scholarly journals Effect of scan speed on grain and microstructural morphology for laser additive manufacturing of 304 stainless steel

2021 ◽  
Vol 60 (1) ◽  
pp. 744-760
Author(s):  
Rongxia Chai ◽  
Yapu Zhang ◽  
Bin Zhong ◽  
Chuanwei Zhang
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Growth ◽  
Laser Scanning ◽  
Growth Direction ◽  
304 Stainless Steel ◽  
Laser Additive Manufacturing ◽  
Cladding Layer ◽  
Microstructural Morphology ◽  
Scan Speed

Abstract The laser scanning parameters used in laser additive manufacturing (LAM) can impact the growth direction of the columnar grains produced during rapid solidification. This growth direction affects the mechanical properties of the manufactured parts after cladding. The effective use of a high laser power and a rapid scanning speed for LAM requires an accurate analysis of the relationships between the laser scanning process parameters and the grain growth direction and microstructural morphology of the scanned material. An experimental study was conducted to determine the macromorphology, microstructural morphology, and grain growth direction of 304 stainless steel material obtained during the laser scanning process at different scan speeds. The impact of the scan speed on different regions in the cladding layer (the clad zone (CZ), the heat affected zone (HAZ), and the dilution zone (DZ)) was determined, as well as on the direction of grain growth, the grain morphology and the grain size (which are the microstructures of the cladded materials), the degree of elemental mixing during laser scanning (which are changes in material composition of cladded material), and the microscopic hardness of the CZ (which is one of the mechanical properties of cladded material). With increasing scan speed, the CZ, HAZ, DZ, and dilution rate (DR) of the material gradually decreased, and grain growth gradually oriented towards the building direction of the cladding layer. At a 16 mm·s−1 scan speed, the angle between the grain growth direction and the scan direction was 84°. Changing the scan speed from 4 to 16 mm·s−1 caused the columnar grain size to gradually decrease from 13.3 to 9.2 μm and the corresponding microhardness to gradually increase.

Mechanical Properties of Electroplated Copper Thin Films

1999 ◽  
Vol 594 ◽  
Author(s):  
R. Spolenak ◽  
C. A. Volkert ◽  
K. Takahashi ◽  
S. Fiorillo ◽  
J. Miner ◽  
...  
Keyword(s):  
Thin Films ◽  
Mechanical Properties ◽  
Grain Size ◽  
Film Thickness ◽  
Yield Stress ◽  
Laser Scanning ◽  
Focused Ion Beam ◽  
Ion Beam ◽  
Cu Films ◽  
Electroplated Copper

AbstractIt is well known that the mechanical properties of thin films depend critically on film thickness However, the contributions from film thickness and grain size are difficult to separate, because they typically scale with each other. In one study by Venkatraman and Bravman, Al films, which were thinned using anodic oxidation to reduce film thickness without changing grain size, showed a clear increase in yield stress with decreasing film thickness.We have performed a similar study on both electroplated and sputtered Cu films by using chemical-mechanical polishing (CMP) to reduce the film thickness without changing the grain size. Stress-temperature curves were measured for both the electroplated and sputtered Cu films with thicknesses between 0.1 and 1.8 microns using a laser scanning wafer curvature technique. The yield stress at room temperature was found to increase with decreasing film thickness for both sets of samples. The sputtered films, however, showed higher yield stresses in comparison to the electroplated films. Most of these differences can be attributed to the different microstructures of the films, which were determined by focused ion beam (FIB) microscopy and x-ray diffraction.

