicated strictly to loess mineralogical investigation by automated mineralogy system QEMSCAN® (quantitative evaluation of minerals by scanning electron microscopy (SEM)), which couples SEM and energy dispersive X-ray spectrometry to automatically deliver mineral and phase mapping. The present study provides guidelines for further loess investigation in Poland, in order to maintain the complete comparability of results which will be obtained. The methodology is then used to obtain the data on complex mineralogical composition (heavy, light, transparent and opaque phases). In total 1,159,107 particles have been measured for five bulk loess samples and 4–6% of them were heavy minerals (c.a. 10,000 per sample). The bulk samples are dominated by quartz (57.3–62.9%) and contain plagioclase (7.8–9.2%), K-feldspar (7.9–8.7%), carbonates (5.0–7.8%), muscovite (3.2–6.2%), biotite (4.2–7.5%), heavy minerals (4.3–5.8%) and clay minerals (0.9–1.6%). The heavy minerals (as a group recalculated to 100%) are mainly represented by phases such as clinopyroxene (38–51%), garnets (14–21%), TiO2 polymorphs (8–12%), Al2SiO5 polymorphs (3–7%), ilmenite (3–6%), iron oxides, e.g., hematite and magnetite (2–5%) and zircon (∼2%). Nearly 50% of the heavy minerals is classified in the 16–31 µm fraction, which determine the changes in the current research procedure traditionally used for Polish loess.

2017 ◽  
Vol 13 (15) ◽  
pp. 195
Author(s):  
Boukhir Mohammed ◽  
Chaouni Abdel-Ali ◽  
Lahrach Abderrahim

The mineralogical investigation of sand fraction of different sectors of filling of Montgaudier deposit revealed that heavy minerals are mainly composed of amphiboles and disthene in all analyzed samples. The other mineralogical species encountered appear having only a secondary role in the composition of heavy mineral processions. These minerals are: Andalusite, brookite, chlorite, epidote, garnet, pyroxene, rutile, sillimanite and sphene. The opaque minerals are relatively numerous in all the studied samples which they are in different stages of alteration, associated with other minerals presenting a fresh appearance. The light minerals consist mainly of hyaline or translucent quartz grains and milky or opalescent grains. The study of clay minerals generally showed a predominance of kaolinite in all sectors, followed by illite and chlorite. Smectite comes in only fourth place. This cortege is complemented by interstratified smectite-chlorite, which are very poorly represented. The mineralogical study of the deposits at the different parts of the layers filling of the Montgaudier deposit and the sediments in the immediate vicinity permitted to determine the origin of these deposits. Their procession is largely influenced by the geological nature of the Tardoire watershed but also of the mineralogical composition of the surrounding rock in which this cave was.


Minerals ◽  
2020 ◽  
Vol 10 (6) ◽  
pp. 509
Author(s):  
Pura Alfonso ◽  
Sarbast Ahmad Hamid ◽  
Hernan Anticoi ◽  
Maite Garcia-Valles ◽  
Josep Oliva ◽  
...  

The strategic importance of tantalum and its scarcity in Europe makes its recovery from low grade deposits and tailings interesting. In Penouta, the contents of Ta and Sn in old tailings from an Sn mine are of economic interest. Due to the relatively low grade of Ta of around 100 ppm, a detailed study of the mineralogy and liberation conditions is necessary. In this study, the mineralogy and the liberation characteristics of Sn and Ta ores of the Penouta tailings were investigated and compared with the current leucogranite outcropping ores. The characterization was conducted through X-ray diffraction, scanning electron microscopy, and electron microprobe. In addition, automated mineralogy techniques were used to determine the mineral associations and liberation characteristics of ore minerals. The grade of the leucogranite outcropping was found to be about 80 ppm for Ta and 400 ppm for Sn, and in the tailings used for the liberation study, the concentrations of Ta and Sn were about 100 ppm Ta and 500 ppm Sn, respectively. In both, the leucogranite outcropping and tailings, the major minerals found were quartz, albite, K-feldspar, and white mica. Ore minerals identified were columbite-group minerals (CGM), microlite, and cassiterite. The majority of CGM examined were associated with cassiterite, quartz, and muscovite particle compositions and cassiterite was mainly associated with CGM, quartz, and muscovite. The liberation size was 180 µm for CGM.


Heritage ◽  
2020 ◽  
Vol 3 (4) ◽  
pp. 1109-1123
Author(s):  
Elena Marrocchino ◽  
Chiara Telloli ◽  
Martina Pedrini ◽  
Carmela Vaccaro

Ancient buildings are important components of the Italian Cultural Heritage and, since the Etruscan Period, Bologna (north-eastern Italy) has always been one of the most flourishing cities both culturally and economically in the Italian and European panorama. The Orsi-Marconi Palace in Bologna presents a monumental façade decorated with many sandstone ornaments of the 16th century. Different samples from different parts of the façade of the building were collected and firstly characterised by macroscopic observations to determine the structural aspect. A petro-mineralogical study on the surfaces of the samples was conducted using a stereomicroscope and Optical Transmitted Light Polarized Microscopy. In addition, X-Ray Fluorescence and X-Ray Powder Diffractometer analyses were carried out to better understand the mineralogical composition of the sandstone materials used and the degradation products from the façades of this historical building. The aim of this work was to better understand how to revalue the sandstone decorations severely affected by deterioration phenomena.


