Microstructural Evolution and Mechanical Properties of Pure Magnesium during Multi-Axial Compression

2015 ◽  
Vol 713-715 ◽  
pp. 2759-2764 ◽  
Author(s):  
Xiao Hui Yang ◽  
Song Ni ◽  
Min Song
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Growth ◽  
Axial Compression ◽  
Microstructural Evolution ◽  
Pure Magnesium ◽  
Compression Tests ◽  
Axial Deformation ◽  
Lower Strain ◽  
Significant Difference

The effects of multi-axial compression (MAC) on the microstructures and mechanical properties of pure magnesium were investigated. It has been shown that grain refinement and grain growth occurred simultaneously during the MAC process. After 5 MAC passes, the grain size is mainly distributed in the range of 5~25 μm. The hardness of the specimens increases with increasing the strain (MAC pass), with the increment at lower strain being more obvious than that at higher strain. Compression tests showed that the samples show significant difference in mechanical properties along different directions due to the texture development. With increasing the MAC pass, the texture has been weakened due to multi-axial deformation.

Production and Mechanical Properties of Nanocrystalline Intermetallics Based on TiAl3-X

2003 ◽  
Vol 791 ◽  
Author(s):  
H. A. Calderon ◽  
J. C. Aguilar-Virgen ◽  
F. Cruz-Gandarilla ◽  
M. Umemoto
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Growth ◽  
High Strength ◽  
Compression Tests ◽  
Grain Sizes ◽  
Intermetallic Materials ◽  
Plasma Sintering ◽  
Average Grain Size ◽  
Spark Plasma

ABSTRACTProduction of intermetallic materials in the system TiAl3-X (X = Cr, Mn, Fe) has been achieved by means of mechanical milling and sintering techniques. Spark plasma sintering is used since it reduces time at high temperature and inhibits grain growth. The produced materials have grain sizes in the nano and microscale depending on the material and processing variables. The TiAl3-X alloys are formed mostly by the cubic L12 phase. The average grain size ranges between 30 and 50 nm in the as sintered condition. Aging at elevated temperature has been used to promote grain growth. Compression tests have been performed to evaluate mechanical properties as a function of temperature and grain size. In all cases yield stresses higher that 700 MPa are obtained together with a ductility that depends upon temperature and grain size. No ductility is found for the smallest grains sizes tested (30 nm) at room temperature. Above 673 K, these materials show ductility and additionally they present a quasi superplastic behavior at temperatures higher that 973 K. On the other hand ductility can also be developed in the TiAl3-X alloys by inducing grain growth via annealing. Alloys with grains sizes around 500 nm show high ductility and a large density of microcraks after deformation suggesting that the yield strenght becomes lower than the stress to propagate the cracks. In such materials, a considerably high strength is retained up to 873 K.

Recrystallization and Grain Growth during Alloy 718 Processing

2007 ◽  
Vol 539-543 ◽  
pp. 3094-3099
Author(s):  
Nho Kwang Park ◽  
Jeoung Han Kim ◽  
Jong Taek Yeom
Keyword(s):  
Grain Size ◽  
Grain Growth ◽  
Heat Treatments ◽  
Grain Structure ◽  
Alloy 718 ◽  
Compression Tests ◽  
Δ Phase ◽  
Grain Boundary Characteristics ◽  
The Difference ◽  
Boundary Characteristics

In Alloy 718 ingot cogging process, dynamic and metadynamic recrystallizations, and static grain growth occur, and also the presence of δ phase plays a key role in controlling the grain size. In this study, the evolution of grain structure in VIM/VAR-processed Alloy 718 ingots during post-cogging heat treatments is dealt with. Compression tests were made on VIM/VAR-processed Alloy 718 ingot at temperatures between 900oC ~ 1150oC. Heat treatments were made on the compression-tested specimens, and the variation of grain size was evaluated. Constitutive equations for the grain growth are established to represent the evolution of microstructures. Special attention is paid to the evolution of grain structure under the condition of dynamic and metadynamic recrystallizations, and grain growth. The grain growth rate depends mainly on the presence of δ-phase below the δ-solvus temperature, and on the difference in the grain boundary characteristics above it.