The Influence of High Magnetic Field on the Stability of CryoECAPed 1050 Alloy

2013 ◽  
Vol 774-776 ◽  
pp. 968-973
Author(s):  
Yi Heng Cao ◽  
Li Zi He ◽  
Xiao Tao Liu ◽  
Hai Tao Zhang ◽  
Ping Wang ◽  
...  
Keyword(s):  
Magnetic Field ◽  
Mechanical Properties ◽  
Grain Size ◽  
Diffraction Pattern ◽  
Grain Growth ◽  
High Magnetic Field ◽  
Hardness Test ◽  
Abnormal Grain Growth ◽  
Back Scattering ◽  
The Stability

The evolutions of mechanical properties and microstructure of cryoECAPed 1050 alloy annealed at various temperatures from 150°C to 400°C for 1h with and without high magnetic field (HMF) were investigated by hardness test and electron back scattering diffraction pattern (EBSD) analysis. The abnormal grain growth happens in sample annealing at 400°C without a field. With the application of high magnetic field, the formation of the HABs is suppressed, the grain size distribution is homogeneous and no abnormal grain growth occurs.

Effect of (Ni,Mo) and (W,Ti)C on the Microstructure and Mechanical Properties of TiB2 Ceramic Tool Materials

2012 ◽  
Vol 723 ◽  
pp. 233-237 ◽  
Author(s):  
Tong Chun Yang ◽  
Chuan Zhen Huang ◽  
Han Lian Liu ◽  
Bin Zou ◽  
Hong Tao Zhu ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Grain Size ◽  
Flexural Strength ◽  
Grain Growth ◽  
Vickers Hardness ◽  
Ceramic Tool ◽  
Tool Materials ◽  
Sintering Additive ◽  
Microstructure And Mechanical Properties

TiB2-(W,Ti)C composites with (Ni,Mo) as sintering additive have been fabricated by hot-pressing technique, and the microstructure and mechanical properties of the composites have been investigated. (Ni,Mo) promotes grain growth of the composites. In the case of 7vol.% (Ni,Mo), the grain size decreases consistently with an increase in the content of (W,Ti)C. When the proper content of (W,Ti)C is added to TiB2 composites, the growth of matrix grains is inhibited and the mechanical properties of the composites are improved. The best mechanical properties of the composites are 1084.13MPa for three-point flexural strength, 7.80MPa•m 1/2 for fracture toughness and 17.92GPa for Vickers hardness.

Influence of Al2O3 Addition on the Microstructure and Mechanical Properties of Pressureless Sintered Ce-TZP

2005 ◽  
Vol 492-493 ◽  
pp. 783-0 ◽  
Author(s):  
Shui Gen Huang ◽  
Lin Li ◽  
Jef Vleugels ◽  
Pei Ling Wang ◽  
Omer Van der Biest
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Grain Size ◽  
Grain Growth ◽  
Vickers Hardness ◽  
Good Combination ◽  
Al2o3 Content ◽  
Pressureless Sintering ◽  
Sintering Time ◽  
Microstructure And Mechanical Properties

Mixtures of 12 mol% CeO2-stabilised ZrO2 with 5 to 20 wt % Al2O3 were prepared and densified through pressureless sintering in air at 1450° C for 1 to 4 h. The influence of the Al2O3 content and sintering time on the phase constitution, microstructure and mechanical properties of the as-sintered composites were investigated. Fully dense Ce-TZP/Al2O3 ceramics with a good combination of hardness and fracture toughness can be obtained by pressureless sintering in air for only 1 h. The addition of Al2O3 to Ce-TZP improves the mechanical properties and suppresses ZrO2 grain growth. The average ZrO2 grain size increases with increasing sintering time and decreasing Al2O3 content. This leads to an increase in toughness. An excellent fracture toughness of 14.3 MPam1/2 in combination with a Vickers hardness of 9.14 GPa was obtained for 12 mol % CeO2-TZP with 5 wt % Al2O3, sintered for 4 h.