2000 ◽  
Vol 15 (1) ◽  
pp. 51-55 ◽  
Author(s):  
A. Bentayeb ◽  
O. Masson ◽  
Y. Noack ◽  
A. Yacoubi ◽  
A. Nadiri

A chemical and mineralogical investigation of a Moroccan pyrophyllite is presented. X-ray powder diffraction has been largely used for phase identification and crystal symmetry determination. It is shown that this mineral has a triclinic symmetry with cell parameters: a=5.160 Å, b=8.993 Å, c=9.360 Å, α=90.77°, β=100.57°, and γ=89.71°.


2014 ◽  
Vol 5 (1) ◽  
Author(s):  
Gordana Оstojić ◽  
Dragica Lazić ◽  
Branko Škundrić ◽  
Jelena Penavin Škundrić ◽  
Slavica Sladojević ◽  
...  

From the aspect of their chemical and mineralogical composition, bauxites are very complex multicomponent raw materials. The paper presents the characterization of bauxite from several different deposits: Brazil, Milići, Čitluk and Kosovo. Chemical characteristics were determined by a combination of different analytical methods: gravimetry, potentiometric titration, atomic absorption spectroscopy (AAS) and UV-VIS spectrophotometry. Mineralogical composition was determined using X-ray diffraction and thermal analysis methods. Chemical and structural characterization is complemented by the results of scanning electron microscopy with EDX analysis. The information obtained was used for the assessment of the quality of investigated bauxites from the aspect of their application in the production of alumina.


2014 ◽  
Vol 685 ◽  
pp. 37-42
Author(s):  
Jie Liu ◽  
Ming Shun Zhou ◽  
Li Wei Zhai ◽  
Hui Zhang ◽  
Li Bing Xu

In order to improve the qualities of sinter of Ansteel, the sinter’s metallurgical property was examined and analyzed that from the second workshop and the fourth workshop of ironmaking plant. And mineralogical composition and microstructure in high basicities sinter were investigated and analyzed by the X-ray diffraction, the optical microscope and the scanning electron microscope in laboratory. It was found that the differences between in sinter’s mineralogical composition and microstructures are according with the differences in chemical composition and the metallurgical indexes. Both the sinter’s minerals are mainly composed of hematite, magnetite or maghemite, calcium ferrite, dicalcium silicate, silicate glass phase. The content of the carbon in the fourth workshop is higher. So, it should decrease the content of the carbon that makes the microstructure of the sinter more rational.


2018 ◽  
Vol 24 (5) ◽  
pp. 461-470 ◽  
Author(s):  
Orkun Furat ◽  
Thomas Leißner ◽  
Ralf Ditscherlein ◽  
Ondřej Šedivý ◽  
Matthias Weber ◽  
...  

AbstractIn this paper, three-dimensional (3D) image data of ore particle systems is investigated. By combining X-ray microtomography with scanning electron microscope (SEM)-based image analysis, additional information about the mineralogical composition from certain planar sections can be gained. For the analysis of tomographic images of particle systems the extraction of single particles is essential. This is performed with a marker-based watershed algorithm and a post-processing step utilizing a neural network to reduce oversegmentation. The results are validated by comparing the 3D particle-wise segmentation empirically with 2D SEM images, which have been obtained with a different imaging process and segmentation algorithm. Finally, a stereological application is shown, in which planar SEM images are embedded into the tomographic 3D image. This allows the estimation of local X-ray attenuation coefficients, which are material-specific quantities, in the entire tomographic image.


1959 ◽  
Vol 39 (2) ◽  
pp. 185-196 ◽  
Author(s):  
Carol I. Dell

A mineralogical study of the fine sand fraction of unweathered tills and stratified sands chosen to represent the deposits of the major ice lobes of southern Ontario was carried out. In addition, a few analyses were made of the coarse silt and coarser sands.In general there was the same variety of minerals in all samples and they varied only in their proportions. Tills overlying Palaeozoic bedrock contained abundant carbonates and shale fragments constituting up to 70 per cent of some fine sands. In the coarse sands, carbonates and shale increased sharply. In the coarse silt and fine sand, feldspars were more abundant than quartz whereas in the medium and coarse sand the reverse was true. Quartz increased in quantity with increasing grain size and reached a maximum in the medium sand. Heavy minerals usually constituted less than 15 per cent of the fine sand. Some of the minerals present in the coarse silt and fine sand were not found in the coarser sands. Usually the order of abundance of the heavy minerals was: hornblende, garnet, micas, magnetite, pyroxenes and sphene. Epidote, rutile, apatite, tourmaline, staurolite, kyanite and others were also noted. A chart listing the plant nutrient elements found in these minerals was prepared.


2021 ◽  
pp. 4791-4801
Author(s):  
Ali Ismail Al-Juboury ◽  
Noor Talal Al-Taee ◽  
Zaid A. Malak

     A mineralogical study using X-ray diffraction supported by scanning electron microscopic examination on the Paleocene- Eocene Kolosh and Gercus formations from northern Iraq is conducted to show the distribution of clay minerals and their paleoenvironmental implications. Smectite palygorskite, kaolinite, illite, and chlorite are commonly present in varying proportions within the Kolosh and Gercus formations. Association of smectite and chlorite in the claystone of the Paleocene Kolosh Formation refers to marine environment of this formation, whereas development of palygorskite fibers from smectite precursor may relate to post-depositional diagenesis. In addition, the abundance of illite and kaolinite in the Eocene Gercus Formation suggests a greater influence of terrigenous input in humid conditions, affecting the distribution of these clay minerals. The study shows vertical change in clay minerals distribution when illite and kaolinite dominate in the Eocene Gercus Formation, in comparison to chlorite and smectite abundance in the Paleocene Kolosh Formation which may relate to global warming in the Eocene.


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