Effect of Thermomechanical Processing on Grain Size, Texture and Mechanical Properties of Pure Magnesium

2020 ◽  
Vol 985 ◽  
pp. 97-108
Author(s):  
Mouhamadou Moustapha Sarr ◽  
Motohiro Yuasa ◽  
Hiroyuki Miyamoto
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Yield Stress ◽  
Thermomechanical Processing ◽  
Pure Magnesium ◽  
Grain Structure ◽  
Misorientation Distribution ◽  
Processed Material ◽  
Texture Characterization

This study aims to investigate the effect of processing routes (A and Bc) and temperature on microstructure, texture and mechanical properties of pure magnesium was studied in this research. An extruded pure magnesium (~99,9 %) was subjected to severe plastic deformation (SPD) by ECAP. Deformation was conducted at 523K and 473K and two different processing routes (A and Bc) were used to control the texture. The microstructure and texture characterization of the pressed materials were carried out. It was found that the microstructure displayed a bimodal grain structure after two passes and then became homogeneous after four passes following both routes A and Bc. The misorientation distribution was examined and the results revealed that the fraction of high angle grain boundaries (HAGB) was higher at temperature 473K. The texture was randomized following route Bc whereas it became strengthened in route A after four passes. According to the Hall-Petch (HP) relationship, the yield stress of polycrystalline metals increases with a decrease in grain size. In this study, a positive slope k was achieved in the strengthened texture while a negative one was obtained in the softened texture. The ductility of ECAP processed material was considerably improved (from 23% to 38%) without sacrificing the yield stress by route Bc at 423K.

scholarly journals Mechanical Properties of Dye 3 Greenland Deep Ice Cores

1984 ◽  
Vol 5 ◽  
pp. 1-8 ◽  
Author(s):  
Nobuhiko Azuma ◽  
Akira Higashi
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Power Law ◽  
Ice Core ◽  
Ice Cores ◽  
Uniaxial Stress ◽  
Strain Rates ◽  
Compression Tests ◽  
Polycrystalline Ice ◽  
Relationship Of

Uniaxial compression tests were carried out with specimens cut from several deep ice cores obtained at Dye 3, Greenland, in 1980 and 1981. The power law relationship of = Αση was obtained between the uniaxial strain-rate and the uniaxial stress σ. In a range of strain-rates between 10−8 and 10−7 s−1, the value of the power n for samples with strong single maximum fabric was approximately 4, significantly larger than the value of 3 which has been generally accepted from experiments using artificial polycrystalline ice. A work-hardening effect was found in the ice-core samples taken from a depth of 1900 m, which had a smaller grain size than the others. Recrystallization occurred when the temperature of the specimen was raised during the test and this ultimately caused the formation of the so-called diamond pattern ice fabric.

scholarly journals Microstructural Evolution and Mechanical Properties of Friction Stir Welded Butt Joints of 5A06 Alloy Ultra-Thin Sheets

Materials ◽  
2019 ◽  
Vol 12 (23) ◽  
pp. 3906 ◽  
Author(s):  
Yang Han ◽  
Xiaoqing Jiang ◽  
Tao Yuan ◽  
Shujun Chen ◽  
Dongxiao Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Boundaries ◽  
Microstructural Evolution ◽  
Welding Speed ◽  
Base Material ◽  
Thin Plates ◽  
Al Alloy ◽  
Minimum Thickness ◽  
Friction Stir

Ultra-thin plates have great potential for applications in aircraft skin, the packaging industry, and packaging of electronic products. Herein, 1 mm-thick 5A06 Al alloy was welded with friction stir welding. The microstructural evolution of the welds was investigated in detail with optical microscopy, scanning electron microscopy, and electron backscatter diffraction. The results showed that the friction stir welds of 1 mm-thick 5A06 Al alloy were well formed without obvious defect and with a minimum thickness reduction of 0.025 mm. Further, the grain size and the proportion of low-angle grain boundaries decreased with decreasing welding speed, because of the increasing degree of dynamic recrystallization. Among all of the welded joints, the welding speed of 100 mm/min yielded the smallest grain size and the highest proportion of high-angle grain boundaries, and thus the best mechanical properties. Specifically, the tensile strength of the joint was greater than that of the base material, while the elongation reached 80.83% of the base material.

Hot Deformation Behavior and Microstructure of U720Li Alloy

2013 ◽  
Vol 709 ◽  
pp. 143-147 ◽  
Author(s):  
Tao Wang ◽  
Zhao Li ◽  
Shu Hong Fu ◽  
Yong Zhang ◽  
Yu Xin Zhao ◽  
...  
Keyword(s):  
Grain Size ◽  
Flow Stress ◽  
Strain Rate ◽  
Hot Deformation ◽  
Deformation Behavior ◽  
Primary Phase ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
Fine Grain ◽  
Lower Strain

The hot deformation behavior of U720Li was investigated by isothermal compression tests at temperature ranging from 1060-1180°C and strain rate from 0.001s-1 to 20s-1. The flow stress-strain curves and microstructures were investigated and a constitutive equation was established. It is found that flow stress is sensitive to stain rate and deformation temperature greatly. The higher stain rate resultes in a larger fluctuation in flow stress. The hot deformation activation energy is determined to be 552.8kJ/mol. Grain size increases with increasing temperature and decreases firstly and then increases with increasing strain rate. U720Li alloy should be deformed below the solve temperature of γ primary phase with lower strain rate in order to obtain the even and fine grain size.