Microstructural Evolution and Mechanical Properties of Pure Magnesium during Multi-Axial Compression

2015 ◽  
Vol 713-715 ◽  
pp. 2759-2764 ◽  
Author(s):  
Xiao Hui Yang ◽  
Song Ni ◽  
Min Song
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Growth ◽  
Axial Compression ◽  
Microstructural Evolution ◽  
Pure Magnesium ◽  
Compression Tests ◽  
Axial Deformation ◽  
Lower Strain ◽  
Significant Difference

The effects of multi-axial compression (MAC) on the microstructures and mechanical properties of pure magnesium were investigated. It has been shown that grain refinement and grain growth occurred simultaneously during the MAC process. After 5 MAC passes, the grain size is mainly distributed in the range of 5~25 μm. The hardness of the specimens increases with increasing the strain (MAC pass), with the increment at lower strain being more obvious than that at higher strain. Compression tests showed that the samples show significant difference in mechanical properties along different directions due to the texture development. With increasing the MAC pass, the texture has been weakened due to multi-axial deformation.

Microstructure and Mechanical Properties of a Rapid Directionally Solidified Ti47Al Alloy

2011 ◽  
Vol 117-119 ◽  
pp. 217-221
Author(s):  
Rui Run Chen ◽  
Hong Sheng Ding ◽  
Jing Jie Guo ◽  
Yan Qing Su ◽  
Heng Zhi Fu
Keyword(s):  
Mechanical Properties ◽  
Compressive Strength ◽  
Grain Growth ◽  
Axial Direction ◽  
Longitudinal Section ◽  
Growth Direction ◽  
Directionally Solidified ◽  
Compressive Properties ◽  
Dendritic Core ◽  
Columnar Grains

The ingot of Ti47Al alloy was prepared by a newly developed rapid directional solidification, the microstructure and compressive properties of the ingot was observed and tested. The results show that the macrostructure consisted mainly of coarse columnar grains parallel to the axial direction, with the size of 0.5mm wide and 10mm in length. The direction of lamellar is almost perpendicular to the growth direction in the longitudinal section and no dendritic core is found. The average ultimate compressive strength of the specimens with grain growth parallel/perpendicular to the compressive direction is 1233.3 and 861.7 MPa respectively. The fracture mode for specimens with grain growth parallel to the compressive direction exhibits predominantly translamellar fracture, however, that for specimens with grain growth perpendicular to the compressive direction exhibits predominantly delamenation or interlamellar fracture.

Influence of Process Parameters on the Mechanical Response of Various Layers Processed Using Direct Metal Laser Sintering (DMLS)

2014 ◽  
Author(s):  
S. Ahmed ◽  
H. Doak ◽  
A. Mian ◽  
R. Srinivasan
Keyword(s):  
Mechanical Properties ◽  
Process Parameters ◽  
Laser Power ◽  
Laser Scanning ◽  
Mechanical Response ◽  
Scanning Speed ◽  
Direct Metal Laser Sintering ◽  
Influence Of Process Parameters ◽  
Microstructural Morphology ◽  
Laser Scanning Speed

During the DMLS process, sintering of the top layer creates melting and heat affected zone in previously sintered layers. In this paper, we will examine the effects of any given process parameter, such as laser power and laser scanning speed, on the mechanical properties and microstructural morphology within the processed layers.

Effect of CoO Doping on the Sintering Ability and Mechanical Properties of Y-TZP

2004 ◽  
Vol 449-452 ◽  
pp. 265-268 ◽  
Author(s):  
Tetsuhiko Onda ◽  
H. Yamauchi ◽  
Motozo Hayakawa
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Boundary ◽  
Grain Refinement ◽  
Grain Growth ◽  
Sintering Temperature ◽  
Tetragonal Zirconia ◽  
Boundary Structure ◽  
Grain Boundary Structure ◽  
Boundary Strength

The effect of CoO addition into Y-TZP (Yttria doped Tetragonal Zirconia Polycrystals) was studied on the evolution of its sintering ability, grain size, grain boundary structure and mechanical properties. The doping of a small amount of CoO effectively reduced the sintering temperature. A small amount of CoO up to ~ 0.3 mol% was effective for the suppression of grain growth, but the addition of 1.0 mole % resulted in an enhanced grain growth. The hardness and toughness of the CoO doped TZP were about the same as those of undoped TZP. Furthermore, despite the grain refinement, CoO doped TZP did not exhibit improved mechanical properties. This may be suggesting that CoO dopant had weakened the grain boundary strength.

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