The Influence of High Magnetic Field on the Stability of CryoECAPed 1050 Alloy

2013 ◽  
Vol 774-776 ◽  
pp. 968-973
Author(s):  
Yi Heng Cao ◽  
Li Zi He ◽  
Xiao Tao Liu ◽  
Hai Tao Zhang ◽  
Ping Wang ◽  
...  
Keyword(s):  
Magnetic Field ◽  
Mechanical Properties ◽  
Grain Size ◽  
Diffraction Pattern ◽  
Grain Growth ◽  
High Magnetic Field ◽  
Hardness Test ◽  
Abnormal Grain Growth ◽  
Back Scattering ◽  
The Stability

The evolutions of mechanical properties and microstructure of cryoECAPed 1050 alloy annealed at various temperatures from 150°C to 400°C for 1h with and without high magnetic field (HMF) were investigated by hardness test and electron back scattering diffraction pattern (EBSD) analysis. The abnormal grain growth happens in sample annealing at 400°C without a field. With the application of high magnetic field, the formation of the HABs is suppressed, the grain size distribution is homogeneous and no abnormal grain growth occurs.

Microstructural Evolution of Synthetic Forsterite Aggregates Deformed to High Strain

2004 ◽  
Vol 467-470 ◽  
pp. 579-584 ◽  
Author(s):  
A. Kellermann Slotemaker ◽  
J.H.P. de Bresser ◽  
C.J. Spiers ◽  
M.R. Drury
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Grain Growth ◽  
Microstructural Evolution ◽  
Large Scale ◽  
High Strain ◽  
Confining Pressure ◽  
Size Reduction ◽  
Coarse Grained ◽  
Fine Grained

Microstructures provide the crucial link between solid state flow of rock materials in the laboratory and large-scale tectonic processes in nature. In this context, microstructural evolution of olivine aggregates is of particular importance, since this material controls the flow of the Earth’s upper mantle and affects the dynamics of the outer Earth. From previous work it has become apparent that if olivine rocks are plastically deformed to high strain, substantial weakening may occur before steady state mechanical behaviour is approached. This weakening appears directly related to progressive modification of the grain size distribution through competing effects of dynamic recrystallization and syn-deformational grain growth. However, most of our understanding of these processes in olivine comes from tests on coarse-grained materials that show grain size reduction through dynamic recrystallization. In the present study we focused on fine-grained (~1 µm) olivine aggregates (i.e., forsterite/Mg2SiO4), containing ~0.5 wt% water and 10 vol% enstatite (MgSiO3), Samples were axially compressed to varying strains up to a maximum of ~45%, at 600 MPa confining pressure and a temperature of 950°C. Microstructures were characterized by analyzing full grain size distributions and textures using SEM/EBSD. We observed syndeformational grain growth rather than grain size reduction, and relate this to strain hardening seen in the stress-strain curves.

Influence of Mg Content, Grain Size and Strain Rate on Mechanical Properties and DSA Behavior of Al-Mg Alloys Processed by ECAP and Annealing

2014 ◽  
Vol 794-796 ◽  
pp. 870-875 ◽  
Author(s):  
Min Zha ◽  
Yan Jun Li ◽  
Ragnvald H. Mathiesen ◽  
Christine Baumgart ◽  
Hans J. Roven
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Strain Rate ◽  
Room Temperature ◽  
Uniform Elongation ◽  
Mg Alloys ◽  
Lower Strain Rate ◽  
Lower Strain ◽  
Mg Content ◽  
Al Mg Alloys

Ultrafine-grained (UFG) binary Al-xMg (x=1, 5 and 7 wt %) alloys were processed by equal channel angular pressing (ECAP) at room temperature via route Bccombined with inter-pass annealing. The effects of Mg content, grain size and strain rate on mechanical properties and dynamic strain aging (DSA) behaviour of the Al-Mg alloys upon tensile testing at room temperature were studied. An increase in Mg content from 5 to 7 wt % leads to a pronounced increase in strength and uniform elongation in both the as-homogenized and as-ECAP Al-Mg alloys. Thereby, the Al-7Mg alloy, either prior to or after ECAP processing, possess significantly higher strength and comparable or even higher uniform elongation than the more dilute Al-Mg alloys. However, the as-ECAP Al-Mg alloys exhibit significantly higher strength but little work hardening and hence rather limited uniform elongation. In general, decreasing grain size leads to significant increase in strength while dramatic decrease in ductility. Moreover, DSA serration amplitudes increase with reducing grain size in the micrometer range. However, the UFG Al-Mg alloys exhibit much less DSA effect than the micrometer scaled grain size counterparts, i.e. probably due to the high dislocation densities and special grain boundary features in the UFG materials. Also, the Al-Mg alloys, especially those with a UFG structure, exhibit higher strength and ductility at lower strain rate than at higher strain rate, due mainly to enhanced DSA effect and hence work hardening at a lower strain rate.

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